CN206081753U - Horizontal profit phase splitter - Google Patents
Horizontal profit phase splitter Download PDFInfo
- Publication number
- CN206081753U CN206081753U CN201621127788.3U CN201621127788U CN206081753U CN 206081753 U CN206081753 U CN 206081753U CN 201621127788 U CN201621127788 U CN 201621127788U CN 206081753 U CN206081753 U CN 206081753U
- Authority
- CN
- China
- Prior art keywords
- phase
- splitter
- horizontal
- water
- oil phase
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 50
- 210000005239 tubule Anatomy 0.000 claims abstract description 17
- 239000000945 filler Substances 0.000 claims description 9
- 238000003825 pressing Methods 0.000 claims description 9
- 238000007747 plating Methods 0.000 claims description 8
- 230000006641 stabilisation Effects 0.000 claims description 7
- 238000011105 stabilization Methods 0.000 claims description 7
- 238000012856 packing Methods 0.000 claims description 4
- 239000011148 porous material Substances 0.000 claims description 3
- 238000010276 construction Methods 0.000 claims description 2
- 239000000463 material Substances 0.000 claims description 2
- 238000003466 welding Methods 0.000 claims description 2
- 239000012071 phase Substances 0.000 abstract description 47
- 238000004581 coalescence Methods 0.000 abstract description 11
- 238000000926 separation method Methods 0.000 abstract description 11
- 230000000694 effects Effects 0.000 abstract description 8
- 239000008346 aqueous phase Substances 0.000 abstract 2
- 230000008676 import Effects 0.000 abstract 1
- 235000019198 oils Nutrition 0.000 description 38
- 239000007788 liquid Substances 0.000 description 14
- 238000000034 method Methods 0.000 description 14
- 238000007600 charging Methods 0.000 description 6
- 230000008569 process Effects 0.000 description 5
- 239000012074 organic phase Substances 0.000 description 4
- 238000005265 energy consumption Methods 0.000 description 3
- 230000005484 gravity Effects 0.000 description 3
- 238000012423 maintenance Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 235000019476 oil-water mixture Nutrition 0.000 description 3
- 238000011953 bioanalysis Methods 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 238000005192 partition Methods 0.000 description 2
- WQKGAJDYBZOFSR-UHFFFAOYSA-N potassium;propan-2-olate Chemical compound [K+].CC(C)[O-] WQKGAJDYBZOFSR-UHFFFAOYSA-N 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- 230000004888 barrier function Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000003139 buffering effect Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000004080 punching Methods 0.000 description 1
- 238000000066 reactive distillation Methods 0.000 description 1
- 230000008439 repair process Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Removal Of Floating Material (AREA)
Abstract
The utility model discloses a horizontal profit phase splitter, including entry, phase splitter body, export to and it is regional to lie in these internal stationary flow parts of phase splitter, coalescence parts and gravitational settling, and the export includes feeding member, water drum and prevent baffle soon including oil phase and aqueous phase outlet, stationary flow parts that the feeding member lies in jar vertical position of body head the import is managed and is taken over, takes over the bottom and sets up a weep hole, and the takeover of stretching into inside lower part of phase splitter or well lower part sets up a plurality of tubules that stretch out the endcapped all over the body, and horizontal the opening of tubule intermediate position level has symmetrical aperture, it prevents baffle soon to be provided with the cross in the stationary flow part directly over the water drum of aqueous phase outlet upper end, the utility model discloses a mixed phase velocity of flow can be slowed down to this structure, can effectively avoid the turbulent fluctuation of rivers, improves whole coalescence effect, and the cross prevents that the baffle can avoid the discharge water phase time to produce the phenomenon of turning round and round with the combination of water drum soon, eliminates the shortcoming of the easy disturbance of interface, draws clean oil phase, improves separation efficiency.
Description
Technical field
The utility model is related to a kind of water-oil phase separator, and in particular to one kind is mainly used in pharmaceutical industry extraction
The profit phase-splitter of oil phase.
