CN206045455U - A kind of magnetic distillation system - Google Patents

A kind of magnetic distillation system Download PDF

Info

Publication number
CN206045455U
CN206045455U CN201621083923.9U CN201621083923U CN206045455U CN 206045455 U CN206045455 U CN 206045455U CN 201621083923 U CN201621083923 U CN 201621083923U CN 206045455 U CN206045455 U CN 206045455U
Authority
CN
China
Prior art keywords
rectifying column
magnetic
distillation system
reboiler
outlet
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201621083923.9U
Other languages
Chinese (zh)
Inventor
段秀丽
李世泰
程金云
肖阳
付冠亚
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tianjin University of Technology
Original Assignee
Tianjin University of Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tianjin University of Technology filed Critical Tianjin University of Technology
Priority to CN201621083923.9U priority Critical patent/CN206045455U/en
Application granted granted Critical
Publication of CN206045455U publication Critical patent/CN206045455U/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

This utility model provides a kind of magnetic distillation system, including rectifying column, cooler and reboiler, wherein, the top export of the rectifying column is connected with the steam inlet of the cooler, and the liquid outlet of the cooler is connected with the reflux inlet of the rectifying column;The steam inlet of the rectifying column is connected with the steam (vapor) outlet of the reboiler, and the bottom end outlet of the rectifying column is connected with the top entry of the reboiler;And the outside of the reboiler is provided with magnetic material layer.The magnetic distillation system changes physical property and the liquid vapor equilibrium conditions such as the viscosity of material, surface tension, saturated vapor, so as to forced fluid vapour separation process, improves separation efficiency by arranging externally-applied magnetic field in the outside of reboiler.The system adopts externally-applied magnetic field, has the advantages that advanced, environmentally friendly, energy-conservation and resource utilization are high, without the need for increasing artificial operation, and does not increase labor intensity;Its equipment requires that without particular design technology is simple, it is short to invest the low, construction period.

