CN206014814U - A kind of waste lubricating oil comprehensive recycling device - Google Patents

A kind of waste lubricating oil comprehensive recycling device Download PDF

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Publication number
CN206014814U
CN206014814U CN201620883536.7U CN201620883536U CN206014814U CN 206014814 U CN206014814 U CN 206014814U CN 201620883536 U CN201620883536 U CN 201620883536U CN 206014814 U CN206014814 U CN 206014814U
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oil
breakdown
waste
lubricating oil
distillation column
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CN201620883536.7U
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庞流
郏彩霞
田锦文
张兆龙
张春志
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Huiyang Huizhou District Environmental Protection Co Ltd
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Huiyang Huizhou District Environmental Protection Co Ltd
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Abstract

The utility model discloses a kind of waste lubricating oil comprehensive recycling device, breakdown of emulsion Sedimentation tank that described device includes being sequentially connected, preheater, distillation column, condenser, light-weight fuel oil collection device and absorbent charcoal adsorber is connected to after the condenser, wherein, agitating device is provided with the breakdown of emulsion Sedimentation tank, waste oil is delivered to the preheater by pump by the breakdown of emulsion Sedimentation tank, waste oil is pumped in distillation column by feeding after preheater preheating, and the bottom of the distillation column is provided with residual oil outlet.Waste lubricating oil comprehensive recycling device process is simple of the present utility model, safe and reliable, small investment, device motility are strong.

Description

A kind of waste lubricating oil comprehensive recycling device
Technical field
This utility model is related to waste process field, more particularly to a kind of waste lubricating oil comprehensive recycling device.
Background technology
Lubricating oil is used in all kinds automobile, plant equipment reducing the liquid of friction, protection machinery and workpiece Or semisolid lubricants, act primarily as the effect such as lubrication, cooling, antirust, cleaning, sealing and buffering
Due to high temperature, air oxidation during use, gradually aged deterioration, along with mechanical part rubs sassafras lubricating oil The metal dust of generation, from the environment into moisture, impurity etc., cause the pollution such as mineral oil, oxidation, therefore, waste lubricating oil In in addition to C, H etc., can also contain a small amount of other elements, the element such as including Fe, Mg, Ca, Zn, Cu, Sn, Al and Ni.Wherein, Fe, Cu, Al and Ni belong to Wear metal;Si, B and Na can be summarized as pollution element, and such as Si is due to air filter The dust foul of imprecision suction comes from defoamer in oil, and B and Na is mixed into due to the leakage of engine-cooling system Antifreezing agent, and Mg, Ca, Zn and Mo be additive element.
The method that mineral waste lubrication recovery of oil is adopted has:High-temperature cracking method, acid-hargil method, way of distillation etc..Wherein, high temperature Cracking process be by temperature and pressure effect realizing cracking of oil, thermal cracking is exactly the macromole for making one class of diesel oil using high temperature Hydrocarbon, decomposes cracking become the small molecule hydrocarbon of one class of gasoline, and under cracking conditions, hydro carbons is mainly decomposed and condensation two Class is reacted;Used oil thermal cracking product mainly has cracked gas, gasoline, diesel oil and residual oil etc.;Thermal cracking yield is higher, but energy consumption Height, contains more unsaturated hydrocarbons in product, stability is bad;Meanwhile, the condensation reaction occurred during Pintsch process can make Coke heavy in the pipeline of heating furnace, does not adopt Pintsch process in waste oil regeneration technology substantially.Acid-hargil method is to use concentrated sulphuric acid React with the undesirable constituentss in oil, generate acid sludge, after precipitation with separating of oil, now, oil then is used at hargil in acidity Reason, so that it may obtain that acid number is little, the oil product of good security;But after using sulphuric acid, oily hair life in part is esterified, and it is low that waste oil reclaims yield; The acid waste residue of by-product and other side-products, cause secondary pollution, according to《Waste lubricating oil recycles pollution control technology rule Model》(HJ607-2011), forbid at present being continuing with sulphuric acid/hargil method regeneration waste lubricating oil.
High temperature distillation method is different using Organic substance boiling point, and material is separated, and the technology is simple and reliable.Waste oil is heated, Lower boiling Organic substance is first distilled from tower top, and high boiling point stays in bottom.
Utility model content
The purpose of this utility model is that the purpose of this utility model is to research and develop a kind of process is simple, safety can Lean on, small investment, a kind of strong waste lubricating oil comprehensive recycling device of device motility.
In order to solve above-mentioned technical problem, the technical solution adopted in the utility model is:A kind of waste lubricating oil is comprehensively returned Receipts utilize device, and breakdown of emulsion Sedimentation tank that described device includes being sequentially connected, preheater, distillation column, condenser, after the condenser Light-weight fuel oil collection device and absorbent charcoal adsorber is connected to, wherein, in the breakdown of emulsion Sedimentation tank, stirring is provided with Waste oil is delivered to the preheater by pump by device, the breakdown of emulsion Sedimentation tank, and waste oil passes through feeding after preheater preheating It is pumped in distillation column, the bottom of the distillation column is provided with residual oil outlet.
Specifically, the bottom of the breakdown of emulsion Sedimentation tank is provided with waste water and dregs of fat discharger.
Technology of the processing meanss of waste lubricating oil of the present utility model using the high-temperature pressure-reduction way of distillation.In due to waste lubricating oil Containing a small amount of impurity and moisture, waste lubricating oil need to be carried out pretreatment, waste lubricating oil is transported to by breakdown of emulsion Sedimentation tank by pump In (Sedimentation tank is using covered and enclosed process), and add a certain amount of demulsifier (nonionic surfactant, Propylene Glycol polyoxy Ethylene polyethenoxy ether) carry out breakdown of emulsion.Breakdown of emulsion mainly replaces emulsifying agent of the absorption on oil-water interfaces by adding demulsifier, Reduce the elasticity and stickiness of interfacial film, so as to reduce interfacial film strength, accelerate the coalescence of drop, separate profit.Breakdown of emulsion It is 3.5kg that agent addition is waste lubricating oil demulsifier addition per ton.For preferably reaching the effect of breakdown of emulsion, during breakdown of emulsion It is stirred so that in oil product, each molecular motion acutely, with good mobility, reaches more preferable demulsification.Breakdown of emulsion is stirred The time is mixed for 20~30 minutes, temperature is room temperature.After through breakdown of emulsion process, stirring system is turned off, oil product standing separation is made, due to The density ratio water of oil product is little, through standing after, oil product is located at the upper strata of breakdown of emulsion Sedimentation tank, and water and other impurities are located at lower floor, through one The standing of section time, then the water and impurity (dregs of fat S1) of bottom are discharged.The waste lubricating oil of oily waste water W1 and the dregs of fat is separated Waste oil is delivered in preheater by pump, steam heating-up temperature is 90 DEG C, separates moisture content, is then pumped into distillating still through feeding In, heating up, control tower top temperature is at 200~250 DEG C or so.Slow programming rate is kept, bumping is prevented, lower boiling Organic substance First distill from tower top, condensed device condensation (about 20 DEG C of condensation temperature) is collected afterwards and obtains light-weight fuel oil, and condensation process is produced Raw incoagulable gas (G1) is with being discharged by aiutage after activated carbon adsorption.When the fuel oil color for distilling gradually becomes Deep, and after the residual oil outlet examination at random flash-point by distillation column bottom and viscosity, stop distillation, the remaining oil product in distillating still bottom is For residual oil (S2), in residual oil based on heavy oil composition, also contain a small amount of colloid, asphaltene precipitation thing, with certain calorific value, Belong to hazardous waste (HW11), otherwise processed.Meanwhile, fixed gas is processed using activated carbon adsorption.
In sum, waste lubricating oil comprehensive recycling device process is simple of the present utility model, safe and reliable, investment Few, device motility is strong.
Description of the drawings
Accompanying drawing described herein is used for providing further understanding to of the present utility model, constitutes the part of the application, Do not constitute to improper restriction of the present utility model, in the accompanying drawings:
Fig. 1 is the structured flowchart of waste lubricating oil comprehensive recycling device of the present utility model.
Specific embodiment
Describe this utility model, here signal of the present utility model below in conjunction with accompanying drawing and specific embodiment in detail Property embodiment and explanation be used for explaining this utility model, but be not intended as to restriction of the present utility model.
As shown in figure 1, a kind of waste lubricating oil comprehensive recycling device, described device includes the breakdown of emulsion sedimentation being sequentially connected Pond 1, preheater 2, distillation column 3, condenser 4, specifically, are the effect for preferably reaching breakdown of emulsion, are stirred during breakdown of emulsion Mix so that in oil product, each molecular motion acutely, with good mobility, reaches more preferable demulsification, the breakdown of emulsion sedimentation The bottom in pond 1 is provided with 12 discharger of waste water 11 and the dregs of fat;
Light-weight fuel oil collection device 41 and absorbent charcoal adsorber 42, wherein, institute is connected to after the condenser 4 State in breakdown of emulsion Sedimentation tank 1 and be provided with agitating device, waste oil is delivered to the preheater 2 by pump by the breakdown of emulsion Sedimentation tank, specifically , through breakdown of emulsion process after, turn off stirring system, make oil product standing separation, due to the density ratio water of oil product little, through standing after, Oil product is located at the upper strata of breakdown of emulsion Sedimentation tank, and water and other impurities are located at lower floor, through the standing of a period of time, then by the water of bottom and Impurity (dregs of fat S1) is discharged;
Waste oil is pumped in distillation column 3 by feeding after the preheating of the preheater 2, and the bottom of the distillation column 3 is arranged There is residual oil to export, residual oil outlet connection residual oil collection device 31.
Specifically, the waste lubricating oil for having separated oily waste water W1 and the dregs of fat is delivered to waste oil in preheater by pump, steam Heating-up temperature is 90 DEG C, separates moisture content, is then pumped in distillating still through feeding, heats up, and controls tower top temperature 200~250 DEG C or so, slow programming rate is kept, bumping is prevented, lower boiling Organic substance is first distilled from tower top, condensed device condensation (about 20 DEG C of condensation temperature) is collected afterwards and obtains light-weight fuel oil, and the incoagulable gas (G1) that condensation process is produced uses activated carbon adsorption Discharged by aiutage afterwards.When the fuel oil color for distilling gradually is deepened, and taken out by the residual oil outlet of distillation column bottom After testing flash-point and viscosity, stop distillation, the remaining oil product in distillating still bottom is residual oil (S2), in residual oil with heavy oil composition is Main, also containing a small amount of colloid, asphaltene precipitation thing, with certain calorific value, belong to hazardous waste (HW11), otherwise processed. Meanwhile, fixed gas is processed using activated carbon adsorption.
Above the technical scheme provided by this utility model embodiment is described in detail, used herein specifically Individual example is set forth to the principle of this utility model embodiment and embodiment, and the explanation of above example is only applicable to help Assistant solves the principle of this utility model embodiment;Simultaneously for one of ordinary skill in the art, implement according to this utility model Example, will change in specific embodiment and range of application, and in sum, this specification content should not be construed as To restriction of the present utility model.