Background technology
In fields such as chemical industry, pharmacy, environmental protection, oily water separating equipment is important production equipment, and isolation technics is sent out industry
Exhibition is most important.With industrial expansion and the attention to environmental protection, oily water separation technique receives much concern.
In the reactive distillation process of potassium isopropoxide synthesis, tower is looped back through the detached organic phase solution of phase-splitter, if
The too high levels of water can suppress the synthesis of potassium isopropoxide in the part organic phase solution, so as to extend manufacture cycle and increased product
Product energy consumption, it is therefore desirable to which the cleaning of organic phase is ensured using efficient separation method.
Water-oil separating belongs to the category of Liquid liquid Separation, and separation process is more complicated.The method of water-oil separating has many kinds, but
It is the requirement for needing existence and process according to oil in water, water-oil separating is carried out using different methods.It is currently known
Oil-water separation method mainly have：Gravity separate, centrifugal partition method, bioanalysis, coarse separation method etc..
The principle of coalescence method is：Utilize " shallow pond " principle that dispersed phase drop is fallen under gravity coalescing medium table
Face, and the process such as adsorb, soak, colliding, coalescing, makes dispersed phase drop collide to form big drop or liquid film, in gravity and
In the presence of flow of fluid, liquid film or big drop are removed from coalescing medium surface, so as to realize separating.
Coalescence method is compared with settling methods, and separative efficiency is higher, can more efficient process mixed liquor, to tankage
Dimensional requirement is relatively low；Compare with centrifugal partition method, the energy consumption for coalescing method is relatively low with maintenance cost；Compared with bioanalysis,
The disposal ability of coalescence method is bigger.
Chinese utility model patent CN201320084484.3 discloses oily water separating equipment, introduction member, current stabilization component,
Coalescent pack, oil phase overflow component are located in tank body, and water mutually produces component positioned at tank body outside；Be provided with tank body charging aperture,
Drain, oil phase outlet, water are mutually exported and manhole；Charging aperture is located above introduction member, drain is located at introduction member lower end,
Oil phase outlet is mutually exported positioned at oil phase outlet downside, positioned at current stabilization left member side tank body positioned at top, the water of introduction member offside
The manhole of top；Introduction member is located at inner tank wall downside, and current stabilization component is located between introduction member and coalescent pack, through tank
Up and down, the 1/3 of whole tank body is filled in coalescent pack to body, and oil phase overflow component is located on introduction member offside tank body, and water is mutually produced
Component is on the outside of oil phase overflow component tank body.
In the technical scheme, inlet component includes horizontal feed distributor and vertical liquid barrier, causes water-oil separating
The Flow Field Distribution of device entrance is uneven, and vortex is there is behind baffle plate, affects the coalescence effect of oil phase；Current stabilization component is adopted
With the metal sieve plate of perforate, separator interior liquid stream is difficult to be evenly distributed in vertical direction, causes oil-water separation not good；It is poly-
Structural member adopts the corrugated plating of perforate, it is difficult to improve droplet coalescence effect.
Utility model content
The purpose of this utility model is to overcome the shortcoming in prior art, there is provided a kind of Operation and Maintenance is more convenient, take
With oily water separating equipment cheaper, that separation oil phase is cleaner.
The utility model is to be achieved through the following technical solutions：
A kind of horizontal profit phase-splitter, including entrance, phase-splitter body, outlet, and it is intrinsic steady positioned at phase-splitter
Stream unit, aggregated component and gravitational settling region, outlet includes that oil phase outlet is mutually exported with water, and current stabilization part includes charging structure
Part, water bag, swirl reducting baffle, filler pressing and fixed plate, filler pressing is located between introduction member and aggregated component, and fixed plate exists
Between aggregated component and gravitational settling region, filler pressing and fixed plate are and phase-splitter body internal diameter identical sieve plate, described
Water mutually export immediately below the water bag, oil phase outlet positioned at the outside top of phase-splitter body tail section end socket, positioned at afterbody envelope
The top in the centre position of head, introduction member is located at phase-splitter body head vertical position, including inlet tube and adapter, described
Adapter bottom arranges a drain hole, and pore diameter range is 6～8mm, and the adapter whole body for stretching into the bottom inside phase-splitter or middle and lower part sets
Put it is multiple stretch out tubule, tubule endcapped, and tubule centre position horizontal cross is provided with symmetrical aperture.
