CN206027671U - Heating and thermal cycling device in softener production process - Google Patents

Heating and thermal cycling device in softener production process Download PDF

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Publication number
CN206027671U
CN206027671U CN201621056727.2U CN201621056727U CN206027671U CN 206027671 U CN206027671 U CN 206027671U CN 201621056727 U CN201621056727 U CN 201621056727U CN 206027671 U CN206027671 U CN 206027671U
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China
Prior art keywords
heat
heating
exchanger tube
heat exchanger
softener
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CN201621056727.2U
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Chinese (zh)
Inventor
麦国耀
周巧燕
麦信恒
麦理恒
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Guangzhou xieyanlai Industrial Co., Ltd
Original Assignee
GUANGZHOU PANYU XIE YUN LAI CHEMICAL NECESSITIES FACTORY
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Priority to CN201621056727.2U priority Critical patent/CN206027671U/en
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Abstract

The utility model provides a heating and thermal cycling device in softener production process, including pyroreaction cauldron and low temperature reation kettle, the pyroreaction cauldron is equipped with first feed inlet and first discharge gate, the softener material is got into in the pyroreaction cauldron by first feed inlet, low temperature reation kettle is equipped with second feed inlet and second discharge gate, be equipped with material pumping pump between second feed inlet and the first discharge gate, be equipped with first heat exchange tube in the pyroreaction cauldron, be equipped with the second heat exchange tube in the low temperature reation kettle, the import of first heat exchange tube is connected in heating system through a heat conductive oil pipe, the export of first heat exchange tube is connected in the import of second heat exchange tube through the 2nd heat conductive oil pipe, the export of second heat exchange tube is connected in heating system through the 3rd heat conductive oil pipe, be equipped with the high temperature conduction oil in the heat conductive oil pipe. The utility model discloses utilize after waste heat and the heat exchange of reaction back material the heat of conduction oil to heat heat preservation low temperature reation kettle, can the make full use of heat, the heat conduction oil circulation heat exchange realizes heating and heat retaining cycle control.

Description

Heating and heat insulation circulating device in a kind of softener production process
Technical field
This utility model is related to a kind of softener production equipment, the heating in more particularly to a kind of softener production process With heat insulation circulating device.
Background technology
Need temperature-gradient method to be incubated in softener production process, be that material is positioned over into different reactors in prior art In heated, heating-up temperature in different reactor is different, need to heat respectively, heats high energy consumption, and each reactor expends heat Amount is more, and the temperature of each reactor need to be controlled, it is difficult to which control or control structure are complicated, in order to heat many reactors Need to keep vacuum state, realize difficult.
Utility model content
For the problem that prior art is present, this utility model provides one kind and does not need vacuum condition, under low-temperature condition Total overall reaction just can be completed the short period, simpler, accurate, saving time, and the softener production process of energy-conservation is operated In heating and heat insulation circulating device.
To achieve these goals, this utility model is adopted the following technical scheme that:
Heating and heat insulation circulating device in a kind of softener production process, including pyroreaction kettle and low-temp reaction kettle, The pyroreaction kettle is provided with first charging aperture and the first discharging opening, and softener material enters the height by the first charging aperture In warm reactor, the low-temp reaction kettle is provided with second charging aperture and the second discharging opening, the second charging aperture and described first Mateiral pump is provided between discharging opening, is provided with the first heat exchanger tube, is provided with second in the low-temp reaction kettle in the pyroreaction kettle Heat exchanger tube, the import of first heat exchanger tube be connected to heating system by the first heat-conducting oil pipes, and first heat exchanger tube goes out Mouth is connected to the import of second heat exchanger tube by the second heat-conducting oil pipes, and the outlet of second heat exchanger tube passes through the 3rd heat conduction Oil pipe is connected to the heating system, is provided with high temperature heat conductive oil in first heat-conducting oil pipes.
Further, motor is additionally provided between first discharging opening and the second charging aperture, driven by the motor The mateiral pump, by low-temp reaction kettle described in the softener material suction in the pyroreaction kettle.
Further, first heat-conducting oil pipes are provided with valve, for control into the heat conduction in first heat exchanger tube The flow of oil.
Further, first heat exchanger tube or/and the second heat exchanger tube spiral be arranged at the pyroreaction kettle or/and In the low-temp reaction kettle.
Further, the softener is with stearic acid, polyamines, emulsifying agent, cross-linking agent as raw material, through amidation process, season Ammonium reaction and emulsion reaction are formed.
The beneficial effects of the utility model:
Softener material is incubated in being evacuated to low-temp reaction kettle after the completion of reacting in pyroreaction kettle by mateiral pump, meanwhile, Conduction oil after first heat exchange intraductal heat exchange is entered in the second heat exchanger tube, more than reacting rear material by the second heat-conducting oil pipes After heat and heat exchange, the heat of conduction oil carrys out heating and thermal insulation low-temp reaction kettle, can make full use of heat, and above-mentioned heating is not Vacuum condition is needed, total overall reaction just can be completed under normal conditions the short period, heat conduction is oil circulation after the completion of reaction carries out hot friendship Change, realize the loop control of heating and insulation, it is easy to control, it is simple to operate.
Description of the drawings
Fig. 1 is the heating in this utility model softener production process and the structural representation of heat insulation circulating device;
In figure, 1 pyroreaction kettle, 2 first charging apertures, 3 first discharging openings, 4 first heat exchanger tubes, 5 low temperature Reactor, 6 second charging apertures, 7 second discharging openings, 8 second heat exchanger tubes, 9 mateiral pumps, 10 motors, 11 first Heat-conducting oil pipes, 12 valves, 13 second heat-conducting oil pipes, 14 the 3rd heat-conducting oil pipes, 15 heating systems.
Specific embodiment
Below in conjunction with the accompanying drawing in this utility model embodiment, the technical scheme in this utility model embodiment is carried out Clearly and completely describe, it is clear that described embodiment is only a part of embodiment of the present utility model, rather than all Embodiment.Based on the embodiment in this utility model, those of ordinary skill in the art are not making creative work premise Lower obtained every other embodiment, belongs to the scope of this utility model protection.
Such as Fig. 1, this utility model provides the heating in a kind of softener production process and heat insulation circulating device, including high temperature Reactor 1 and low-temp reaction kettle 5.The top of pyroreaction kettle 1 is provided with first charging aperture 2 and the first discharging opening 3, softener material Entered in pyroreaction kettle 1 by first charging aperture 2, in pyroreaction kettle 1, be provided with the first heat exchanger tube 4,4 spiral of the first heat exchanger tube It is arranged in pyroreaction kettle 1, the first heat exchanger tube 4 that spiral is arranged can increase heat exchange area.The entrance point of the first heat exchanger tube 4 The first heat-conducting oil pipes 11 are connected with, the first heat-conducting oil pipes 11 connect built with high temperature heat conductive oil, the other end of the first heat-conducting oil pipes 11 Heating system 15 is connected to, and by heating system 15 by heat-conducting oil heating, then first is flowed into through the first heat-conducting oil pipes 11 and is exchanged heat In pipe 4, heat exchange is carried out with the softener material in pyroreaction kettle 1, so as to provide high temperature ring for the reaction of softener material Border.Preferably, the first heat-conducting oil pipes 11 are provided with valve 12, the flow of the conduction oil entered in the first heat exchanger tube 4 for control, So as to control the temperature in pyroreaction kettle 1.In the present embodiment, the temperature control of pyroreaction kettle 1 is at 180 DEG C or so.
The top of low-temp reaction kettle 5 is provided with second charging aperture 6 and the second discharging opening 7, second charging aperture 6 and the first discharging opening Mateiral pump 9 and motor 10 is provided between 3, drives mateiral pump 9 to be evacuated to softener material by pyroreaction kettle 1 by motor 10 low In warm reactor 5.Above-mentioned valve, mateiral pump and motor are all connected to electric-control system, automatically control conduction oil by electric-control system Flow and mateiral pump and motor switch.It is provided with the second heat exchanger tube 8 in low-temp reaction kettle 5,8 spiral of the second heat exchanger tube sets It is placed in pyroreaction kettle 5, the second heat exchanger tube 8 that spiral is arranged can increase heat exchange area.The import of the second heat exchanger tube 8 passes through Second heat-conducting oil pipes 13 are connected to the outlet of the first heat exchanger tube 4, and the outlet of the second heat exchanger tube 8 is connected by the 3rd heat-conducting oil pipes 14 In heating system 15.The conduction oil in First Heat Exchanger 4 is introduced in the second heat exchanger tube 8 by the second heat-conducting oil pipes 13, utilized After the waste heat of reacting rear material and heat exchange, the heat of conduction oil carrys out heating and thermal insulation low-temp reaction kettle 5, can make full use of heat Amount.Temperature stabilization of the softener material in low-temp reaction kettle 5 now adds in low-temp reaction kettle 5 at 100 DEG C -110 DEG C or so Enter cross-linking agent, temperature has a small amount of intensification, temperature control made at 110 DEG C -115 DEG C, until reaction terminates.Reaction is submissive after terminating Agent material is discharged by the second discharging opening 7.After the completion of reaction, conduction oil is flow back into by the 3rd heat-conducting oil pipes 14 of 8 Jing of the second heat exchanger tube Reheat in heating system 15, realize the loop control of heating and insulation, heat utilization ratio is high.
Softener of the present utility model with stearic acid, polyamines, emulsifying agent, cross-linking agent as raw material, through amidation process, season Ammonium reaction and emulsion reaction are formed, it is not necessary to vacuum condition, under the heating of above-mentioned circulating device just can the short period it is complete Into total overall reaction, operation is simpler, accurate, saves the time, so as to improve work efficiency, it is ensured that product quality.
Above example is only unrestricted to illustrate the technical solution of the utility model, although with reference to preferred embodiment pair This utility model has been described in detail, it will be appreciated by those skilled in the art that can enter to the technical solution of the utility model Row modification or equivalent, without deviating from the objective and scope of the technical program, which all should be covered in power of the present utility model In sharp claimed range.