Claims (2)

1. a kind of waste lubricating oil comprehensive recycling device, it is characterised in that:Described device includes the breakdown of emulsion sedimentation being sequentially connected Pond, preheater, distillation column, condenser, are connected to light-weight fuel oil collection device and activated carbon adsorption after the condenser Device, wherein, is provided with agitating device in the breakdown of emulsion Sedimentation tank, and waste oil is delivered to described pre- by the breakdown of emulsion Sedimentation tank by pump Hot device, waste oil are pumped in distillation column by feeding after preheater preheating, and the bottom of the distillation column is provided with residual oil Outlet.
2. a kind of waste lubricating oil comprehensive recycling device according to claim 1, it is characterised in that:The breakdown of emulsion sedimentation The bottom in pond is provided with waste water and dregs of fat discharger.
CN201620883536.7U 2016-08-15 2016-08-15 A kind of waste lubricating oil comprehensive recycling device Active CN206014814U (en)

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Application Number Priority Date Filing Date Title
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108341477A (en) * 2018-02-09 2018-07-31 无锡日月水处理有限公司 The method of Combined Treatment industrial emissions
CN109111011A (en) * 2018-10-30 2019-01-01 上海天汉环境资源有限公司 A kind of waste emulsified mixture innocuity disposal system and demulsifier
CN111154510A (en) * 2020-01-22 2020-05-15 韦祖军 Waste mineral oil treatment system and application method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108341477A (en) * 2018-02-09 2018-07-31 无锡日月水处理有限公司 The method of Combined Treatment industrial emissions
CN109111011A (en) * 2018-10-30 2019-01-01 上海天汉环境资源有限公司 A kind of waste emulsified mixture innocuity disposal system and demulsifier
CN111154510A (en) * 2020-01-22 2020-05-15 韦祖军 Waste mineral oil treatment system and application method thereof

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