CN205981978U - Fracturing fluid insoluble solid in water and residue survey device - Google Patents

Fracturing fluid insoluble solid in water and residue survey device Download PDF

Info

Publication number
CN205981978U
CN205981978U CN201620569293.XU CN201620569293U CN205981978U CN 205981978 U CN205981978 U CN 205981978U CN 201620569293 U CN201620569293 U CN 201620569293U CN 205981978 U CN205981978 U CN 205981978U
Authority
CN
China
Prior art keywords
filter
fracturing fluid
residue
water
measure device
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201620569293.XU
Other languages
Chinese (zh)
Inventor
王佳
李俊华
董晓军
王帅
崔国涛
冯虎强
张建国
田世伟
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shaanxi Chemical Research Institute Co ltd
Original Assignee
Shaanxi Research Design Institute of Petroleum and Chemical Industry
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shaanxi Research Design Institute of Petroleum and Chemical Industry filed Critical Shaanxi Research Design Institute of Petroleum and Chemical Industry
Priority to CN201620569293.XU priority Critical patent/CN205981978U/en
Application granted granted Critical
Publication of CN205981978U publication Critical patent/CN205981978U/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Separation Using Semi-Permeable Membranes (AREA)

Abstract

The utility model provides a fracturing fluid insoluble solid in water and residue survey device, includes filtering support, and filtering component passes through the valve and connects filtering support, and filtering support connects liquid collection bottle, and liquid collection bottle connects the vacuum pump, and when survey fracturing fluid insoluble solid in water and residue, the department of being connected puts the filter membrane above filter bowl below and the filter, and the air cock is continuous with the vacuum pump. Pouring into broken glue solution into filter bowl, opening the switch on the filtering support, open the vacuum pump, broken glue solution leads to filtration membrane and flows in the collection liquid chamber with filtering support, after treating among the filter bowl that broken glue solution is whole and flowing in the collection liquid chambers, washes filter bowl 2~3 times with distilled water, takes off the filter membrane and dries and weigh, leads to around the filtration membrane insoluble solid in water and residue that the quality difference calculated the fracturing fluid, simple structure, and convenient to use can measure fracturing fluid insoluble solid in water and residue fast, has improved fracturing fluid insoluble solid in water and residue survey efficiency.