Preferably, the phase-splitter body is horizontal tank body, and swirl reducting baffle is cross, is arranged on water and mutually exports upper end water
The surface of bag.
Preferably, the profit phase-splitter also includes oil phase overflow component, and oil phase overflow modular level is welded in tank body tail
Centre inside portion's end socket.
Preferably, the diameter of the oil phase overflow modular level welded plate is equal to tank body internal diameter.
Preferably, the plate of the baffle plate vertical portion of described oil phase overflow component is highly the 2/3 of tank interior diameter
～3/4.
Preferably, described aggregated component for sandwich construction not perforate mellapak packing, every layer of corrugated plating spacing be 4～
6mm。
Preferably, described aggregated component is corrosion resistant plate ripple packing, and corrugated plating and horizontal line angle are 45 °～60 °.
Preferably, the 1/2～3/4 of whole tank body is filled in described coalescent pack.
Preferably, the outlet also includes the emptying mouth of pipe, and the emptying mouth of pipe is located at phase-splitter body tail section top.
Because the utility model employs the technical scheme of the above, what it was produced has the technical effect that significantly：
1) introduction member that the utility model is adopted, the adapter whole body for stretching into the bottom inside phase-splitter or middle and lower part is arranged
It is multiple to stretch out tubule, tubule endcapped, and tubule centre position horizontal cross is provided with symmetrical aperture, so as to slow down mixed phase flow
Speed, can be prevented effectively from the turbulent fluctuation of current, improve overall coalescence effect.
2) introduction member that the utility model is adopted is used with coalescent pack collocation of not punching, and improve equipment flow behavior,
Separator interior liquid stream is uniformly distributed in vertical direction, prevent short circuit and the channel of liquid stream, improve water-oil separating
Efficiency.
3) produce when the cross swirl reducting baffle that the utility model is adopted can avoid discharging water phase with the combination of water bag and beat
Rotation phenomenon, eliminates the shortcoming of interface easily disturbance, and improves drainage efficiency.
The utility model can avoid aqueous in organic phase, and then extract clean oil phase, shorten the production cycle, reduce energy
Consumption, can be simultaneously reached discharge standard, obtain certain economic benefit.
Description of the drawings
Fig. 1 is the structural representation of the one of embodiment of the utility model.
Fig. 2 is the structural representation of the introduction member of the one of embodiment of the utility model.
The structural representation that Fig. 3 is closed for the swirl reducting baffle of the one of embodiment of the utility model with water package.
In figure：1- cover flanges, 2- tank bodies, the 3- mouths of pipe, 4- introduction members, 5- filler pressings, 6- coalescent packs, 7- is fixed
Plate, the 8- emptying mouths of pipe, 9- oil phases outlet, 10- oil phase overflow components, 11- water is mutually exported, 12- water bags, 13- swirl reducting baffles, 14-
Movable bearing support, 15- gravitational settlings region, 16- adapters, 17- drain holes, 18- stretches out tubule, the aperture on 19- tubules, 20- chargings
The inlet tube of component.
Specific embodiment
In conjunction with accompanying drawing detailed process of the present utility model and effect are illustrated by implementation below.
