A kind of can serialization distillation, row residue distilling apparatus
Technical field
This utility model be related to a kind of can serialization distillation, row residue distilling apparatus, belong to chemical technology field.
Background technology
When being distilled with conventional distilling apparatus, the material that every batch materials distillation terminates in rear tower section cannot reclaim, meeting
Discharge with bottoms, and distillation column cannot work when discharging bottoms, amount of heat is discharged with bottoms,
This does not only result in work efficiency and reduces, and also results in the waste of material, heat.
Utility model content
The purpose of this utility model be to provide a kind of can serialization distillation, the distilling apparatus of row's residue, distillation and row residual
Slag is carried out simultaneously, substantially increases work efficiency, it is to avoid the waste of material and heat.
Described can serialization distillation, the distilling apparatus of row's residue, including distillating still, the top of described distillating still is provided with
Packed tower, it also includes the residue distillating still being connected with distillating still, the charging aperture phase of the discharging opening of distillating still and residue distillating still
Even, the gas outlet of residue distillating still is connected with the gas feed of distillating still, and gas outlet passes through attachment means with gas feed
It is connected, the bottom of residue distillating still is provided with residue discharging opening.
Described attachment means are gas phase connecting tube.
Described attachment means are to install packed tower section additional.
Compared with prior art the beneficial effects of the utility model are:
This utility model increases a residue distillating still on the basis of distillating still, when every batch materials distill close to terminal
When, bottoms are proceeded in residue distillating still using liquid level difference, using the temperature higher than distillating still, by bottoms
Material steams in distillating still again, and this utility model not only substantially increases work efficiency, and avoids material and heat
Waste moreover it is possible to ensure the stability of product content, considerably reduce production cost.
Brief description
Fig. 1 be described in the utility model can serialization distillation, row residue distilling apparatus schematic diagram;
In figure, 1, gas feed;2nd, packed tower;3rd, distillating still;4th, discharging opening;5th, charging aperture;6th, residue discharging opening;7th, residual
Slag distillating still;8th, gas outlet;9th, attachment means.
Specific embodiment
Below in conjunction with the accompanying drawings this utility model is described further.
As shown in figure 1, described can serialization distillation, the distilling apparatus of row's residue, including distillating still 3, described distillation
The top of kettle 3 is provided with packed tower 2, also includes the residue distillating still 7 being connected with distillating still 3, the discharging opening 4 of distillating still 3 and residue
The charging aperture 5 of distillating still 7 is connected, and the gas outlet 8 of residue distillating still 7 is connected with the gas feed 1 of distillating still 3, gas outlet 8
It is connected by attachment means 9 with gas feed 1, the bottom of residue distillating still 7 is provided with residue discharging opening 6.Attachment means 9 are gas phase
Connecting tube.
Attachment means 9 can also be to install packed tower section additional.
During work, when the bottoms in distillating still 3 are more, open discharging opening 4, by the bottoms in distillating still 3
It is transferred in residue distillating still 7 using liquid level difference, heating residue distillating still 7 to temperature is higher than distillating still 3, the material gas in residue
After change, distillating still 3 is again introduced into by attachment means 9 through gas feed 1 by gas outlet 8, material is through distillating still 3 distillation gas
Change and enter packed tower 2.Think no material when reaching uniform temperature attachment means 9 temperature drop in residue distillating still 7, you can close
Close gas outlet 8, allow residue distillating still 7 keep atmospheric pressure state, open residue discharging opening 6 and discharge residue, this process distillating still 3 is still
In normal work.