Claims (5)

1. the heating in a kind of softener production process and heat insulation circulating device, it is characterised in that include:Pyroreaction kettle and low Warm reactor, the pyroreaction kettle are provided with first charging aperture and the first discharging opening, and softener material is by the first charging aperture Into in the pyroreaction kettle, the low-temp reaction kettle is provided with second charging aperture and the second discharging opening, the second charging aperture Mateiral pump is provided between first discharging opening, is provided with the first heat exchanger tube, the low-temp reaction kettle in the pyroreaction kettle Second heat exchanger tube is provided with inside, the import of first heat exchanger tube is connected to heating system by the first heat-conducting oil pipes, described first The outlet of heat exchanger tube is connected to the import of second heat exchanger tube by the second heat-conducting oil pipes, and the outlet of second heat exchanger tube is led to Cross the 3rd heat-conducting oil pipes and be connected to the heating system, in first heat-conducting oil pipes, be provided with high temperature heat conductive oil.
2. the heating in softener production process according to claim 1 and heat insulation circulating device, it is characterised in that:It is described Motor is additionally provided between first discharging opening and the second charging aperture, the mateiral pump is driven by the motor, will be described In low-temp reaction kettle described in softener material suction in pyroreaction kettle.
3. the heating in softener production process according to claim 1 and heat insulation circulating device, it is characterised in that:It is described First heat-conducting oil pipes are provided with valve, the flow of the conduction oil entered in first heat exchanger tube for control.
4. the heating in softener production process according to claim 1 and heat insulation circulating device, it is characterised in that:It is described First heat exchanger tube or/and the second heat exchanger tube spiral are arranged in the pyroreaction kettle or/and the low-temp reaction kettle.
5. the heating in softener production process according to claim 1 and heat insulation circulating device, it is characterised in that:It is described Softener with stearic acid, polyamines, emulsifying agent, cross-linking agent as raw material, through amidation process, quaterisation and emulsion reaction shape Into.
CN201621056727.2U 2016-09-14 2016-09-14 Heating and thermal cycling device in softener production process Active CN206027671U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201621056727.2U CN206027671U (en) 2016-09-14 2016-09-14 Heating and thermal cycling device in softener production process

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201621056727.2U CN206027671U (en) 2016-09-14 2016-09-14 Heating and thermal cycling device in softener production process

Publications (1)

Publication Number Publication Date
CN206027671U true CN206027671U (en) 2017-03-22

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CN201621056727.2U Active CN206027671U (en) 2016-09-14 2016-09-14 Heating and thermal cycling device in softener production process

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112047763A (en) * 2020-09-14 2020-12-08 河南理工大学 Device and process method for preparing fertilizer by utilizing kitchen waste
CN113521780A (en) * 2021-09-02 2021-10-22 东营益盛化工有限公司 Esterification tower for producing butyl acetate
CN114768574A (en) * 2022-05-06 2022-07-22 沈慧 System for producing cosmetic products

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112047763A (en) * 2020-09-14 2020-12-08 河南理工大学 Device and process method for preparing fertilizer by utilizing kitchen waste
CN113521780A (en) * 2021-09-02 2021-10-22 东营益盛化工有限公司 Esterification tower for producing butyl acetate
CN114768574A (en) * 2022-05-06 2022-07-22 沈慧 System for producing cosmetic products

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CP03 Change of name, title or address

Address after: 510000 Room 101, building 4, No. 23, sukeng street, Panyu District, Guangzhou City, Guangdong Province

Patentee after: Guangzhou xieyanlai Industrial Co., Ltd

Address before: Meishan village Panyu District Hualong Town Guangzhou Guangdong province 510000 City Gang of two face three four

Patentee before: Guangzhou Panyu Xie Yun Lai Chemical Necessities Factory