CN205965091U - Crystallization reaction kettle - Google Patents

Crystallization reaction kettle Download PDF

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Publication number
CN205965091U
CN205965091U CN201620947385.7U CN201620947385U CN205965091U CN 205965091 U CN205965091 U CN 205965091U CN 201620947385 U CN201620947385 U CN 201620947385U CN 205965091 U CN205965091 U CN 205965091U
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China
Prior art keywords
blade
inner tube
tube wall
conically shaped
shaped bottom
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Active
Application number
CN201620947385.7U
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Chinese (zh)
Inventor
项飞勇
吴尖平
王新伟
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Kente Catalysts Inc
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Kente Catalysts Inc
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Priority to CN201620947385.7U priority Critical patent/CN205965091U/en
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Abstract

The utility model discloses a crystallization reaction kettle, including a cauldron section of thick bamboo, a cauldron section of thick bamboo has cylindrical barrel and toper bobbin base, and cylindrical barrel and toper bobbin base have the double -layer barrel wall, double -layer barrel wall intermediate formation coolant liquid business turn over chamber, and its characterized in that: be equipped with the (mixing) shaft in the cauldron section of thick bamboo, the last axle head of (mixing) shaft expose in a cauldron section of thick bamboo and with gear motor's output shaft, the (mixing) shaft from top to bottom in proper order the installation be equipped with first, and secondly, the third, the fourth, the the 5th and the 6th paddle, it is first, and secondly, third and fourth paddle have the inner tube wall of outside blade surface corresponding circle cylindricality barrel respectively, it is first, and secondly, the regional inner tube wall that covers whole cylindrical barrel of scraping of third and fourth paddle, the the 5th and the 6th paddle has the inner tube wall that outside blade surface corresponds the toper bobbin base respectively, the regional inner tube wall that covers whole toper bobbin base of scraping of the 5th and the 6th paddle. The utility model discloses it is little that the dead angle is piled up in the crystallization, does benefit to crystallization speed and improve.

Description

Crystallization reaction kettle
Technical field
This utility model is related to a kind of reactor and in particular to a kind of tie for forcing in chemical products manufacturing process to cool down Brilliant crystallization reaction kettle.
Background technology
In chemical industry, the manufacturing process of such as tetrabutyl ammonium bromide, tetrabutyl ammonium bromide needs in crystallization reaction kettle Inside carry out compulsory crystallisation by cooling, crystallization reaction kettle has cylindrical tube and conically shaped bottom, cylindrical tube and conically shaped bottom There is double-deck barrel, double-deck barrel intermediate formation coolant passes in and out chamber, by the entrance of coolant to four in crystallization reaction kettle Butylammonium bromide carries out forcing cooling to be allowed to crystallize.But, the crystallization reaction kettle of prior art, the crystallization of kettle cylinder inwall is piled up Dead angle is many, and in crystallization process, crystalline solid can be attached to and can not strike off in time on barrel, and crystalline solid can block coolant and four fourths Conduction of heat between base ammonium bromide, therefore crystallization rate are slow.
Content of the invention
In view of the shortcomings of the prior art, the purpose of this utility model aims to provide a kind of crystallization little, profit of piling up dead angle The crystallization reaction kettle improving in crystallization rate.
This utility model adopts the following technical scheme that to complete:
Crystallization reaction kettle, including kettle cylinder, kettle cylinder has cylindrical tube and conically shaped bottom, cylindrical tube and conically shaped bottom There is double-deck barrel, double-deck barrel intermediate formation coolant turnover chamber it is characterised in that:It is provided with shaft, shaft in kettle cylinder Upper axle head expose to kettle cylinder and be connected with the output shaft of reducing motor, shaft installs successively up and down and is provided with first, second, the 3rd, the four, the 5th and the 6th blade, first, second, third and fourth blade is respectively provided with outer lobe face and corresponds to cylindrical tube Inner tube wall, the inner tube wall of the whole cylindrical tube of scraping region overlay of first, second, third and fourth blade, the 5th He 6th blade is respectively provided with the inner tube wall at the corresponding conically shaped bottom in outer lobe face, and the scraping region overlay of the 5th and the 6th blade is whole The inner tube wall at conically shaped bottom.
First, second, third, fourth and fifth blade is single-blade leaf, and the 6th blade is double blade.
The switching position at cylindrical tube and conically shaped bottom is provided with the 7th blade, and the 7th blade has outside narrow leaf face and corresponds to Cylindrical tube and the inner tube wall at conically shaped bottom switching position, and there is the upper table of the corresponding kettle cylinder internal thermometer pipe in bottom blade face Face, temperature gauge pipe laterally passes inside and outside kettle cylinder from the switching position at cylindrical tube and conically shaped bottom.
After technique scheme, this utility model is provided with shaft inside kettle cylinder and installs many on shaft Piece blade, the inner tube wall of the whole cylindrical tube of scraping region overlay of first, second, third and fourth blade, the 5th and The inner tube wall at the scraping region overlay whole conically shaped bottom of six blades, the scraping area of the 7th blade then covers cylindrical tube and cone The inner tube wall at shape cylinder bottom switching position and the upper surface of kettle cylinder internal thermometer pipe, thus realize crystallizing the minimum piling up dead angle Change, improve beneficial to crystallization rate.
Brief description
This utility model has drawings described below:
Fig. 1 is structural representation of the present utility model.
Specific embodiment
As illustrated, crystallization reaction kettle of the present utility model, including kettle cylinder 3, kettle cylinder 3 has cylindrical tube 4 and taper Cylinder bottom 7, cylindrical tube 4 and conically shaped bottom 7 have double-deck barrel, and double-deck barrel intermediate formation coolant passes in and out chamber 5, kettle cylinder 3 Inside it is provided with shaft 2, the upper axle head of shaft 2 exposes to kettle cylinder 3 and the output shaft with reducing motor 1 is connected, and shaft is about 2 Install successively and be provided with the first blade 11, the second blade 12, the 3rd blade 13, the 4th blade 14, the 5th blade 15 and the 6th blade 16, first, second, third and fourth blade is respectively provided with the inner tube wall of the corresponding cylindrical tube 4 in outer lobe face, and first and the 2nd, second and the three, the third and fourth blade have in the height direction overlapped, so can achieve first, second, third With the inner tube wall of the whole cylindrical tube of scraping region overlay 4 of the 4th blade, the 5th and the 6th blade is respectively provided with outer lobe The inner tube wall at the corresponding conically shaped bottom 7 in face, the 5th and the 6th blade has overlapped in the height direction, so can achieve the 5th With the inner tube wall at the scraping region overlay whole conically shaped bottom 7 of the 6th blade, first, second, third, fourth and fifth blade is Single-blade leaf, the 6th blade is double blade;The switching position at cylindrical tube 4 and conically shaped bottom 7 is provided with the 7th blade 17, the 7th oar Leaf 17 has the corresponding cylindrical tube 4 in outside narrow leaf face and the inner tube wall at conically shaped bottom 7 switching position, and has bottom blade face pair Answer the upper surface of kettle cylinder internal thermometer pipe 6, temperature gauge pipe 6 is horizontal from the switching position at cylindrical tube 4 and conically shaped bottom 7 Pass inside and outside kettle cylinder.

