CN206064399U - Continuous nitrification automaton - Google Patents

Continuous nitrification automaton Download PDF

Info

Publication number
CN206064399U
CN206064399U CN201620901956.3U CN201620901956U CN206064399U CN 206064399 U CN206064399 U CN 206064399U CN 201620901956 U CN201620901956 U CN 201620901956U CN 206064399 U CN206064399 U CN 206064399U
Authority
CN
China
Prior art keywords
nitrator
pump housing
motor
liquid level
automaton
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201620901956.3U
Other languages
Chinese (zh)
Inventor
马建华
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hubei Snow Fly Chemical Co Ltd
Original Assignee
Hubei Snow Fly Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hubei Snow Fly Chemical Co Ltd filed Critical Hubei Snow Fly Chemical Co Ltd
Priority to CN201620901956.3U priority Critical patent/CN206064399U/en
Application granted granted Critical
Publication of CN206064399U publication Critical patent/CN206064399U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Mixers Of The Rotary Stirring Type (AREA)

Abstract

This utility model provides a kind of continuous nitrification automaton.Include a nitrator, nitrator is built with agitating device, motor is installed at the top of nitrator, bottom passes through the pipeline communication pump housing, one liquid level sensor is installed on the left of described nitrator, right side is provided with a temperature sensor, and wherein liquid level sensor, temperature sensor and motor is all connected with controller;Liquid level warning module and temperature alarming module are installed in described controller;The described pump housing is connected with pump housing activate switch, pump housing activate switch connection controller.This utility model simple structure, can be stirred automatically according to the change of temperature and liquid level, reduce energy resource consumption, and improve production efficiency reduces security risk.

Description

Continuous nitrification automaton
Technical field
This utility model is related to nitrify equipment technical field, is related specifically to a kind of continuous nitrification for experimental branch line certainly Dynamic control device.
Background technology
Nitration reaction is that nitro is introduced in organic molecule(-NO2)Course of reaction.Aliphatic compound has when nitrifying The side reaction of oxidation-scission of link, it is industrial seldom to adopt.Nitromethane, nitroethane, four kinds of nitroparaffin hydrocarbon gas of 1- and 2- nitropropanes Phase method production process, is the american goods solvent company exploitation thirties.The method is still to produce the main work of nitroparaffins so far Industry method.Additionally, nitrification also refers to the forming process of nitrogen oxide.
Nitrifying process is carried out in the liquid phase, generally using tank reactor.According to nitrating agent and the difference of medium, can adopt Enamel still, steel kettle, cast iron kettle or rustless steel kettle.With during mixed acid nitrification in order to remove reaction heat as soon as possible to keep suitable reaction Temperature, in addition to cooling down using chuck, also installs cooling worm in kettle.The little nitrifying process of yield adopts intermittently operated mostly. The big nitrifying process of yield can be operated continuously, and using autoclave continuous nitrification reactor or ring-like continuous nitrification reactor, carry out many Platform series connection completes nitration reaction.The advantage of ring-like continuous nitrification reactor is that heat transfer area is big, and stirring is good, and production capacity is big, Many nitro compounds of by-product and nitrophenols are few.
Nitrator refers to that for carrying out the reactor of nitration reaction the tank reactor for generally being stirred using band by kettle, is stirred Mix the composition such as device, actuating device, chuck or coiled pipe (being heated or cooled if desired).Nitrator is generally intermittently operated, material Added in kettle by top, promptly mix in the presence of agitator and carry out nitration reaction.If necessary to heat, can be in chuck Or steam in coiled pipe, is passed through, if necessary to cool down, cooling water or cryogen can be passed through.
Existing nitrator is generally single chamber nitrator, and artificial constantly charging is needed during use, and in order to ensure Nitration reaction it is abundant, in addition it is also necessary to be stirred for a long time, will also be according to the change of liquid level and temperature, to stirring during stirring Mix speed to be adjusted, the safety of production efficiency and personnel has been had a strong impact on using traditional nitrator.
The content of the invention
Technical problem to be solved in the utility model is the defect for overcoming prior art, there is provided a kind of simple structure, energy It is enough to be stirred according to the change of temperature and liquid level automatically, energy resource consumption is reduced, improve production efficiency reduces the company of security risk Continuous nitrification automaton.
To achieve these goals, this utility model is employed the following technical solutions:
Continuous nitrification automaton, includes a nitrator, nitrator built with agitating device, at the top of nitrator Motor is installed, bottom passes through the pipeline communication pump housing, it is characterised in that a level sensing is provided with the left of described nitrator Device, right side are provided with a temperature sensor, and wherein liquid level sensor, temperature sensor and motor is all connected with controller;It is described Controller in liquid level warning module and temperature alarming module are installed;The described pump housing is connected with pump housing activate switch, the pump housing Activate switch connects controller.
In such scheme, described motor is servomotor, and the control of the controlled device of motor is started or closed, electric Heat ray filter is installed between machine and nitrator.
In such scheme, described agitating device includes a main shaft and the stirring vane on main shaft, stirs It is horizontally disposed to mix blade, and equidistantly distribute on main shaft, and stirring vane is shaped as banding.
This utility model is had the advantages that as a result of above-mentioned technical proposal:
This utility model simple structure, can be stirred automatically according to the change of temperature and liquid level, reduce energy resource consumption, Improve production efficiency, reduces security risk.
Description of the drawings
Fig. 1 is the overall structure figure of this utility model embodiment;
In figure:1 nitrator, 2 motors, 3 pump housings, 4 liquid level sensors, 5 temperature sensors, 6 controllers, 7 pump housings start to be opened Close.
Specific embodiment
In order that content of the present utility model is readily apparent understood, below according to specific embodiment and with reference to attached Figure, is described in further detail to this utility model.
Continuous nitrification automaton, includes a nitrator 1 as shown in Figure 1, and nitrator 1 is built with stirring dress Put, motor 2 is installed at the top of nitrator 1, bottom is provided with a liquid by the pipeline communication pump housing 3 on the left of described nitrator 1 Level sensor 4, right side are provided with a temperature sensor 5, and wherein liquid level sensor 4, temperature sensor 5 and motor 2 is all connected with Controller 6;Liquid level warning module and temperature alarming module are installed in described controller 6;The described pump housing 3 is connected with the pump housing Activate switch 7, the connection controller 6 of pump housing activate switch 7.
In the present embodiment, described motor 2 is servomotor, and the control of 2 controlled device 6 of motor started or closed Close, heat ray filter is installed between motor 2 and nitrator 1.
In the present embodiment, described agitating device includes a main shaft and the stirring vane on main shaft, stirs It is horizontally disposed to mix blade, and equidistantly distribute on main shaft, and stirring vane is shaped as banding.
Particular embodiments described above, the technical problem solved to this utility model, technical scheme and beneficial effect are entered Go further description, it is be should be understood that to the foregoing is only specific embodiment of the utility model, and without It is in this utility model is limited, all within spirit of the present utility model and principle, any modification, equivalent substitution and improvements done Deng should be included within protection domain of the present utility model.

Claims (3)

1. continuous nitrification automaton, includes a nitrator, and nitrator is pacified at the top of nitrator built with agitating device Equipped with motor, bottom passes through the pipeline communication pump housing, it is characterised in that a level sensing is provided with the left of described nitrator Device, right side are provided with a temperature sensor, and wherein liquid level sensor, temperature sensor and motor is all connected with controller;It is described Controller in liquid level warning module and temperature alarming module are installed;The described pump housing is connected with pump housing activate switch, the pump housing Activate switch connects controller.
2. continuous nitrification automaton as claimed in claim 1, it is characterised in that:Described motor is servomotor, The control of the controlled device of motor is started or is closed, and heat ray filter is provided between motor and nitrator.
3. continuous nitrification automaton as claimed in claim 1, it is characterised in that:Described agitating device includes one Root main shaft and the stirring vane on main shaft, stirring vane are horizontally disposed, and are equidistantly distributed on main shaft, paddle Piece is shaped as banding.
CN201620901956.3U 2016-08-19 2016-08-19 Continuous nitrification automaton Expired - Fee Related CN206064399U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201620901956.3U CN206064399U (en) 2016-08-19 2016-08-19 Continuous nitrification automaton

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201620901956.3U CN206064399U (en) 2016-08-19 2016-08-19 Continuous nitrification automaton

Publications (1)

Publication Number Publication Date
CN206064399U true CN206064399U (en) 2017-04-05

Family

ID=58430505

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201620901956.3U Expired - Fee Related CN206064399U (en) 2016-08-19 2016-08-19 Continuous nitrification automaton

Country Status (1)

Country Link
CN (1) CN206064399U (en)

Similar Documents

Publication Publication Date Title
CN107999011B (en) Methyl ethyl ketone peroxide production system and production technology
CN206064399U (en) Continuous nitrification automaton
CN113121356A (en) Automatic power continuous nitration method and device
CN101691663A (en) Method and device for on-line regeneration of sulfuric acid pickling waste liquid
CN102827008A (en) Method and device for producing phenylenediamine by taking water as solvent through liquid phase continuous hydrogenation method
CN104177243B (en) A kind of pipe type continuously prepares the method for 2-MNQ
CN103755520B (en) Method for producing substituted benzyl alcohol, substituted benzaldehyde and substituted benzyl acid through oxidizing substituted methylbenzene with air based on gas-liquid-solid heterogeneous reaction separation synchronization reactor
CN104844462A (en) Synthesis process of dimido dipheny compound
CN104447362B (en) Autoclave continuously hydrogen adding prepares the reaction system and method for para-aminophenol
CN206064398U (en) Eight room nitrators
CN106349086A (en) Method for preparing p-phenylenediamine rubber aging inhibitor
CN203018092U (en) Device for synthesising accelerant CBS via oxygen oxidation process
CN214892011U (en) Chlorination cauldron cooling device
CN101362699A (en) Method for synthesizing 2,4-dichloroaniline
CN110590527B (en) Process for continuously synthesizing anthraquinone by liquid phase method and synthesis system thereof
CN207951442U (en) A kind of mixing plant producing ferric trichloride
CN111018788A (en) Preparation method of 2-nitroimidazole
CN203155228U (en) Nitrating pot with automatic overflow function
CN217796139U (en) Nitration equipment for H acid solvent
CN219174345U (en) Wastewater degradation treatment device
CN106000267B (en) A kind of adipic acid synthesizer and its application method
CN214106932U (en) Nitro-benzoic acid production is with nitrifying cauldron
CN211514482U (en) Preparation facilities of fluid loss additive for drilling fluid
CN202099222U (en) Device used for synthesizing accelerator NS (N-tertiary Butyl-2-Benzothiazole Sulfenamide) by utilizing oxidation method
CN109317035A (en) Agitator tank in a kind of manganese slag disposal system

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170405

Termination date: 20170819