CN206058722U - A kind of improvement device of copperoxide reduction with carbon monoxide experiment - Google Patents

A kind of improvement device of copperoxide reduction with carbon monoxide experiment Download PDF

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Publication number
CN206058722U
CN206058722U CN201620673459.2U CN201620673459U CN206058722U CN 206058722 U CN206058722 U CN 206058722U CN 201620673459 U CN201620673459 U CN 201620673459U CN 206058722 U CN206058722 U CN 206058722U
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China
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flexible pipe
carbon monoxide
pipe
iii
bottleneck
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CN201620673459.2U
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Chinese (zh)
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高云腾
王明余
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Abstract

This utility model is related to the construction applications of accumulator, and in particular to a kind of improvement device of copperoxide reduction with carbon monoxide experiment.A kind of improvement device of copperoxide reduction with carbon monoxide experiment, including the caisson, reaction unit, exhaust gas processing device that are sequentially connected, described caisson is connected with reaction unit right angle hollow pipe, described reaction unit is connected with glass tubing with exhaust gas processing device, and described caisson and exhaust gas processing device are fixed with iron stand.The beneficial effects of the utility model are:Substantially, effect is preferable for phenomenon;Whole experiment is carried out in the system of a closing, does not have the excessive theory for having fully demonstrated environmental protection of poison CO (carbon monoxide converter) gas;Experiment miniaturization, while economizing in raw materials, can with a description of test elemental copper by the dioxygen oxidation in air into copper oxide, the copper oxide for just having generated is then elemental copper two chemical principles by Carbon monoxide reduction, experiment is continuous, and preferable teaching efficiency has been reached in field research.

Description

A kind of improvement device of copperoxide reduction with carbon monoxide experiment
Technical field
This utility model is related to the construction applications of accumulator, is specifically related to a kind of copperoxide reduction with carbon monoxide experiment Improve device.
Background technology
The experiment of copperoxide reduction with carbon monoxide in junior middle school chemistry teaching material, in the teaching material before people teaches 2012 editions, also Lecture experiment legend, present teaching material directly legend also without, analyze reason, be the lecture experiment in field research, One is loaded down with trivial details;Two are because that CO (carbon monoxide converter) gas are poisonous;Three is dangerous(CO (carbon monoxide converter) gas and air or oxygen mixing, reach To certain content, light and blast can occur);During four are former teaching material legend, CO (carbon monoxide converter) gas only one of which arrow is indicated, allows people Seen, be existing system or it is early in advance make it is standby.
If if producing with hall, there is trouble, danger, poisonous, more allow teacher cannot control be exactly on It is not enough between class hour, it is impossible to the teaching task of the class is completed within the class period of regulation.If it is in advance early make it is standby, Generally it is necessary to use gas storage device, ready-made gas storage device is heavy, and complex operation is unfavorable for that teacher is imparted knowledge to students, causes Make many teachers experiment be instead of with explanation or video display in field research, but chemistry is a section based on experiment Learn, if do not test supported, the interest of student substantially will be reduced, the teaching efficiency of subject will also decline, therefore, an oxygen The experiment for changing Reduction of cupric oxide by carbon needs to be improved in field research.
Utility model content
The purpose of this utility model be for above-mentioned defect and to provide a kind of raw material simple and easy to get, operation is held Easily, test continuously, phenomenon is obvious, low cost, the improvement device of the copperoxide reduction with carbon monoxide experiment of asepsis environment-protecting, this practicality New concrete scheme is as follows:
A kind of improvement device of copperoxide reduction with carbon monoxide experiment, including the caisson, reaction unit being sequentially connected, Exhaust gas processing device, described caisson, reaction unit and exhaust gas processing device are fixed with iron stand, are connected between each device It is simple and convenient, processing ease.
Described caisson includes syringe, and the syringe needle on described syringe is connected with flexible pipe I, and described is soft There is the inverted bottle I with bottleneck I below pipe I, described bottleneck I nearby has hole I, and described flexible pipe I is by near bottleneck I Hole I is flexibly connected with bottle I, and described flexible pipe I nearby has clip I near bottleneck I, and described bottleneck I has the single hole with consent I Piston, has the bottle II with bottleneck II below described bottle I, described bottleneck II has the diplopore with consent II and consent III to live Plug, between described bottleneck I and bottleneck II, the consent II of the consent I and diplopore piston of a piece insertion single hole piston of insertion is hollow Pipe, described hollow pipe two ends are inserted at bottom of bottle 1-3cm of bottle I and bottle II respectively;Described consent III inserts one directly Angle hollow pipe, described bottleneck II nearby have hole II, and described hole II is connected with flexible pipe II, and described flexible pipe II is attached near hole II Closely there is clip II.
Described reaction unit includes the flexible pipe III being connected with right angle hollow pipe, has clip III, institute on described flexible pipe III A " u "-shaped pipe is connected with the left of the flexible pipe III stated, described " u "-shaped pipe curves flat with horizontal plane near one end of flexible pipe III OK, one end and the horizontal plane away from flexible pipe III of described " u "-shaped pipe.
Described exhaust gas processing device includes air bag, and described air bag uses thin with one end of horizontal plane with " u "-shaped pipe Line binding connection.
The connected mode of syringe needle and flexible pipe I on described syringe is grafting, activity between described flexible pipe I and hole I Connected mode is also grafting, and this connected mode is simple and convenient, easily operates, is tested beneficial to teacher student.
Described flexible pipe I, flexible pipe II and flexible pipe III are all rubber tube or latex tubing, and pliability is good, easy to operate, is entirely filling Flexibly can change in putting.
Described hollow pipe, " u "-shaped pipe and right angle hollow pipe are all glass tubing, and corrosion-resistant, hardness is good, and raw material is simply easy Obtain, " u "-shaped pipe therein and right angle hollow pipe all can use straight hollow glass tube heating bending to obtain.
There is graduation mark on described bottle II, beneficial to the grasp and control of the consumption of carbon monoxide.
Described clip I, clip II and clip III are all alligator clamp or torsion folder.
The beneficial effects of the utility model are:(1)The use of syringe is beneficial to the control of carbon monoxide flow and consumption, effect Fruit is preferably;(2)Whole experiment is carried out in the system of a closing, and no poison CO (carbon monoxide converter) gas are excessive, fully demonstrate The theory of environmental protection;(3)The design raw material such as experiment miniaturization, syringe, flexible pipe, hollow pipe is simple and easy to get, easy to operate, section About cost;(4)Originally the lecture experiment on textbook can only represent copper oxide by Carbon monoxide reduction into elemental copper, after improvement, both Can reflect elemental copper by the dioxygen oxidation in air into copper oxide, can also represent the copper oxide of firm generation then by carbon monoxide also Originally it was elemental copper, two chemical principles of a description of test, experiment are continuous, and phenomenon substantially, reached in field research Preferable teaching efficiency.
Description of the drawings
Fig. 1 is 1 Experimental equipment of embodiment;
Wherein, 1- syringes, 101- syringe needles, 102- syringe glands, 2- flexible pipes I, 201- clips I, 3- bottles I, 301- bottles I, 302- of mouth holes I, 4- single hole pistons, 401- consents I, 5- bottles II, 501- bottlenecks II, 502- graduation marks, 503- holes II, 6- diplopores Piston, 601- consents II, 602- consents III, 7- hollow pipes, 8- flexible pipes II, 801- clips II, 9- right angles hollow pipe, 10- flexible pipes III, 1001- clip III, 11- " u "-shaped pipes, 12- clarification lime water, 13- copper wires, 14- balloons, 15- alcohol burners, 1501- alcohol burners Platform, 16- iron stands.
Specific embodiment
Embodiment 1
1 pair of the technical solution of the utility model is described in detail below in conjunction with the accompanying drawings.
This embodiment scheme is as follows:A kind of improvement device of copperoxide reduction with carbon monoxide experiment, including what is be sequentially connected Caisson, reaction unit, exhaust gas processing device, described caisson, reaction unit and exhaust gas processing device iron stand 16 fix.
Described caisson includes syringe 1, and the syringe needle 101 on described syringe 1 is connected with flexible pipe I 2, institute There is the inverted bottle I 3 with bottleneck I 301 below the flexible pipe I 2 stated, described bottleneck I 301 nearby has hole I 302, and described is soft Pipe I 2 is flexibly connected with bottle I 3 by the hole I 302 near bottleneck I 301, and described flexible pipe I 2 nearby has clip near bottleneck I 301 I 201, described bottleneck I 301 has the single hole piston 4 with consent I 401, has with bottleneck II 501 below described bottle I 3 Bottle II 5, described bottleneck II 501 has the diplopore piston 6 with consent II 601 and consent III 602, described bottleneck I 301 and bottle The hollow pipe 7 of the consent II 601 of the consent I 401 and diplopore piston 6 of an insertion single hole piston 4, institute are inserted between mouth II 501 7 two ends of hollow pipe stated are inserted at bottom of bottle 1cm of bottle I 3 and bottle II 5 respectively;Described consent III 602 inserts a right angle Hollow pipe 9, described bottleneck II 501 nearby have hole II 503, and described hole II 503 is connected with flexible pipe II 8, described flexible pipe II 8 Nearby there is clip II 801 near hole II 503.
Described reaction unit includes the flexible pipe III 10 being connected with right angle hollow pipe 9, has clip on described flexible pipe III 10 III 1001, it is connected with a " u "-shaped pipe 11 on the left of described flexible pipe III 10, described " u "-shaped pipe 11 is near the one of flexible pipe III 10 End curves and plane-parallel, one end and the horizontal plane away from flexible pipe III 10 of described " u "-shaped pipe 11.
Described exhaust gas processing device includes air bag 14, described air bag 14 and " u "-shaped pipe 11 and the one of horizontal plane End is connected with fine rule binding.
The connected mode of syringe needle 101 and flexible pipe I 2 on described syringe is grafting, described flexible pipe I 2 and bottle I 3 it Between movable connection method also be grafting.
Described flexible pipe I 2, flexible pipe II 8 and flexible pipe III 10 are all latex tubing.
Described hollow pipe 7, " u "-shaped pipe 11 and right angle hollow pipe 9 are all glass tubing.
There is graduation mark 502 on described bottle II 5.
Described clip I 201, clip II 801 and clip III 1001 are all torsion folder.
The specific implementation step of the present embodiment is as follows:
1st, equipment is got out, the copper wire 13 of one section of 15 centimeter length is fallen into the oxide on surface with sand papering then, wound Curl, and 11 horizontal segment middle of " u "-shaped pipe is put into, the stone of ten drop left and right clarifications is instilled in " u "-shaped pipe 11 with dropper Buck is to vertical port, and tightly wraps an air bag 14 in the mouth of pipe fine rule with horizontal plane one end, and the effect of air bag 14 is Responseless carbon monoxide is absorbed, prevents toxic gas to be emitted in air, to environment, then with one section 4-5 li The long flexible pipe III 10 of rice is enclosed within the horizontal pipe port of " u "-shaped pipe 11, and the latex mouth of pipe is stoppered with a stopper, is allowed to air tight, according to Equipment is connected shown in Fig. 1.
When the 2nd, using, the syringe thromboembolism 102 of syringe 1 is first pulled out, flexible pipe III 10 is clamped with clip III 1001, open folder Son II 801, water are entered by flexible pipe II 8, and bottle II 5 is filled.During air storage, gas enters following bottle II 5, bottle II 5 by flexible pipe II 8 In water be pressed into bottle I 3 above, when the water almost all in following bottle II 5 is pressed into bottle I 3 above, illustrate bottle II Gas is filled with 5, has been stopped ventilation, flexible pipe II 8 is clamped with clip II 801, be allowed to air tight, put the stand-by device well light Flexibly, get up very convenient used in field research, as long as gas that is water insoluble or not reacting with water can all be used and is somebody's turn to do Caisson is stored.
3rd, clip I 201, clip II 801, clip III 1001 are begun to shut off, alcohol burner 15 are placed on ethanol lamp-stand 1501, Alcohol burner 15 is lighted, is first preheated to the horizontal segment of " u "-shaped pipe 11, then placing concentration heating at helical form thin copper wire, for a moment Just see that the thin copper wire of redness becomes black, this is because the oxygen and copper wire in the air in " u "-shaped pipe 11 is in the bar being heated Part issues raw combination reaction, generates the metal oxide copper of black.
4th, syringe thromboembolism 102 is inserted into 1 syringe of syringe, it is noted that in the syringe space reserved by certain capacity, is opened Clip III 1001 and clip I 201, slow pushing syringe 1, while constantly mobile alcohol burner 15, so prevents alcohol burner 15 solid It is scheduled at one and heats, the horizontal segment of " u "-shaped pipe 11 is burnt curved easily;With being slowly passed through for carbon monoxide, in " u "-shaped pipe 11 The lime water 12 of clarification is pressed to the vertical end of " u "-shaped pipe 11 by CO (carbon monoxide converter) gas, at this moment controls one by syringe thromboembolism 102 Carbonoxide is passed through speed, can be appreciated that the lime water of clarification gradually becomes muddy, and the copper wire of black gradually becomes redness, and effect is very bright It is aobvious.