Description

A kind of magnetic distillation system
Technical field
This utility model is related to chemical industry rectifying device technical field, more particularly to a kind of magnetic distillation system.
Background technology
Rectification is that the difference of each component volatile performance using mixture carries out detached operational approach, is widely used in In commercial production, and occupy leading position in all of separation method for a long time.Traditional rectification isolation technics energy consumption is big, and And solvent used has larger toxicity or corrosivity, for improve production efficiency, reduce environmental pollution, reduce producing into Sheet and energy consumption, what is currently used are all the rectificating methods after improving.
Reinforcing rectificating method under prior art is roughly divided into two classes:One kind is to add separating medium, such as catalyst, absorption Agent, organic active component, inorganic electrolyte etc. carry out coupling rectification;Another kind is to improve device structure, for example, improve two phase flow The new packing and spray that dynamic and contact is developed arranges Cocurrent packed Columns plate.But the method for adding separating medium, its catalyst, suction Attached dose, organic active component, contain heavy metal in inorganic electrolyte, original thing system can be polluted, and be recycled tired Difficulty, another aspect heavy metal it is expensive, can cause the waste of resource after discharge, improve production cost.
And the method for improving device structure, which is invested and energy consumption is relatively large, and packed tower requires strict, behaviour to filler material Make also more complicated, construction cost is higher, while the distributor anti-blockage capability and operating flexibility in rectifying column requires also higher, tower Interior mist entrainment problem is difficult to solve.Packed tower also there is a problem of following to be studied and solve at present:Filler is in normal pressure and adds Research etc. that what the unstable properties analysis of causes of application, pressurized systems in laminate system, packed tower designed a model theorize.
Utility model content
For the problems referred to above, this utility model aims to solve the problem that problem as described above.A purpose of the present utility model is A kind of any one magnetic distillation system solved in problem above is provided.Specifically, this utility model provide can energy-conservation subtract Consumption, avoid polluting, and the high magnetic distillation system of separation efficiency.
To solve above-mentioned technical problem, this utility model provides a kind of magnetic distillation system, and the magnetic distillation system includes Rectifying column, cooler and reboiler, wherein, the top export of the rectifying column is connected with the steam inlet of the cooler, The liquid outlet of the cooler is connected with the reflux inlet of the rectifying column;The steam inlet of the rectifying column with it is described again The steam (vapor) outlet of boiling device is connected, and the bottom end outlet of the rectifying column is connected with the top entry of the reboiler;And it is described The outside of reboiler is provided with magnetic material layer.
Wherein, the magnetic distillation system also includes storage device and supply pump, the outlet of the storage device and the confession It is connected to the entrance of pump, the outlet of the supply pump is connected with the feed(raw material)inlet of the rectifying column.
Wherein, the magnetic distillation system also includes positive displacement pump, the bottom end outlet of the rectifying column by the positive displacement pump with The top entry of the reboiler is connected.
Wherein, the magnetic distillation system also includes fluid reservoir, and the fluid reservoir is connected with the liquid outlet of the cooler It is logical.
Wherein, the magnetic distillation system also includes waste liquid tank, and the waste liquid outlet of the reboiler is connected with the waste liquid tank It is logical.
Wherein, the reflux inlet is located in the top sidewall of the rectifying column.
Wherein, the steam inlet is located in the bottom sidewall of the rectifying column.
Wherein, the feed(raw material)inlet is located in the middle part of sliding channel of the rectifying column.
Wherein, the rectifying column is plate distillation column or material filling type rectifying column.
The magnetic distillation system that this utility model is provided changes the viscous of material by arranging externally-applied magnetic field in the outside of reboiler The physical propertys such as degree, surface tension, saturated vapor and liquid vapor equilibrium condition, so as to forced fluid vapour separation process, improve and separate effect Rate.The system adopts externally-applied magnetic field, has the advantages that advanced, environmentally friendly, energy-conservation and resource utilization are high, without the need for increasing artificial behaviour Make, and do not increase labor intensity;Its equipment requires that without particular design technology is simple, it is short to invest the low, construction period.
It is read with reference to the drawings the following description for exemplary embodiment, other property features of the present utility model and excellent Point will become apparent from.
Description of the drawings
In being incorporated into description and the accompanying drawing of the part that constitutes description shows embodiment of the present utility model, and And be used to explain principle of the present utility model together with the description.In the drawings, similar reference is used to represent similar Key element.Drawings in the following description are some embodiments of the present utility model, rather than whole embodiments.It is general for this area For logical technical staff, on the premise of not paying creative work, other accompanying drawings can be obtained according to these accompanying drawings.
Fig. 1 schematically illustrates the structural representation of magnetic distillation system of the present utility model.
Specific embodiment
It is to make purpose, technical scheme and the advantage of this utility model embodiment clearer, new below in conjunction with this practicality Accompanying drawing in type embodiment, is clearly and completely described to the technical scheme in this utility model embodiment, it is clear that retouched The embodiment stated is a part of embodiment of this utility model, rather than the embodiment of whole.Based on the enforcement in this utility model Example, the every other embodiment obtained under the premise of creative work is not made by those of ordinary skill in the art are belonged to The scope of this utility model protection.It should be noted that in the case where not conflicting, in the embodiment and embodiment in the application Feature can mutual combination in any.
Basic thought of the present utility model is to arrange permanent magnetic field by the periphery in reboiler, improve solution interior molecules Stressing conditions, the surface tension and viscosity that reduce the latent heat of vaporization, reduce solution, improve the mobility of solution, improve and separate effect Rate.This setup not only reduces the change to original distillation system, and operates without the need for special messenger, saves labour force;Meanwhile, Additive is not introduced in original thing system, energy consumption is substantially reduced.
Below in conjunction with the accompanying drawings, to being described in detail according to magnetic distillation system provided by the utility model.