As shown in drawings, a kind of horizontal profit phase-splitter of the utility model, by cover flange 1, tank body 2, the mouth of pipe 3, charging
Component 4, filler pressing 5, coalescent pack 6, fixed plate 7, the emptying mouth of pipe 8, oil phase outlet 9, oil phase overflow component 10, water is mutually exported
11, water bag 12, swirl reducting baffle 13, movable bearing support 14, gravitational settling region 15 is constituted；Wherein tank body 2 is metal or other materials
Cylinder, be connected to outside tank body 2 cover flange 1, introduction member 4, emptying the mouth of pipe 8, oil phase outlet 9, water mutually export 11, Shui Bao
12nd, movable bearing support 14.Cover flange 1 is located at introduction member left side, the emptying mouth of pipe 8 and is located at tank body upper rear；Oil phase overflow structure
The level of part 10 is welded in the centre inside the afterbody end socket of tank body 2；Oil phase outlet 9 is located at the outside top of the afterbody end socket of tank body 2, position
In the top in the centre position of afterbody end socket；Cross swirl reducting baffle 13 is placed in directly over water bag 12；Water mutually exports 11 and is located at water
Immediately below bag 12, the diameter of the horizontal welded plate of oil phase overflow component 10 is equal to tank body internal diameter；Movable bearing support 14 is located at the bottom of tank body 2
Portion；The 1/2～3/4 of whole tank body is filled in coalescent pack 6.Described tank body 2 is the container of the similar horizontal tank of profile, is needed
Bright, tank body is a type of phase-splitter body.
The plate of the baffle plate vertical portion of oil phase overflow component 10 is highly the 2/3～3/4 of the inside diameter of tank body 2.
Introduction member 4 is located at the head upright position of tank body 2, including the inlet tube 20 of introduction member and stretches into tank interior
Bottom or the middle and lower part whole body arrange multiple adapters 16 for stretching out tubule 18, the endcapped of tubule 18, and the centre position water of tubule 18
It is flat to be laterally provided with symmetrical aperture 19, the drain hole 17 that bottom is provided with 6～8mm of pore diameter range is taken over, the structure of feed pipe can be further
Distribution liquid flowing, plays buffering liquid charging, is allowed to the effect being evenly distributed.
Most of tank body 2 is filled in coalescent pack 6, is not perforate on corrugated plate packing, and corrugated plating, corrugated plating and level
Wire clamp angle is 45 °～60 °, and every layer of corrugated plating spacing is 4～6mm, oil water mixture through this modes of emplacement coalescent pack,
Dispersion phase can fully be collided, coalesced, and internal liquid is evenly distributed in vertical direction, so as to reach the purpose of profit layering.
The level of overflow component 10 is welded in the centre inside the afterbody end socket of tank body 2, is made up of two baffle plates, so as to oil phase
Baffle plate is crossed in overflow, improves oil phase clean level.
Water bag 12 has thereon cross swirl reducting baffle 13 on the downside of the afterbody of tank body 2, and lower section welding water mutually exports 11；End socket
Flange 1 can improve oily water separating equipment is cleaned and repair and maintenance convenience.
When using, oil water mixture carries out water-oil separating by introduction member 4 with certain flow rate into oil water separator, according to
It is secondary by introduction member 4, filler pressing 5, coalescent pack 6 and fixed plate 7, oil water mixture arranges multiple overhanging through the whole body
Tubule 18 slow down after liquid velocity, in coalescent pack section 6 after coarse separation, oil phase overflow across overflow component 10 top oil
Mutually outlet 9 is discharged, and after cross swirl reducting baffle 13 slows down, is suitably buffered in stream water inlet bag 12, and oil phase exports 9 normally opened, water
Mutually outlet 11 is normally closed, after final oil phase is from the emptying of the mouth of pipe 9, then the valve discharge water phase for opening 11 adapters.So as to realize profit
Separation, obtain clean oil phase, water is mutually discharged up to standard.
The utility model a kind of horizontal profit phase-splitter newly developed, using shallow pool principle and coalescence principle, using special
Inside separating component, it is ensured that in certain volume of equipment, oil droplet buoyance lift area can be improved, increase oil droplet coalescence efficiency, and
The oil droplet in water is set to coalesce in buoyance lift, the buoyance lift in coalescence, and internal liquid is evenly distributed in vertical direction, it is therefore prevented that liquid
The short circuit of stream and channel, can obtain higher separating effect within the shorter time of staying, obtain clean oil phase.