Claims (3)

1. crystallization reaction kettle, including kettle cylinder, kettle cylinder has cylindrical tube and conically shaped bottom, cylindrical tube and conically shaped bottom tool Have a double-deck barrel, double-deck barrel intermediate formation coolant turnover chamber it is characterised in that:It is provided with shaft in kettle cylinder, shaft Upper axle head is exposed to kettle cylinder and is connected with the output shaft of reducing motor, and shaft installs successively up and down and be provided with first, second, the 3rd, the four, the 5th and the 6th blade, first, second, third and fourth blade is respectively provided with outer lobe face and corresponds to cylindrical tube Inner tube wall, the inner tube wall of the whole cylindrical tube of scraping region overlay of first, second, third and fourth blade, the 5th He 6th blade is respectively provided with the inner tube wall at the corresponding conically shaped bottom in outer lobe face, and the scraping region overlay of the 5th and the 6th blade is whole The inner tube wall at conically shaped bottom.
2. crystallization reaction kettle as claimed in claim 1 it is characterised in that:First, second, third, fourth and fifth blade is Single-blade leaf, the 6th blade is double blade.
3. crystallization reaction kettle as claimed in claim 1 it is characterised in that:The switching position at cylindrical tube and conically shaped bottom sets There is the 7th blade, the 7th blade has the inner tube wall at the corresponding cylindrical tube in outside narrow leaf face and conically shaped bottom switching position, and There is the upper surface of the corresponding kettle cylinder internal thermometer pipe in bottom blade face, temperature gauge pipe is from the switching of cylindrical tube and conically shaped bottom Position laterally passes inside and outside kettle cylinder.
CN201620947385.7U 2016-08-26 2016-08-26 Crystallization reaction kettle Active CN205965091U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201620947385.7U CN205965091U (en) 2016-08-26 2016-08-26 Crystallization reaction kettle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201620947385.7U CN205965091U (en) 2016-08-26 2016-08-26 Crystallization reaction kettle

Publications (1)

Publication Number Publication Date
CN205965091U true CN205965091U (en) 2017-02-22

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201620947385.7U Active CN205965091U (en) 2016-08-26 2016-08-26 Crystallization reaction kettle

Country Status (1)

Country Link
CN (1) CN205965091U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109485073A (en) * 2018-12-13 2019-03-19 余小海 A kind of heavy alkali crystallization reactor
CN113842859A (en) * 2021-09-24 2021-12-28 枣阳市华新化工有限公司 Modified silicone oil reation kettle

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109485073A (en) * 2018-12-13 2019-03-19 余小海 A kind of heavy alkali crystallization reactor
CN113842859A (en) * 2021-09-24 2021-12-28 枣阳市华新化工有限公司 Modified silicone oil reation kettle

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