CN206008110U - A kind of gas-liquid separator for producing chloropropyl triethoxysilane - Google Patents
A kind of gas-liquid separator for producing chloropropyl triethoxysilane Download PDFInfo
- Publication number
- CN206008110U CN206008110U CN201620971572.9U CN201620971572U CN206008110U CN 206008110 U CN206008110 U CN 206008110U CN 201620971572 U CN201620971572 U CN 201620971572U CN 206008110 U CN206008110 U CN 206008110U
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- gas
- liquid
- knockout drum
- baffle plate
- producing
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Abstract
A kind of gas-liquid separator for producing chloropropyl triethoxysilane, is made up of some, and the gas-liquid separator includes：Knockout drum, gas-liquid mixture import, deflector, water circulating pump, macropore baffle plate, mesopore baffle plate, aperture baffle plate, pressure gauge, nitrogen inlet, liquid outlet, gas vent, condenser and vavuum pump, the beneficial effects of the utility model are：By the structure of flow distribution plate in the gas-liquid separator for producing chloropropyl triethoxysilane, gas-liquid mixture can be made to be laid on flow distribution plate, and heat, mixing gas in a liquid is made to overflow rapidly, and by the baffle plate of different pore size to gas in liquid particles filter, the less liquid vapour carried in gas is condensed back in knockout drum eventually through condenser, reach the purpose of gas-liquid separation.
Description
Technical field
The utility model is related to a kind of gas-liquid separator, is used for producing chloropropyl triethoxy more particularly, to a kind of
The gas-liquid separator of silane.
Background technology
When chloropropyl triethoxysilane is produced, the product in course of reaction is often in the form of gas-liquid mixed phase
Occur, before follow-up distilation operation is carried out, need to be separated gas and liquid, to avoid to subsequent operation
Affect, as often containing small bubble, if routinely separated, the not thorough of gas-liquid separation will necessarily be caused in liquid
Bottom, so that affect follow-up process.
Utility model content
Based on gas-liquid separation problem of the chloropropyl triethoxysilane in production, the purpose of this utility model is to provide
A kind of gas-liquid separator for producing chloropropyl triethoxysilane.
The purpose of this utility model is mainly realized by following technical scheme.
A kind of gas-liquid separator for producing chloropropyl triethoxysilane, which includes：Knockout drum, gas-liquid mixture enter
Mouth, deflector, water circulating pump, macropore baffle plate, mesopore baffle plate, aperture baffle plate, pressure gauge, nitrogen inlet, liquid outlet, gas go out
Mouth, condenser and vavuum pump, the knockout drum are cylindrical structure, seal down through arc surface, the gas-liquid mixture import
The side of knockout drum is located at, the deflector is middle high, and the low platy structure in edge is on the inwall of knockout drum, interior
Portion is provided with heating tank, deflector is heated by water circulating pump, and the macropore baffle plate, mesopore baffle plate and aperture baffle plate are under
Supreme uniform have macropore, mesopore and aperture thereon on the inwall of knockout drum, for the liquid in air-flow
Grain is filtered, and installed in the upper surface of knockout drum, the nitrogen inlet is located at the side of knockout drum to the pressure gauge, for right
Tonifying Qi supercharging is carried out in knockout drum, and the liquid outlet is located at knockout drum bottom centre position, and the gas vent is located at and separates
Tank upper end centre position, the condenser are connected with gas vent, and the gas in knockout drum are extracted by vavuum pump,
And by extraction after gas be further processed.
Preferably, the upper surface of the deflector is maintained an equal level with the lower surface of gas-liquid mixture import, is arranged close to gaseous mixture
Liquid entrance point, leaves certain gap away from gas-liquid mixture entrance point with top tank structure is separated.
Preferably, the macropore baffle plate, mesopore baffle plate and aperture baffle plate be arc surface structure, and the jag of arc surface to
Under.
Preferably, the gas-liquid mixture import, deflector and nitrogen inlet are located at the lower section of macropore baffle plate, and nitrogen inlet
It is located at the top of gas-liquid mixture import.
Preferably, the condenser is vertically installed at the top of knockout drum, condensed liquid is entered in knockout drum.
Compared with prior art, a kind of gas-liquid separator for producing chloropropyl triethoxysilane of the present utility model
Beneficial effect be：
By the structure of flow distribution plate in the gas-liquid separator for producing chloropropyl triethoxysilane, can make to mix
Close gas-liquid to be laid on flow distribution plate, and heat, mixing gas in a liquid is overflowed rapidly, and by the baffle plate of different pore size
Liquid particles in gas are filtered, and are condensed back the less liquid vapour carried in gas eventually through condenser and are divided
In tank, the purpose of gas-liquid separation is reached.
Description of the drawings
Fig. 1 is the gas-liquid for producing chloropropyl triethoxysilane point constituted according to the utility model preferred embodiment
Structural representation from device.
In figure：
1- knockout drums；2- gas-liquid mixture imports；3- deflectors；4- water circulating pumps；5- macropore baffle plates；6- mesopore baffle plates；7-
Aperture baffle plate；8- pressure gauges；9- nitrogen inlets；10- liquid outlets；11- gas vents；12- condensers；13- vavuum pumps.
Specific embodiment
Hereinafter, refer to the attached drawing is described in detail to specific embodiment of the utility model, detailed according to these
Thin description, one of ordinary skill in the art are it can be clearly understood that the utility model, and can implement the utility model.Do not disobeying
In the case of back of the body the utility model principle, the feature in each different embodiment can be combined to obtain new embodiment party
Formula, or some of some embodiments feature is substituted, obtain other preferred embodiment.
Embodiment 1：Fig. 1 shows and be used for producing three second of chloropropyl according to one kind that the utility model preferred embodiment is constituted
The structural representation of the gas-liquid separator of TMOS.As shown in figure 1, a kind of gas for producing chloropropyl triethoxysilane
The structural representation of liquid/gas separator, which is made up of some.The gas-liquid separator includes：Knockout drum 1, gas-liquid mixture import
2nd, deflector 3, water circulating pump 4, macropore baffle plate 5, mesopore baffle plate 6, aperture baffle plate 7, pressure gauge 8, nitrogen inlet 9, liquid outlet
10th, gas vent 11, condenser 12 and vavuum pump 13, the knockout drum 1 is cylindrical structure, and stainless steel inside and outside is scribbled
Waterproof anti-corrosion coating, down through arc surface solder up, 2 welded and installed of gas-liquid mixture import is in the side of knockout drum 1
Face, the deflector 3 is middle high, the low platy structure in edge, welded and installed on the inwall of knockout drum 1, inside be provided with plus
Heat channel, is heated to deflector 3 by water circulating pump 4, and the lower surface of the upper surface of deflector 3 and gas-liquid mixture import 2
Maintain an equal level, be arranged close to 2 end of gas-liquid mixture import, away from 2 end of gas-liquid mixture import and 1 inwall of knockout drum leave certain between
Gap, uniform welding is arranged on the inwall of knockout drum 1, no from bottom to up for the macropore baffle plate 5, mesopore baffle plate 6 and aperture baffle plate 7
Rust steel matter, scribbles erosion shield, is arc surface structure, and the jag of arc surface is downwards, has thereon a diameter of
The hole of 2mm, 1mm and 0.5mm, filters for the liquid particles in air-flow, and the pressure gauge 8 is arranged on knockout drum 1
Upper surface, for detecting to the pressure in knockout drum 1, the nitrogen inlet 9 sealing be spirally connected installed in the side of knockout drum 1
Face, position are higher than gas-liquid mixture import 2, for carrying out supplementing protection nitrogen and supercharging, and gas-liquid mixture import in knockout drum 1
2nd, deflector 3 and nitrogen inlet 9 are located at the lower section of macropore baffle plate 5, and the liquid outlet 10 is welded on 1 bottom interposition of knockout drum
Put, the gas vent 11 is welded on 1 upper end centre position of knockout drum, the condenser 12 is connected with gas vent 11, vertically
Installed in the top of knockout drum 1, condensed liquid is enable smoothly to enter in knockout drum 1, the vavuum pump 13 is through condensation
Device 12 is extracted to the gas in knockout drum 1, and by extraction after gas be further processed.
Although being described to the utility model above by referring to specific embodiment, art technology people
Member is it should be appreciated that in the utility model principle disclosed and scope, can be directed to the disclosed configuration of the utility model and details
Make many modifications.Protection domain of the present utility model is determined by appended claim, and claim is intended to
Whole modifications that the equivalent literal meaning of technical characteristic or scope are included in claim.
Claims (5)
1. a kind of gas-liquid separator for producing chloropropyl triethoxysilane, is made up of some, the gas-liquid separation
Device includes：Knockout drum (1), gas-liquid mixture import (2), deflector (3), water circulating pump (4), macropore baffle plate (5), mesopore baffle plate
(6), aperture baffle plate (7), pressure gauge (8), nitrogen inlet (9), liquid outlet (10), gas vent (11), condenser (12) and
Vavuum pump (13), it is characterised in that described knockout drum (1) is cylindrical structure, seals down through arc surface, the gaseous mixture
Liquid import (2) is located at the side of knockout drum (1), and described deflector (3) are middle high, the low platy structure in edge, installed in point
On the inwall of tank (1), inside is provided with heating tank, deflector (3) is heated by water circulating pump (4), the macropore gear
Plate (5), mesopore baffle plate (6) and aperture baffle plate (7) are uniformly arranged on the inwall of knockout drum (1) from bottom to up, are opened respectively thereon
There are macropore, mesopore and aperture, filter for the liquid particles in air-flow, described pressure gauge (8) are arranged on knockout drum (1)
Upper surface, described nitrogen inlet (9) are located at the side of knockout drum (1), for carrying out tonifying Qi supercharging, institute in knockout drum (1)
Liquid outlet (10) is stated positioned at knockout drum (1) bottom centre position, described gas vent (11) are located in the middle of knockout drum (1) upper end
Position, condenser (12) are connected with gas vent (11), and the gas in knockout drum (1) are carried out by vavuum pump (13)
Extract, and by extraction after gas be further processed.
2. the gas-liquid separator for producing chloropropyl triethoxysilane is used for as claimed in claim 1, it is characterised in that water conservancy diversion
The upper surface of plate (3) is maintained an equal level with the lower surface of gas-liquid mixture import (2), is arranged close to gas-liquid mixture import (2) end, away from mixed
Close gas-liquid import (2) end certain gap is left with knockout drum (1) inwall.
3. the gas-liquid separator for producing chloropropyl triethoxysilane is used for as claimed in claim 1, it is characterised in that macropore
Baffle plate (5), mesopore baffle plate (6) and aperture baffle plate (7) are arc surface structure, and the jag of arc surface is downward.
4. the gas-liquid separator for producing chloropropyl triethoxysilane is used for as claimed in claim 1, it is characterised in that mixing
Gas-liquid import (2), deflector (3) and nitrogen inlet (9) are located at the lower section of macropore baffle plate (5), and nitrogen inlet (9) is located at mixing
The top of gas-liquid import (2).
5. the gas-liquid separator for producing chloropropyl triethoxysilane is used for as claimed in claim 1, it is characterised in that condensation
Device (12) is vertically installed at the top of knockout drum (1), condensed liquid is entered in knockout drum (1).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620971572.9U CN206008110U (en) | 2016-08-29 | 2016-08-29 | A kind of gas-liquid separator for producing chloropropyl triethoxysilane |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620971572.9U CN206008110U (en) | 2016-08-29 | 2016-08-29 | A kind of gas-liquid separator for producing chloropropyl triethoxysilane |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206008110U true CN206008110U (en) | 2017-03-15 |
Family
ID=58254149
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620971572.9U Expired - Fee Related CN206008110U (en) | 2016-08-29 | 2016-08-29 | A kind of gas-liquid separator for producing chloropropyl triethoxysilane |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206008110U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109839426A (en) * | 2017-11-28 | 2019-06-04 | 中国科学院大连化学物理研究所 | Method that is a kind of while improving transference tube interior air-flow and temperature uniformity |
| CN111727351A (en) * | 2017-09-14 | 2020-09-29 | 查特能源化工股份有限公司 | Mixed refrigerant condenser outlet manifold separator |
-
2016
- 2016-08-29 CN CN201620971572.9U patent/CN206008110U/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111727351A (en) * | 2017-09-14 | 2020-09-29 | 查特能源化工股份有限公司 | Mixed refrigerant condenser outlet manifold separator |
| CN111727351B (en) * | 2017-09-14 | 2023-03-28 | 查特能源化工股份有限公司 | Mixed refrigerant condenser outlet manifold separator |
| CN109839426A (en) * | 2017-11-28 | 2019-06-04 | 中国科学院大连化学物理研究所 | Method that is a kind of while improving transference tube interior air-flow and temperature uniformity |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170315 Termination date: 20180829 |