Fig. 1 shows a kind of structural representation of the embodiment according to magnetic distillation system of the present utility model, with reference to Fig. 1 institutes Show, the magnetic distillation system includes rectifying column 1, cooler 2 and reboiler 3.Wherein, the top export 11 and cooler 2 of rectifying column 1 Steam inlet 21 be connected, the gaseous material that rectifying column 1 is isolated is cooled down in being directly entered cooler 2;Cooler 2 Liquid outlet 22 is connected with the reflux inlet 12 of rectifying column 1, cooler 2 cooling condense partial condensation liquid as backflow from Reflux inlet 12 is returned in rectifying column 1, carries out heat exchange, to improve rectification precision.The steam inlet 13 of rectifying column 1 and reboiler 3 steam (vapor) outlet 31 is connected, and the bottom end outlet 14 of rectifying column 1 is connected with the top entry 32 of reboiler 3;Flow into rectifying column The liquid of 1 bottom of towe is transported to after carrying out liquid vapour conversion in reboiler 3, and the steam of generation is carried out in returning again to rectifying column 1 point From.Further, the outside of reboiler 3 is provided with magnetic material layer 4, forms permanent magnetic field, to improve the vapour-liquid in reboiler 3 point From the steam that efficiency, preliminary purification are entered in rectifying column 1.
Wherein, magnetic material layer 4 can both be ferrum rubidium boron based material, Al-Ni-Co series material, ferrite, siderochrome cobalt system material Material, can also be that the magnetic materials such as rare earth material are constituted.
Specifically, the magnetic distillation system also includes storage device 5 and supply pump 6, outlet and the supply pump 6 of storage device 5 Entrance be connected, the outlet of supply pump 6 is connected with the feed(raw material)inlet 15 of rectifying column 1.It is stored in treating point in storage device 5 From raw material, feed(raw material)inlet 15 is transported to by supply pump 6, to be separated in rectifying column 1.
Specifically, the magnetic distillation system also includes positive displacement pump 7, and the bottom end outlet 14 of rectifying column 1 passes through positive displacement pump 7 and boils again The top entry 32 of device 3 is connected.The liquid in 1 bottom of rectifying column is accumulated in the presence of positive displacement pump 7, smoothly into reboiler After being vaporized in 3 again, enter back into via the steam (vapor) outlet 31 of reboiler 3 and separated in rectifying column 1.
Specifically, the magnetic distillation system also includes fluid reservoir 8, and fluid reservoir 8 is connected with the liquid outlet 22 of cooler 2. Through gaseous material that rectifying column 1 is isolated under the cooling effect of cooler 2, liquid is condensed into, part is returned in rectifying column 1 Heat exchange is carried out with steam, to purify steam, another part is high purity product, then entered in fluid reservoir 8 through liquid outlet 22 Stored.
In addition, also include waste liquid tank 9 according to magnetic distillation system of the present utility model, the waste liquid outlet 33 of reboiler 3 with it is useless Flow container 9 is connected.The bottom hydrops of rectifying column 1 carries out boiling vaporization into reboiler 3, and the liquid that cannot wherein vaporize then Jing Carried out by waste liquid outlet 33 pending in waste liquid tank 9.
When being separated using magnetic distillation system of the present utility model, raw material to be separated is from storage device 5 via confession Send in rectifying column 1 to pump 6, the liquid in raw material is with the liquid flowed down from the top of rectifying column 1 while flowing to tower along rectifying column 1 Bottom;Gas in raw material is then risen to tower top along rectifying column 1 together with the steam entered from 1 bottom of rectifying column.Rise in gas During declining with liquid, gas carries out heat exchange with liquid, and in gas, the component of difficult volatilization switchs to liquid, flows to bottom of towe; Volatile components in liquid are then converted into gaseous state, rise to tower top.Closer to tower top position, the volatile components concentration in steam Higher, closer to bottom of towe, its difficult volatile component is more enriched with, such that it is able to further improve separation accuracy.
Lower boiling steam is condensed into after liquid in cooler 2 via top export 11, or utilize, or storage;It is high The liquid of boiling point flows to bottom of towe, enters in reboiler 3 via bottom end outlet 14, carries out reheating, and in 4 shape of magnetic material layer Into permanent magnetic field in the presence of carry out liquid vapour separation, steam after boiling is separated in returning rectifying column 1 again, and liquid is then Carry out storing in flowing to waste liquid tank 9, it is pending.
Specifically, reboiler 3 is during heating vaporization is carried out, heated material from magnetic field energy absorption dropping The low latent heat of vaporization, the permanent magnetic field that additional magnetic material layer 4 is produced effectively affect the stressing conditions in thing system between solution molecule, reduce The latent heat of vaporization, it is energy-saving;Meanwhile, magnetic field can reduce the surface tension and viscosity of molecules in solution, so as to improve solution Mobility, improves separation efficiency.
Specifically, in order to effectively improve the heat exchanger effectiveness in vapour-liquid counter-current process, reflux inlet 12 is located at rectifying column 1 In top sidewall, steam inlet 13 is located in the bottom sidewall of rectifying column 1, and feed(raw material)inlet 15 is located at the medial side of rectifying column 1 On wall.
It is pointed out that in magnetic distillation system of the present utility model, rectifying column 1 can be plate distillation column or fill out Material formula rectifying column, its use range are extensive.
Magnetic distillation system of the present utility model due to adopting externally-applied magnetic field, therefore for the property of raw material to be separated is without special Require, the raw material of acid or oxidisability can carry out separating treatment.
Descriptions above can combine individually or in a variety of ways enforcement, and these variants all exist Within protection domain of the present utility model.
It should be noted that herein, such as first and second or the like relational terms are used merely to a reality Body or operation are made a distinction with another entity or operation, and are not necessarily required or implied these entities or deposit between operating In any this actual relation or order.And, term " including ", "comprising" or its any other variant are intended to Including for nonexcludability, so that not only including those key elements including the article or equipment of a series of key elements, but also wraps Other key elements being not expressly set out are included, or also includes the key element intrinsic for this article or equipment.Without more Limit in the case of, the key element limited by sentence " including ... ", it is not excluded that in the article including the key element or set Also there is other identical element in standby.
Above example only to illustrate the technical solution of the utility model and unrestricted, reference only to preferred embodiment pair This utility model has been described in detail.It will be understood by those within the art that, can be to technology of the present utility model Scheme is modified or equivalent, without deviating from the spirit and scope of technical solutions of the utility model, all should cover at this In the middle of the right of utility model.

Claims (9)

1. a kind of magnetic distillation system, it is characterised in that the magnetic distillation system includes rectifying column (1), cooler (2) and reboiler (3), wherein, the top export (11) of the rectifying column (1) is connected with the steam inlet (21) of the cooler (2), described The liquid outlet (22) of cooler (2) is connected with the reflux inlet (12) of the rectifying column (1);The steaming of the rectifying column (1) Vapour entrance (13) is connected with the steam (vapor) outlet (31) of the reboiler (3), the bottom end outlet (14) of the rectifying column (1) and institute The top entry (32) for stating reboiler (3) is connected;And the outside of the reboiler (3) is provided with magnetic material layer (4).
2. magnetic distillation system as claimed in claim 1, it is characterised in that the magnetic distillation system also includes storage device (5) With supply pump (6), the outlet of the storage device (5) is connected with the entrance of the supply pump (6), the supply pump (6) Outlet is connected with the feed(raw material)inlet (15) of the rectifying column (1).
3. magnetic distillation system as claimed in claim 1, it is characterised in that the magnetic distillation system also includes positive displacement pump (7), institute The bottom end outlet (14) for stating rectifying column (1) is connected with the top entry (32) of the reboiler (3) by the positive displacement pump (7) It is logical.
4. magnetic distillation system as claimed in claim 1, it is characterised in that the magnetic distillation system also includes fluid reservoir (8), institute State fluid reservoir (8) to be connected with the liquid outlet (22) of the cooler (2).
5. magnetic distillation system as claimed in claim 1, it is characterised in that the magnetic distillation system also includes waste liquid tank (9), institute The waste liquid outlet (33) for stating reboiler (3) is connected with the waste liquid tank (9).
6. magnetic distillation system as claimed in claim 1, it is characterised in that the reflux inlet (12) is positioned at the rectifying column (1) in top sidewall.
7. magnetic distillation system as claimed in claim 1, it is characterised in that the steam inlet (13) is positioned at the rectifying column (1) in bottom sidewall.
8. magnetic distillation system as claimed in claim 2, it is characterised in that the feed(raw material)inlet (15) is positioned at the rectifying column (1) in middle part of sliding channel.
9. magnetic distillation system as claimed in claim 1, it is characterised in that the rectifying column (1) is for plate distillation column or fills out Material formula rectifying column.
CN201621083923.9U 2016-09-27 2016-09-27 A kind of magnetic distillation system Active CN206045455U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201621083923.9U CN206045455U (en) 2016-09-27 2016-09-27 A kind of magnetic distillation system