Claims (6)

1. the improvement device that a kind of copperoxide reduction with carbon monoxide is tested, including the caisson, reaction unit, tail that are sequentially connected Flash Gas Compression Skid System, it is characterised in that described caisson, reaction unit and exhaust gas processing device are fixed with iron stand;
Described caisson includes syringe, and the syringe needle on described syringe is connected with flexible pipe I, described flexible pipe I There is the inverted bottle I with bottleneck I lower section, and described bottleneck I nearby has hole I, and described flexible pipe I is by the hole I near bottleneck I It is flexibly connected with bottle I, described flexible pipe I nearby has clip I near bottleneck I, and described bottleneck I has the single hole with consent I to live Plug, has the bottle II with bottleneck II below described bottle I, described bottleneck II has the diplopore with consent II and consent III to live Plug, between described bottleneck I and bottleneck II, the consent II of the consent I and diplopore piston of a piece insertion single hole piston of insertion is hollow Pipe, described hollow pipe two ends are inserted at bottom of bottle 1-3cm of bottle I and bottle II respectively;Described consent III inserts one directly Angle hollow pipe, described bottleneck II nearby have hole II, and described hole II is connected with flexible pipe II, and described flexible pipe II is attached near hole II Closely there is clip II;
Described reaction unit includes the flexible pipe III being connected with right angle hollow pipe, has clip III on described flexible pipe III, described A " u "-shaped pipe is connected with the left of flexible pipe III, described " u "-shaped pipe is curved near one end of flexible pipe III and plane-parallel, institute One end and the horizontal plane away from flexible pipe III of the " u "-shaped pipe stated;
Described exhaust gas processing device includes air bag, and the one end of described air bag with " u "-shaped pipe with horizontal plane is tied with fine rule Tie up connection.
2. the improvement device that a kind of copperoxide reduction with carbon monoxide as claimed in claim 1 is tested, it is characterised in that described Syringe on syringe needle and flexible pipe I connected mode be grafting, between described flexible pipe I and hole I, movable connection method is also Grafting.
3. the improvement device that a kind of copperoxide reduction with carbon monoxide as claimed in claim 1 is tested, it is characterised in that described Flexible pipe I, flexible pipe II and flexible pipe III be all rubber tube or latex tubing.
4. the improvement device that a kind of copperoxide reduction with carbon monoxide as claimed in claim 1 is tested, it is characterised in that described Hollow pipe, " u "-shaped pipe and right angle hollow pipe be all glass tubing.
5. the improvement device that a kind of copperoxide reduction with carbon monoxide as claimed in claim 1 is tested, it is characterised in that described There is graduation mark on bottle II.
6. the improvement device that a kind of copperoxide reduction with carbon monoxide as claimed in claim 1 is tested, it is characterised in that described Clip I, clip II and clip III are all alligator clamp or torsion folder.
CN201620673459.2U 2016-06-30 2016-06-30 A kind of improvement device of copperoxide reduction with carbon monoxide experiment Expired - Fee Related CN206058722U (en)

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CN201620673459.2U CN206058722U (en) 2016-06-30 2016-06-30 A kind of improvement device of copperoxide reduction with carbon monoxide experiment

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Application Number Priority Date Filing Date Title
CN201620673459.2U CN206058722U (en) 2016-06-30 2016-06-30 A kind of improvement device of copperoxide reduction with carbon monoxide experiment

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108922354A (en) * 2018-07-05 2018-11-30 商洛学院 A kind of experimental method of graphene reductive copper oxide

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108922354A (en) * 2018-07-05 2018-11-30 商洛学院 A kind of experimental method of graphene reductive copper oxide

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Granted publication date: 20170329

Termination date: 20180630