Embodiments above is merely to illustrate and unrestricted the technical solution of the utility model.Without departing from the utility model essence
Any modification or partial replacement of god, all should cover in the middle of right of the present utility model.
Claims (9)
1. a kind of horizontal profit phase-splitter, including entrance, phase-splitter body, outlet, and positioned at the intrinsic current stabilization of phase-splitter
Part, aggregated component and gravitational settling region, outlet include oil phase outlet mutually export with water, current stabilization part including introduction member,
Water bag, swirl reducting baffle, filler pressing and fixed plate, filler pressing is located between introduction member and aggregated component, and fixed plate is poly-
Between knot part and gravitational settling region, filler pressing and fixed plate are and phase-splitter body internal diameter identical sieve plate, described
Water is mutually exported immediately below water bag, the top in centre position of the oil phase outlet on the outside of phase-splitter body tail section end socket, is entered
Material component is located at phase-splitter body head vertical position, including inlet tube and adapter, it is characterised in that：Described adapter bottom sets
A drain hole is put, pore diameter range is 6～8mm, the adapter whole body for stretching into the bottom inside phase-splitter or middle and lower part arranges multiple stretching out
Tubule, tubule endcapped, and tubule centre position horizontal cross is provided with symmetrical aperture.
2. a kind of horizontal profit phase-splitter as claimed in claim 1, it is characterised in that：The phase-splitter body is horizontal tank
Body, swirl reducting baffle is cross, is arranged on the surface that water mutually exports upper end water bag.
3. a kind of horizontal profit phase-splitter as claimed in claim 2, it is characterised in that：The profit phase-splitter also includes oil phase
Overflow component, oil phase overflow modular level is welded in the centre inside tank body afterbody end socket.
4. a kind of horizontal profit phase-splitter as claimed in claim 3, it is characterised in that：The oil phase overflow modular level welding
The diameter of plate is equal to tank body internal diameter.
5. a kind of horizontal profit phase-splitter as claimed in claim 3, it is characterised in that：The baffle plate of described oil phase overflow component
The plate of vertical portion is highly the 2/3～3/4 of tank interior diameter.
6. a kind of horizontal profit phase-splitter as claimed in claim 2, it is characterised in that：Described aggregated component is sandwich construction
Not perforate mellapak packing, every layer of corrugated plating spacing is 4～6mm.
7. a kind of horizontal profit phase-splitter as claimed in claim 6, it is characterised in that：Described aggregated component corrugated plating and water
Horizontal line angle is 45 °～60 °.
8. a kind of horizontal profit phase-splitter as claimed in claim 7, it is characterised in that：Whole tank is filled in described coalescent pack
The 1/2～3/4 of body.
9. a kind of horizontal profit phase-splitter as described in any one of claim 1-8, it is characterised in that：The outlet also includes putting
Blank pipe mouth, the emptying mouth of pipe is located at phase-splitter body tail section top.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621127788.3U CN206081753U (en) | 2016-10-17 | 2016-10-17 | Horizontal profit phase splitter |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621127788.3U CN206081753U (en) | 2016-10-17 | 2016-10-17 | Horizontal profit phase splitter |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206081753U true CN206081753U (en) | 2017-04-12 |
Family
ID=58484139
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621127788.3U Expired - Fee Related CN206081753U (en) | 2016-10-17 | 2016-10-17 | Horizontal profit phase splitter |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206081753U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106422420A (en) * | 2016-10-17 | 2017-02-22 | 青岛科技大学 | Horizontal type oil and water phase separator |
-
2016
- 2016-10-17 CN CN201621127788.3U patent/CN206081753U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106422420A (en) * | 2016-10-17 | 2017-02-22 | 青岛科技大学 | Horizontal type oil and water phase separator |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170412 Termination date: 20191017 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |