CN205914157U - Preparation glass reactor for silver powder - Google Patents
Preparation glass reactor for silver powder Download PDFInfo
- Publication number
- CN205914157U CN205914157U CN201620824791.4U CN201620824791U CN205914157U CN 205914157 U CN205914157 U CN 205914157U CN 201620824791 U CN201620824791 U CN 201620824791U CN 205914157 U CN205914157 U CN 205914157U
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- CN
- China
- Prior art keywords
- reaction kettle
- glass reaction
- kettle
- glass
- argentum powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Abstract
The utility model relates to a machining device especially relates to a preparation glass reactor for silver powder, including having the reation kettle that can dismantle the kettle cover, glass reactor presss from both sides the cover, agitating unit and high pressure nozzle, reation kettle includes at the bottom of glass cauldron body and the polytetrafluoroethylene cauldron, be equipped with the internal thread on the lateral wall of glass cauldron body, be equipped with the external screw thread with glass cauldron internal thread looks adaptation on one's body at the bottom of the polytetrafluoroethylene cauldron on the inside wall, glass reactor presss from both sides the ways and establishes the outside at reation kettle, be equipped with delivery port and water inlet on the glass reactor clamp cover outer wall, the bottom that glass reactor pressed from both sides the cover is equipped with the discharge gate, be equipped with first feed inlet and second feed inlet on the kettle cover, still be equipped with the high pressure nozzle who links to each other with the second feed inlet in the reation kettle, the utility model provides a preparation glass reactor for silver powder can prevent that side reaction and silver powder production efficiency are high.
Description
Technical field
This utility model is related to chemical field, and more particularly, to one kind prepares argentum powder glass reaction kettle.
Background technology
Argentum powder preparing device is to carry out most widely used argentum powder by additive methods such as liquid phase reductions or electrolysis
The preparation facilitiess of volume production, are mainly used in chemical industry and manufacture field；The simple process preparing argentum powder in prior art typically adopts
The preparation method quickly being stirred in clear glass instrument, because the smooth surface of glass apparatus is smooth, therefore would generally go out
Lose face mirror reaction by-product, reduce the yield of argentum powder, also increase production cost.
Utility model content
For solving above-mentioned technical problem, the purpose of this utility model is to provide one kind can prevent side reaction and argentum powder produces
Efficiency high prepare argentum powder glass reaction kettle.
Of the present utility model prepare argentum powder glass reaction kettle, including the reactor with detachable kettle cover, glass reaction
Kettle chuck, agitating device and high-pressure nozzle, described reactor includes glass kettle body and politef bottom, described glass kettle body
Lateral wall be provided with female thread, described politef bottom medial wall is provided with and the female thread phase with described glass kettle
The external screw thread of adaptation, described glass reaction kettle chuck is set in the outside of described reactor, described glass reaction kettle jackets outer wall
It is provided with outlet and water inlet, the bottom of described glass reaction kettle chuck is provided with discharging opening, and described kettle cover is provided with first and enters
Material mouth and second charging aperture, are additionally provided with the described high-pressure nozzle being connected with described second charging aperture in described reactor.
Further, switch valve, high-pressure pump and connecting tube, one end of described connecting tube and described high-pressure pump phase are also included
Even, the other end of described connecting tube is connected through described second charging aperture with described high-pressure nozzle, and described switch valve is arranged on institute
State in the described connecting tube between high-pressure nozzle and high-pressure pump.
Further, described high-pressure nozzle is set to high-pressure rotary shower nozzle, described high-pressure rotary shower nozzle include revolving part with
And the shower nozzle being connected with described revolving part.
Further, described agitating device includes shaft and the turbine type stirring paddle being arranged on shaft.
Further, also include the acidometer that is plugged on described kettle cover.
Further, also include automatic discharging valve, it is anti-that the bottom of described glass reaction kettle chuck is provided through described glass
Answer kettle chuck and the described automatic discharging valve being connected with described politef bottom.
Specifically, described automatic discharging valve is set to polytetrafluoro valve.
By such scheme, this utility model at least has the advantage that to prevent side reaction from avoiding unnecessary damage
Lose, one kind that this utility model provides is prepared argentum powder glass reaction kettle and enabled to prevent silver mirror side reaction, thus greatly improving
The production efficiency of argentum powder.
Described above is only the general introduction of technical solutions of the utility model, in order to better understand skill of the present utility model
Art means, and being practiced according to the content of description, below with preferred embodiment of the present utility model and coordinate accompanying drawing detailed
Describe in detail bright as after.
Brief description
Fig. 1 is the front view preparing argentum powder glass reaction kettle that this utility model provides.
Specific embodiment
With reference to the accompanying drawings and examples, specific embodiment of the present utility model is described in further detail.Below
Embodiment is used for this utility model is described, but is not limited to scope of the present utility model.
Referring to Fig. 1, one kind of this utility model one preferred embodiment prepares argentum powder glass reaction kettle, including with removable
Unload reactor 2, glass reaction kettle chuck 3, agitating device 4 and the high-pressure nozzle 5 of kettle cover 1, reactor 2 includes glass kettle body 6 He
Politef bottom 7, the lateral wall of glass kettle body 6 is provided with female thread, and politef bottom 7 medial wall is provided with and glass
The external screw thread that female thread in glass kettle body 6 is adapted, glass reaction kettle chuck 3 is set in the outside of reactor 2, glass reaction kettle
Chuck 3 outer wall is provided with outlet 8 and water inlet 9, and the bottom of glass reaction kettle chuck 3 is provided with discharging opening 10, and kettle cover 1 is provided with
First charging aperture 11 and second charging aperture 12, are additionally provided with the high-pressure nozzle 5 being connected with second charging aperture 12 in reactor 2.
The operation principle that this utility model prepares argentum powder glass reaction kettle is:
The reactor 2 prepared in argentum powder glass reaction kettle that this utility model provides includes glass kettle body 6 and polytetrafluoro
Ethylene bottom 7, so both can observe the progress of argentum powder preparation in kettle through glass kettle body 6 and glass reaction kettle chuck 3,
The preparation that argentum powder can also be carried out in politef bottom 7 is thus prevent the generation of silver mirror reaction；Can open by reactor 2
The first charging aperture on kettle cover 1 closed adds reactant liquor in reactor 2, is provided with agitating device 4, can promote silver in reactor
Reduction reaction is more rapid and thorough, by second charging aperture, washing can be added molten after the completion of the preparation of argentum powder is reacted
Liquid, and sprayed in high-pressure nozzle 5 is to reactor 2 and clean, wash solution includes hot nitric acid, 10% naoh solution
And distilled water.
In order to preferably control the cleaning device in reactor 2, prepare argentum powder glass reaction kettle also include switch valve 13,
High-pressure pump and connecting tube 14, one end of connecting tube 14 is connected with high-pressure pump, and the other end of connecting tube 14 passes through second charging aperture
12 are connected with high-pressure nozzle 5, and switch valve 13 is arranged in the connecting tube 14 between high-pressure nozzle 5 and high-pressure pump.
In order to the reactor politef bottom 7 in reactor 2 is carried out with 360 degree of sprinkling and flushing, high-pressure nozzle 5
It is set to high-pressure rotary shower nozzle, high-pressure rotary shower nozzle includes revolving part 15 and the shower nozzle being connected with revolving part 15；As such, it is possible to
Reaction residue in reactor 2 is carried out with the thoroughly clean operation at no dead angle, facilitates the carrying out of next group argentum powder preparation reaction.
Stage in order to carry out to argentum powder preparation reaction in reactor 2 is sufficiently grasped, and also includes being plugged on kettle cover 1
Acidometer 16；As such, it is possible to pass through argentum powder in acidometer 16 solution reaction kettle 2 to prepare the soda acid degree of reaction or to reaction
Carry out cleanliness factor detection after the completion of the process that kettle 2 is rinsed.
Carry out discharging in reactor 2 for convenience, also include automatic discharging valve 17, the bottom of glass reaction kettle chuck sets
The automatic discharging valve 17 having through glass reaction kettle chuck and being connected with politef bottom, automatic discharging valve 17 is set to gather
Tetrafluoro valve.
The above is only preferred implementation of the present utility model, be not limited to this utility model it is noted that for
For those skilled in the art, on the premise of without departing from this utility model know-why, if can also make
Dry improvement and modification, these improve and modification also should be regarded as protection domain of the present utility model.
Claims (7)
1. one kind prepare argentum powder glass reaction kettle it is characterised in that: include reactor with detachable kettle cover, glass reaction
Kettle chuck, agitating device and high-pressure nozzle, described reactor includes glass kettle body and politef bottom, described glass kettle body
Lateral wall be provided with female thread, described politef bottom medial wall is provided with and the female thread phase with described glass kettle
The external screw thread of adaptation, described glass reaction kettle chuck is set in the outside of described reactor, described glass reaction kettle jackets outer wall
It is provided with outlet and water inlet, the bottom of described glass reaction kettle chuck is provided with discharging opening, and described kettle cover is provided with first and enters
Material mouth and second charging aperture, are additionally provided with the described high-pressure nozzle being connected with described second charging aperture in described reactor.
2. according to claim 1 prepare argentum powder glass reaction kettle it is characterised in that: also include switch valve, high-pressure pump
And connecting tube, one end of described connecting tube is connected with described high-pressure pump, and the other end of described connecting tube enters through described second
Material mouth is connected with described high-pressure nozzle, and described switch valve is arranged on the described connecting tube between described high-pressure nozzle and high-pressure pump
On.
3. according to claim 1 prepare argentum powder glass reaction kettle it is characterised in that: described high-pressure nozzle is set to height
Pressure rotary nozzle, described high-pressure rotary shower nozzle includes revolving part and the shower nozzle being connected with described revolving part.
4. according to claim 1 prepare argentum powder glass reaction kettle it is characterised in that: described agitating device include stir
Axle and the turbine type stirring paddle being arranged on shaft.
5. according to claim 1 prepare argentum powder glass reaction kettle it is characterised in that: also include being plugged in described kettle cover
On acidometer.
6. according to claim 1 prepare argentum powder glass reaction kettle it is characterised in that: also include automatic discharging valve, institute
The bottom stating glass reaction kettle chuck is provided through described glass reaction kettle chuck and is connected with described politef bottom
Described automatic discharging valve.
7. according to claim 6 prepare argentum powder glass reaction kettle it is characterised in that: described automatic discharging valve is set to gather
Tetrafluoro valve.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620824791.4U CN205914157U (en) | 2016-08-02 | 2016-08-02 | Preparation glass reactor for silver powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620824791.4U CN205914157U (en) | 2016-08-02 | 2016-08-02 | Preparation glass reactor for silver powder |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205914157U true CN205914157U (en) | 2017-02-01 |
Family
ID=57870046
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620824791.4U Active CN205914157U (en) | 2016-08-02 | 2016-08-02 | Preparation glass reactor for silver powder |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205914157U (en) |
-
2016
- 2016-08-02 CN CN201620824791.4U patent/CN205914157U/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |