CN205965091U - Crystallization reaction kettle - Google Patents
Crystallization reaction kettle Download PDFInfo
- Publication number
- CN205965091U CN205965091U CN201620947385.7U CN201620947385U CN205965091U CN 205965091 U CN205965091 U CN 205965091U CN 201620947385 U CN201620947385 U CN 201620947385U CN 205965091 U CN205965091 U CN 205965091U
- Authority
- CN
- China
- Prior art keywords
- blade
- inner tube
- tube wall
- conically shaped
- shaped bottom
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The utility model discloses a crystallization reaction kettle, including a cauldron section of thick bamboo, a cauldron section of thick bamboo has cylindrical barrel and toper bobbin base, and cylindrical barrel and toper bobbin base have the double -layer barrel wall, double -layer barrel wall intermediate formation coolant liquid business turn over chamber, and its characterized in that: be equipped with the (mixing) shaft in the cauldron section of thick bamboo, the last axle head of (mixing) shaft expose in a cauldron section of thick bamboo and with gear motor's output shaft, the (mixing) shaft from top to bottom in proper order the installation be equipped with first, and secondly, the third, the fourth, the the 5th and the 6th paddle, it is first, and secondly, third and fourth paddle have the inner tube wall of outside blade surface corresponding circle cylindricality barrel respectively, it is first, and secondly, the regional inner tube wall that covers whole cylindrical barrel of scraping of third and fourth paddle, the the 5th and the 6th paddle has the inner tube wall that outside blade surface corresponds the toper bobbin base respectively, the regional inner tube wall that covers whole toper bobbin base of scraping of the 5th and the 6th paddle. The utility model discloses it is little that the dead angle is piled up in the crystallization, does benefit to crystallization speed and improve.
Description
Technical field
This utility model is related to a kind of reactor and in particular to a kind of tie for forcing in chemical products manufacturing process to cool down
Brilliant crystallization reaction kettle.
Background technology
In chemical industry, the manufacturing process of such as tetrabutyl ammonium bromide, tetrabutyl ammonium bromide needs in crystallization reaction kettle
Inside carry out compulsory crystallisation by cooling, crystallization reaction kettle has cylindrical tube and conically shaped bottom, cylindrical tube and conically shaped bottom
There is double-deck barrel, double-deck barrel intermediate formation coolant passes in and out chamber, by the entrance of coolant to four in crystallization reaction kettle
Butylammonium bromide carries out forcing cooling to be allowed to crystallize.But, the crystallization reaction kettle of prior art, the crystallization of kettle cylinder inwall is piled up
Dead angle is many, and in crystallization process, crystalline solid can be attached to and can not strike off in time on barrel, and crystalline solid can block coolant and four fourths
Conduction of heat between base ammonium bromide, therefore crystallization rate are slow.
Content of the invention
In view of the shortcomings of the prior art, the purpose of this utility model aims to provide a kind of crystallization little, profit of piling up dead angle
The crystallization reaction kettle improving in crystallization rate.
This utility model adopts the following technical scheme that to complete:
Crystallization reaction kettle, including kettle cylinder, kettle cylinder has cylindrical tube and conically shaped bottom, cylindrical tube and conically shaped bottom
There is double-deck barrel, double-deck barrel intermediate formation coolant turnover chamber it is characterised in that:It is provided with shaft, shaft in kettle cylinder
Upper axle head expose to kettle cylinder and be connected with the output shaft of reducing motor, shaft installs successively up and down and is provided with first, second, the
3rd, the four, the 5th and the 6th blade, first, second, third and fourth blade is respectively provided with outer lobe face and corresponds to cylindrical tube
Inner tube wall, the inner tube wall of the whole cylindrical tube of scraping region overlay of first, second, third and fourth blade, the 5th He
6th blade is respectively provided with the inner tube wall at the corresponding conically shaped bottom in outer lobe face, and the scraping region overlay of the 5th and the 6th blade is whole
The inner tube wall at conically shaped bottom.
First, second, third, fourth and fifth blade is single-blade leaf, and the 6th blade is double blade.
The switching position at cylindrical tube and conically shaped bottom is provided with the 7th blade, and the 7th blade has outside narrow leaf face and corresponds to
Cylindrical tube and the inner tube wall at conically shaped bottom switching position, and there is the upper table of the corresponding kettle cylinder internal thermometer pipe in bottom blade face
Face, temperature gauge pipe laterally passes inside and outside kettle cylinder from the switching position at cylindrical tube and conically shaped bottom.
After technique scheme, this utility model is provided with shaft inside kettle cylinder and installs many on shaft
Piece blade, the inner tube wall of the whole cylindrical tube of scraping region overlay of first, second, third and fourth blade, the 5th and
The inner tube wall at the scraping region overlay whole conically shaped bottom of six blades, the scraping area of the 7th blade then covers cylindrical tube and cone
The inner tube wall at shape cylinder bottom switching position and the upper surface of kettle cylinder internal thermometer pipe, thus realize crystallizing the minimum piling up dead angle
Change, improve beneficial to crystallization rate.
Brief description
This utility model has drawings described below:
Fig. 1 is structural representation of the present utility model.
Specific embodiment
As illustrated, crystallization reaction kettle of the present utility model, including kettle cylinder 3, kettle cylinder 3 has cylindrical tube 4 and taper
Cylinder bottom 7, cylindrical tube 4 and conically shaped bottom 7 have double-deck barrel, and double-deck barrel intermediate formation coolant passes in and out chamber 5, kettle cylinder 3
Inside it is provided with shaft 2, the upper axle head of shaft 2 exposes to kettle cylinder 3 and the output shaft with reducing motor 1 is connected, and shaft is about 2
Install successively and be provided with the first blade 11, the second blade 12, the 3rd blade 13, the 4th blade 14, the 5th blade 15 and the 6th blade
16, first, second, third and fourth blade is respectively provided with the inner tube wall of the corresponding cylindrical tube 4 in outer lobe face, and first and the
2nd, second and the three, the third and fourth blade have in the height direction overlapped, so can achieve first, second, third
With the inner tube wall of the whole cylindrical tube of scraping region overlay 4 of the 4th blade, the 5th and the 6th blade is respectively provided with outer lobe
The inner tube wall at the corresponding conically shaped bottom 7 in face, the 5th and the 6th blade has overlapped in the height direction, so can achieve the 5th
With the inner tube wall at the scraping region overlay whole conically shaped bottom 7 of the 6th blade, first, second, third, fourth and fifth blade is
Single-blade leaf, the 6th blade is double blade;The switching position at cylindrical tube 4 and conically shaped bottom 7 is provided with the 7th blade 17, the 7th oar
Leaf 17 has the corresponding cylindrical tube 4 in outside narrow leaf face and the inner tube wall at conically shaped bottom 7 switching position, and has bottom blade face pair
Answer the upper surface of kettle cylinder internal thermometer pipe 6, temperature gauge pipe 6 is horizontal from the switching position at cylindrical tube 4 and conically shaped bottom 7
Pass inside and outside kettle cylinder.
Claims (3)
1. crystallization reaction kettle, including kettle cylinder, kettle cylinder has cylindrical tube and conically shaped bottom, cylindrical tube and conically shaped bottom tool
Have a double-deck barrel, double-deck barrel intermediate formation coolant turnover chamber it is characterised in that:It is provided with shaft in kettle cylinder, shaft
Upper axle head is exposed to kettle cylinder and is connected with the output shaft of reducing motor, and shaft installs successively up and down and be provided with first, second, the
3rd, the four, the 5th and the 6th blade, first, second, third and fourth blade is respectively provided with outer lobe face and corresponds to cylindrical tube
Inner tube wall, the inner tube wall of the whole cylindrical tube of scraping region overlay of first, second, third and fourth blade, the 5th He
6th blade is respectively provided with the inner tube wall at the corresponding conically shaped bottom in outer lobe face, and the scraping region overlay of the 5th and the 6th blade is whole
The inner tube wall at conically shaped bottom.
2. crystallization reaction kettle as claimed in claim 1 it is characterised in that:First, second, third, fourth and fifth blade is
Single-blade leaf, the 6th blade is double blade.
3. crystallization reaction kettle as claimed in claim 1 it is characterised in that:The switching position at cylindrical tube and conically shaped bottom sets
There is the 7th blade, the 7th blade has the inner tube wall at the corresponding cylindrical tube in outside narrow leaf face and conically shaped bottom switching position, and
There is the upper surface of the corresponding kettle cylinder internal thermometer pipe in bottom blade face, temperature gauge pipe is from the switching of cylindrical tube and conically shaped bottom
Position laterally passes inside and outside kettle cylinder.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201620947385.7U CN205965091U (en) | 2016-08-26 | 2016-08-26 | Crystallization reaction kettle |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201620947385.7U CN205965091U (en) | 2016-08-26 | 2016-08-26 | Crystallization reaction kettle |
Publications (1)
Publication Number | Publication Date |
---|---|
CN205965091U true CN205965091U (en) | 2017-02-22 |
Family
ID=58035866
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201620947385.7U Active CN205965091U (en) | 2016-08-26 | 2016-08-26 | Crystallization reaction kettle |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN205965091U (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109485073A (en) * | 2018-12-13 | 2019-03-19 | 余小海 | A kind of heavy alkali crystallization reactor |
CN113842859A (en) * | 2021-09-24 | 2021-12-28 | 枣阳市华新化工有限公司 | Modified silicone oil reation kettle |
-
2016
- 2016-08-26 CN CN201620947385.7U patent/CN205965091U/en active Active
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109485073A (en) * | 2018-12-13 | 2019-03-19 | 余小海 | A kind of heavy alkali crystallization reactor |
CN113842859A (en) * | 2021-09-24 | 2021-12-28 | 枣阳市华新化工有限公司 | Modified silicone oil reation kettle |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN205965091U (en) | Crystallization reaction kettle | |
CN104892389B (en) | Technique for preparing oxalic acid by performing continuous reaction rectification hydrolysis on dimethyl oxalate | |
CN103480175B (en) | Melting crystallizer | |
CN203540112U (en) | High-purity high-yield medicament recrystallization device | |
CN207552282U (en) | A kind of yellow wine fermentation tank | |
CN204275558U (en) | A kind of crystallization kettle | |
CN203212506U (en) | Efficient ethyl acetate reaction rectification device | |
CN201930569U (en) | Crystallizing tank | |
CN203501855U (en) | Multifunctional cooling tank | |
CN201488607U (en) | Cooling and crystallizing device adopting ammonia as raw material to produce ammonium salt | |
CN202786189U (en) | Reverse-flow system of middle rectification section | |
CN103467285A (en) | Method for reducing acidity of acetate | |
CN203342811U (en) | Reaction kettle provided with cooling coil pipe | |
CN217315782U (en) | Lead brass continuous casting crystallizer with water seal device | |
CN204017843U (en) | A kind of two switching reactors with inner coil pipe | |
CN204815762U (en) | Concentrated crystallizer of edible condiment | |
CN203653265U (en) | Kettle-type crystallizer for producing ammonium bifluoride | |
CN205973797U (en) | High -purity tellurium dioxide preparation facilities | |
CN203829687U (en) | Stirring device of crystallization kettle | |
CN217939177U (en) | Dealcoholization kettle for producing special plasticizer for automotive interiors | |
CN209033797U (en) | Produce sulfolane rectifier unit | |
CN207031452U (en) | A kind of vertical crystallizing tower stirring shaft sealer | |
CN204400975U (en) | Wine brewing condensing works | |
CN221332830U (en) | Crystallization tank for lactose production and processing | |
CN202063893U (en) | Complete equipment for cleaning crude methyl ester in production of biodiesel |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C14 | Grant of patent or utility model | ||
GR01 | Patent grant |