Description

A kind of fracturing fluid water-insoluble and residue measure device
Technical field
This utility model belongs to residue determination techniques field and in particular to a kind of fracturing fluid water-insoluble and residue measure dress Put.
Background technology
Fracturing fluid be fracturing transform oil-gas Layer during working solution, play transmission pressure, formation and extend crack, Carry the effect of proppant.Fracturing fluid and its performance are the key factors affecting pressure break success or failure.At present, widely used both at home and abroad Fracturing fluid system can be divided into aqueous fracturing fluid, foam fracturing fluid, oil base fracturing fluid and Emulsified fracturing fluid.
Breaking glue solution residue is to cause one of principal element of reservoir damage, water-insoluble and residue main with thickening agent used In the broken colloidality of water insoluble matter content and fracturing fluid system can be relevant.Generally fracturing fluid water-insoluble and residue adopt centrifuge Measure, by the water-insoluble calculating fracturing fluid of poor quality and residue before and after centrifuge tube after breaking glue solution centrifugation.But in reality In operation there is following defect in said determination device:Centrifuge tube small volume, pours into during breaking glue solution inevitably toward centrifuge tube Have unrestrained, impact analysis precision;Solidss can be stained with centrifuge tube drying course mesospore, need to rinse, more bother.These lack Fall into have impact on breaking glue solution residue mensure work efficiency, reduce analysis precision so that a kind of more preferable water-insoluble and The device that residue measures is solving these problems.
Content of the invention
In order to overcome the above-mentioned deficiencies of the prior art, the purpose of this utility model there is provided a kind of fracturing fluid water-insoluble And the mensure device of residue, carry out sucking filtration using the negative pressure extracting breaking glue solution that vacuum pump causes.This device can quickly test out pressure Split water-insoluble and the residue of liquid, and test result is accurately, be easy to operate, greatly reduce testing cost, be answering of fracturing fluid With providing theoretical basiss.
To achieve these goals, the technical solution adopted in the utility model is:
A kind of fracturing fluid water-insoluble and residue measure device, and including filter holder, filter assemblies were connected by valve Filter support, filter holder connects liquid-collecting bottle, and liquid-collecting bottle connects vacuum pump.
Described filter assemblies are consisted of the filter membrane filter that is rotatably connected filter bowl, and filter is connected with valve.
Described filter membrane is one or more layers film.
Described filter bowl and filter are attached by screw thread or buckle.
Described filter bowl, filter, valve are stainless steel, and filter bowl thin-wall circular cylindrical structure has scale.
Between 25~80mm, the filter membrane of single or multiple lift different size is filtered described filter membrane diameter simultaneously.
Described filter holder is provided with 1 to 4 branch road, and each branch road described is passed through valve and is connected with filter tip.
Described liquid-collecting bottle has fixed mount, and bottom corner adds rubber cushion.
Described vacuum pump adopts oil-free double piston design, subsidiary vacuum table adjustable negative pressure.
The beneficial effects of the utility model are:
This device can realize the mensure of fracturing fluid water-insoluble and residue, and compared with prior art, this practicality is new Type can quickly measure gel breaker water-insoluble and residue, and measuring accuracy is high, and testing procedure is simple, reduces testing cost, profit In popularization.
Brief description
Fig. 1 is structural representation of the present utility model.
Fig. 2 is the sectional view of filter bowl of the present utility model.
Fig. 3 is the sectional view of filter of the present utility model.
In figure:1 is filter bowl;2 is film;3 is head;4 is filter support;5 is liquid bottle;6 is vacuum pump;7 is filter assemblies;8 are Valve.
Specific embodiment
Below in conjunction with the accompanying drawings this utility model is done with detailed narration.
Include as shown in Figure 1:A kind of fracturing fluid water-insoluble and residue measure device, including filter assemblies 7, filter assemblies 7 connect filter holder 4 by valve 8, and filter holder 4 connects liquid-collecting bottle 5, and liquid-collecting bottle 5 connects vacuum pump 6.
Described filter assemblies 7 are consisted of filter membrane 2 filter 3 that is rotatably connected filter bowl 1, and filter 3 is connected with valve 8.
Described filter membrane 2 is one or more layers film.
Described filter bowl 1 and filter 3 are attached by screw thread or buckle.
Described filter bowl 1, filter 3, valve 8 are stainless steel, and filter bowl 1 thin-wall circular cylindrical structure has scale.
Between 25~80mm, the filter membrane 2 of single or multiple lift different size is filtered described filter membrane 2 diameter simultaneously.
Described filter holder 4 is provided with 1 to 4 branch road, and described branch road is connected with filter 3 end.
Described liquid-collecting bottle 5 has fixed mount, and bottom corner adds rubber cushion.
Described vacuum pump 6 adopts oil-free double piston design, subsidiary vacuum table adjustable negative pressure.
Filter bowl 1 is thin-wall circular cylindrical structure, and arrival end is hatch frame, opens up central through hole for pressure break liquor stream inside it Logical, the port of export is connection end, and fracturing fluid enters from arrival end and flows out filter bowl 1 from the port of export.
Filter bowl 1 is stainless steel, has scale thereon, for reading liquid volume in filter bowl 1.
Filter 3 is conical structure, and arrival end is connection end, opens up central through hole and circulates for fracturing fluid, go out inside it Mouth end is shunk and is diminished for connecting filter holder 4.Wherein, the port of export size phase of the arrival end of shown filter 3 and filter bowl 1 Join, connect filter bowl 1 and filter 3.
Filter 3 is stainless steel it is ensured that the robustness of filter 3.
As Fig. 2 and 3 shows a kind of way of realization of filter bowl 1 and filter 3, the port of export excircle of filter bowl 1 is provided with spiral shell Stricture of vagina, the arrival end inner periphery of filter 3 is provided with female thread, and described filter bowl 1 and filter 3 are attached by screw thread.
The chuck of 2-4 evagination is arranged with the port of export excircle of filter bowl 1, symmetrical on the arrival end inner periphery of filter 3 It is provided with the button platform with chuck quantity identical indent, described filter bowl 1 and filter 3 pass through chuck and buckle the card of platform and be attached.
Filter membrane 2 is filter membrane between 25~80mm for the diameter, one or more layers filter membrane 2 be folded in filter bowl 1 and filter 3 it Between.The filter membrane 2 of single or multiple lift different size is filtered simultaneously.
Filter holder 4 includes branch road and Zong Lu, and branch road is perpendicular with total road, and branch road is fixedly connected with the port of export of filter 3, It is further that described filter holder 4 is provided with 1~4 branch road, and branch road is provided with valve, and valve adopts stainless steel material, use In the connection being switched on or switched off between filter 3 and filter holder 4.
Liquid-collecting bottle 5 is fixed by fixed mount, and one end connects total road of filter holder 4, and the other end connects vacuum pump 6, its Bottom corner adds rubber cushion.
Vacuum pump 6 adopts oil-free double piston design, subsidiary vacuum table adjustable negative pressure.
Operation principle of the present utility model is:
During work, take gel breaker fracturing fluid after breaking gel standby first;Below filter bowl 1 with filter 3 above connection Put the filter membrane 2 of required specification;The valve 8 opened on filter holder 4 opens vacuum pump 6, falls fracturing fluid after breaking gel manually Enter in filter bowl 1;Fracturing fluid passes through filter membrane 2 and filter holder 4 flows in the liquid-collecting bottle 5 of lower section, and remaining residue stays filter membrane 2 On, after in filter bowl 1, breaking glue solution all flows into liquid-collecting bottle 5, with distilled water flushing filter bowl 2~3 times;After sucking filtration is complete, treat filter bowl 1 Interior liquid turns off vacuum pump 6 after all flowing in liquid-collecting bottle 5.Filter membrane 2 is taken out and dries, dry the quality obtaining and formula Fracturing fluid volume ratio, obtains water-insoluble and residue.

Claims (8)

1. a kind of fracturing fluid water-insoluble and residue measure device, including filter holder(4)It is characterised in that filter assemblies(7) By valve(8)Connect filter holder(4), filter holder(4)Connect liquid-collecting bottle(5), liquid-collecting bottle(5)Connect vacuum pump(6);Cross Filter assembly(7)By filter bowl(1)By filter membrane(2)Be rotatably connected filter(3)Composition, filter(3)With valve(8)Connect, filter bowl(1) Thin-wall circular cylindrical structure, has scale.
2. a kind of fracturing fluid water-insoluble according to claim 1 and residue measure device it is characterised in that described filter Film(2)For one or more layers film.
3. a kind of fracturing fluid water-insoluble according to claim 1 and residue measure device it is characterised in that described filter bowl (1)And filter(3)It is attached by screw thread or buckle.
4. a kind of fracturing fluid water-insoluble according to claim 1 and 2 and residue measure device it is characterised in that described Filter bowl(1), filter(3), valve(8)For stainless steel.
5. a kind of fracturing fluid water-insoluble according to claim 1 and residue measure device it is characterised in that described filter membrane (2)Diameter between 25~80mm, the filter membrane of single or multiple lift different size(2)Filtered simultaneously.
6. a kind of fracturing fluid water-insoluble according to claim 1 and residue measure device it is characterised in that described filtration Support(4)It is provided with 1 to 4 branch road, each branch road described passes through valve(8)With filter(3)Most advanced and sophisticated connection.
7. a kind of fracturing fluid water-insoluble according to claim 1 and residue measure device it is characterised in that described liquid collecting Bottle(5)There is fixed mount, bottom corner adds rubber cushion.
8. a kind of fracturing fluid water-insoluble according to claim 1 and residue measure device it is characterised in that described vacuum Pump(6)Using oil-free double piston design, subsidiary vacuum table adjustable negative pressure.
CN201620569293.XU 2016-06-14 2016-06-14 Fracturing fluid insoluble solid in water and residue survey device Active CN205981978U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201620569293.XU CN205981978U (en) 2016-06-14 2016-06-14 Fracturing fluid insoluble solid in water and residue survey device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201620569293.XU CN205981978U (en) 2016-06-14 2016-06-14 Fracturing fluid insoluble solid in water and residue survey device

Publications (1)

Publication Number Publication Date
CN205981978U true CN205981978U (en) 2017-02-22

Family

ID=58020650

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201620569293.XU Active CN205981978U (en) 2016-06-14 2016-06-14 Fracturing fluid insoluble solid in water and residue survey device

Country Status (1)

Country Link
CN (1) CN205981978U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2021017592A1 (en) * 2019-07-31 2021-02-04 山东新希望六和集团有限公司 Method for measuring water insoluble substances in sodium humate

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2021017592A1 (en) * 2019-07-31 2021-02-04 山东新希望六和集团有限公司 Method for measuring water insoluble substances in sodium humate

Similar Documents

Publication Publication Date Title
CN207610824U (en) Novel valve sealing property testing equipment
CN209264364U (en) A kind of medical test sampler
CN205948516U (en) Horizontal type gas and liquid seperator
CN105806750B (en) Method for measuring matching property of microspheres and pore throats of oil reservoirs
CN205981978U (en) Fracturing fluid insoluble solid in water and residue survey device
CN205730480U (en) A kind of two-part plankton settler
CN207950815U (en) Magnetic-type filter
CN206848000U (en) A kind of oil sample sampler
CN105651554A (en) Collection device and collection method of concrete pore solution
CN218710571U (en) Osteoporosis auxiliary diagnosis device based on exosome
CN106267949A (en) Can the Quick suction filtration device of in line liquid
CN205538343U (en) Dirt mite allergen detection device
CN102519840B (en) Viscose filtering resistance detection method
CN204705644U (en) A kind of cardio-vascular clinical diagnostic device
CN205473751U (en) Cord blood stem cells isolated device
CN207742118U (en) A kind of pigment media-resistant experimental rig
CN208568705U (en) A kind of pharmacological experiment titration outfit
CN206270451U (en) Movable submersible pump Insulation Test container
CN210571532U (en) Water sampling device
CN205856152U (en) A kind of modified form suction tube type portable water purifier
CN109540603A (en) Sampling apparatus for the acquisition of skin surface chemical pollutant
CN200960151Y (en) Negative pressure filter for artificial abortion
CN219475150U (en) Active carbon collection tube with pressure filtration function
CN207396455U (en) A kind of sample detection, recycling and the integrated food inspection equipment of cleaning
CN108709842A (en) Oil-water separation metering method and device

Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
CP01 Change in the name or title of a patent holder

Address after: No.61 Xiyan Road, Xi'an City, Shaanxi Province 710054

Patentee after: Shaanxi Chemical Research Institute Co.,Ltd.

Address before: No.61 Xiyan Road, Xi'an City, Shaanxi Province 710054

Patentee before: SHAANXI RESEARCH DESIGN INSTITUTE OF PETROLEUM CHEMICAL INDUSTRY

CP01 Change in the name or title of a patent holder