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201621083923.9U CN206045455U (en) 2016-09-27 2016-09-27 A kind of magnetic distillation system

Publications (1)

Publication Number Publication Date
CN206045455U true CN206045455U (en) 2017-03-29

Family

ID=58365909

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201621083923.9U Active CN206045455U (en) 2016-09-27 2016-09-27 A kind of magnetic distillation system

Country Status (1)

Country Link
CN (1) CN206045455U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108635897A (en) * 2018-04-13 2018-10-12 浙江工业大学 A kind of deflection type overgravity rotary bed magnetic field-intensification rectifying device

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108635897A (en) * 2018-04-13 2018-10-12 浙江工业大学 A kind of deflection type overgravity rotary bed magnetic field-intensification rectifying device
CN108635897B (en) * 2018-04-13 2024-01-12 浙江工业大学 Baffling type supergravity rotating bed magnetic field intensified rectification equipment

Similar Documents

Publication Publication Date Title
CN205925048U (en) Retrieve batch distillation device of ethanol in china cypress paper production process
CN101549929B (en) Method for distilling absorption type negative-pressure thermal cycle coking wastewater
CN107812393A (en) A kind of methanol three-effect rectification system and technique
CN206045455U (en) A kind of magnetic distillation system
CN104667554B (en) A kind of multifunctional efficient rectifying column
CN206089506U (en) Retrieve continuous rectification device of ethanol in china cypress paper production process
CN106730968A (en) A kind of integrated air rectification and purification device
CN107551586A (en) A kind of device using next door tower combination multi-effect distillation production methanol
CN203890081U (en) Environment-friendly energy-saving device for producing concentrated ammonia water
CN207596482U (en) A kind of rectifying device for purifying trichlorosilane
CN205759788U (en) Energy-saving single-action concentrates rectifier unit
CN203794660U (en) Negative-pressure ammonia evaporating device for coking remaining ammonia water
CN203065154U (en) Device for extracting concentrated hydrochloric acid by means of reaction distillation
CN205709899U (en) A kind of ammonia gas purification device
CN107501126B (en) The method and system of high efficiente callback acrylonitrile in a kind of production of high-performance carbon fibre
CN208694635U (en) A kind of purification-recovery system of methylene chloride exhaust gas
CN204490830U (en) Utilize the system of raw gas waste heat recovery coal oven dithio-gas benzene class material
CN203989925U (en) A kind of heat pump distillation energy saver
CN203648111U (en) Waste alcohol recovery device
CN207822550U (en) A kind of solvent recovery continuous rectification apparatus
CN207429733U (en) A kind of rectifying device for being used to prepare watermelon ketone
CN207532818U (en) A kind of methanol three-effect rectification system
CN206269615U (en) A kind of spraying condenser
CN201962221U (en) Improved alcohol recovering device
CN206793073U (en) A kind of medicine intermediate distillation system

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant