CN205874517U - Produce device of magnesium chloride in vacuum mode emission titanium sponge production process - Google Patents
Produce device of magnesium chloride in vacuum mode emission titanium sponge production process Download PDFInfo
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- CN205874517U CN205874517U CN201620894934.9U CN201620894934U CN205874517U CN 205874517 U CN205874517 U CN 205874517U CN 201620894934 U CN201620894934 U CN 201620894934U CN 205874517 U CN205874517 U CN 205874517U
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- magnesium chloride
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- chloride pipe
- titanium sponge
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Abstract
The utility model relates to a produce device of magnesium chloride in vacuum mode emission titanium sponge production process belongs to titanium sponge production technical field. Technical scheme is: be equipped with vacuum pressure meter (3) on vacuum ladle (1), vacuum ladle (1) hangs on gib head balance (2), the one end and the vacuum ladle intercommunication of magnesium chloride pipe (4), the other end pass through flange (12) and two (13) intercommunications of magnesium chloride pipe, magnesium chloride pipe two insertion reaction ware (9) bottom, the one end of flexible coupling (8) is connected with vacuum ladle, and the other end passes through quick -operation joint two (6) to be connected with the first end of three -dimensional valve (7), and vacuum pipeline (11) is connected to the second end of three -dimensional valve. The utility model discloses simple preparation, practicality do not influence production, have promoted the quality of product, reduce the destructiveness of aggressive fume to surrounding environment and equipment, do not stop and expect production, improved the utilization ratio of reducing furnace, improved the stove productivity, reduce argon gas, titanium tetrachloride unit consumption and production power consumption.
Description
Technical field
This utility model produces the device of magnesium chloride during relating to a kind of vacuum mode discharge titanium sponge production, belong to sea
Continuous titanium production technical field.
Background technology
At present, in titanium sponge reduction reacts production process, reactor, generate titanium sponge and the magnesium chloride of liquid of solid-state,
Needing repeatedly to discharge the magnesium chloride produced, vacating space, to guarantee being normally carried out of titanium sponge production.Use owing to producing
The difference of reduction furnace structure, generally has two kinds of discharging modes: upper row's magnesium chloride mode therein is dependent on gas pressure will reaction
Magnesium Chloride Melt bottom device, is discharged by being inserted into the magnesium chloride pipe of reactor；Lower row's magnesium chloride mode is then
Rely on Magnesium Chloride Melt self gravitation and reactor pressure, by tail pipe and a set of taper control valve device of reactor bottom
It is discharged.In discharge process, above two mode all can have magnesium chloride gas to produce pollution surrounding, and corrosion produces
Facility；Upper row's mode there is also stifled charge pipe, needs to stop material or the problem of fall material speed, to consume substantial amounts of argon simultaneously；Lower row
Mode operates complexity, it is desirable to have a set of special taper control valve device, there is also cone valve fault and causes Magnesium Chloride Melt to run leakage
Problem.
Utility model content
This utility model purpose produces the device of magnesium chloride during being to provide a kind of vacuum mode discharge titanium sponge production,
Method is easy, practical, does not affect production, not only has greatly improved the quality of product, moreover it is possible to discharge process is greatly lowered
The corrosive gas of middle generation is to surrounding and the destructiveness of equipment；Do not stop material to produce, improve the utilization of reduction furnace
Rate, improves stove production capacity, reduces argon, titanium tetrachloride unit consumption and produces power consumption, solving the problems referred to above that background technology exists.
The technical solution of the utility model is:
Produce the device of magnesium chloride during a kind of vacuum mode discharge titanium sponge production, comprise vacuum ladle, scale with hook head,
Pressure vacuum gauge, magnesium chloride pipe one, snap joint one, snap joint two, three-dimensional valve, be flexible coupling, adpting flange, magnesium chloride pipe
Two, vacuum ladle is provided with pressure vacuum gauge, and vacuum ladle is suspended on scale with hook head；One end of magnesium chloride pipe one and vacuum ladle
Connection, the other end is connected with magnesium chloride pipe two, bottom magnesium chloride pipe two insertion reaction device by adpting flange；The one end being flexible coupling
Being connected with vacuum ladle by snap joint one, the other end is connected with the first end of three-dimensional valve by snap joint two, three-dimensional
Second end of valve connects vacuum pipeline, the 3rd end connection air of three-dimensional valve.
Described reactor is arranged in reduction furnace.
Three-dimensional valve on vacuum pipeline is forwarded to the direction communicated with vacuum pipeline, namely the first end of three-dimensional valve
Connecting with the second end, implement vacuum ladle evacuation, due to suction function, the magnesium chloride solution in reactor passes through magnesium chloride
Pipe two and magnesium chloride pipe one enter vacuum ladle；Observe the change of data on scale with hook head, when magnesium chloride solution in vacuum ladle
When weight reaches predetermined weight to, three-dimensional valve is forwarded the direction communicated with air, namely first end and of three-dimensional valve
Three end connections, implement, to the destruction of vacuum state in vacuum ladle, to discharge the operation of magnesium chloride before terminating reduction furnace.
The predetermined weight of magnesium chloride solution in described vacuum ladle, calculates according to the weight putting into raw material to reactor and produces
The weight of raw magnesium chloride solution, this weight is predetermined weight.According to putting into material quantity and reduction furnace parameter, calculate generation magnesium molten
The predetermined weight of liquid, is the basic skill of those of ordinary skill in the art, is public.
After discharging magnesium chloride operation before terminating reduction furnace, take the magnesium chloride pipe two being connected with vacuum ladle apart and be flexible coupling,
The vacuum ladle that will be equipped with Magnesium Chloride Melt transports to the magnesium chloride discharge sites of smoke extractor, and Magnesium Chloride Melt is discharged into chlorine
Change in magnesium groove；Vacuum ladle continues discharge magnesium chloride operation next time.
If vacuum ladle capacity is sufficiently large, after discharging magnesium chloride operation before terminating reduction furnace, transport to next reduction furnace
Before, again carry out the operation of stokehold discharge magnesium chloride.
If there being magnesium eletrolysis corollary equipment, vacuum ladle is transported to magnesium electrolysis workshop and is directly discharged in closing down magnesium electrolysis bath.
This utility model good effect: the particularly suitable row's of taking mode produces the production of titanium sponge, method is easy, real
With, do not affect production, not only the quality of product is had greatly improved, moreover it is possible to the corrosion that produce is greatly lowered in discharge process
Property gas is to surrounding and the destructiveness of equipment；Do not stop material to produce, improve the utilization rate of reduction furnace, improve stove and produce
Can, reduce argon, titanium tetrachloride unit consumption and produce power consumption.
Accompanying drawing explanation
Fig. 1 is this utility model embodiment schematic diagram；
In figure: vacuum ladle 1, scale with hook head 2, pressure vacuum gauge 3, magnesium chloride pipe 1, snap joint 1, snap joint two
6, three-dimensional valve 7, be flexible coupling 8, reactor 9, reduction furnace 10, vacuum pipeline 11, adpting flange 12, magnesium chloride pipe 2 13.
Detailed description of the invention
Produce the device of magnesium chloride during a kind of vacuum mode discharge titanium sponge production, comprise vacuum ladle 1, scale with hook head
2, pressure vacuum gauge 3, magnesium chloride pipe 1, snap joint 1, snap joint 26, three-dimensional valve 7, be flexible coupling 8, adpting flange
12, magnesium chloride pipe 2 13, vacuum ladle 1 is provided with pressure vacuum gauge 3, and vacuum ladle 1 is suspended on scale with hook head 2；Magnesium chloride pipe
One end of one 4 connects with vacuum ladle 1, and the other end is connected with magnesium chloride pipe 2 13 by adpting flange 12, magnesium chloride pipe 2 13
Bottom insertion reaction device 9；Be flexible coupling 8 one end be connected with vacuum ladle 1 by snap joint 1, the other end passes through quickly to connect
26 are connected with the first end of three-dimensional valve 7, and the second end of three-dimensional valve 7 connects vacuum pipeline 11, the 3rd of three-dimensional valve 7
End connection air.
Described reactor 9 is arranged in reduction furnace 10.
Three-dimensional valve 7 on vacuum pipeline 11 is forwarded to the direction communicated with vacuum pipeline, namely the of three-dimensional valve 7
One end connects with the second end, implements vacuum ladle 1 evacuation, and due to suction function, the magnesium chloride solution in reactor passes through
Magnesium chloride pipe 2 13 and magnesium chloride pipe 1 enter vacuum ladle 1；Observe the change of data on scale with hook head, when chlorine in vacuum ladle 1
When the weight of change magnesium solution reaches predetermined weight to, three-dimensional valve 7 is forwarded the direction communicated with air, namely three-dimensional valve 7
The first end and the connection of the 3rd end, implement the destruction of vacuum state in vacuum ladle 1, before terminating reduction furnace, discharge magnesium chloride
Operation.
The predetermined weight of magnesium chloride solution in described vacuum ladle 1, the weight according to putting into raw material to reactor calculates
Producing the weight of magnesium chloride solution, this weight is predetermined weight.In the present embodiment, put into 1 ton of raw material to reactor, it is contemplated that produce
Raw 800 kilograms of magnesium chloride solutions.
After discharging magnesium chloride operation before terminating reduction furnace, take the magnesium chloride pipe 2 13 and soft company being connected with vacuum ladle 1 apart
Connecing 8, the vacuum ladle 1 that will be equipped with Magnesium Chloride Melt transports to the magnesium chloride discharge sites of smoke extractor, is arranged by Magnesium Chloride Melt
It is put in magnesium chloride groove；Vacuum ladle 1 continues to discharge magnesium chloride operation next time.
If vacuum ladle 1 capacity is sufficiently large, after discharging magnesium chloride operation before terminating reduction furnace, transport to next reduction furnace
Before, again carry out the operation of stokehold discharge magnesium chloride.
If there being magnesium eletrolysis corollary equipment, vacuum ladle 1 is transported to magnesium electrolysis workshop and is directly discharged in closing down magnesium electrolysis bath.
Claims (2)
1. during a vacuum mode discharge titanium sponge production, produce the device of magnesium chloride, it is characterised in that: comprise vacuum and lift
Bag (1), scale with hook head (2), pressure vacuum gauge (3), magnesium chloride pipe one (4), snap joint one (5), snap joint two (6), three-dimensional
Valve (7), be flexible coupling (8), adpting flange (12), magnesium chloride pipe two (13), vacuum ladle (1) is provided with pressure vacuum gauge (3),
Vacuum ladle (1) is suspended on scale with hook head (2)；One end of magnesium chloride pipe one (4) connects with vacuum ladle (1), and the other end passes through
Adpting flange (12) connects with magnesium chloride pipe two (13), magnesium chloride pipe two (13) insertion reaction device (9) bottom；Be flexible coupling (8)
One end is connected with vacuum ladle (1) by snap joint one (5), and the other end is by snap joint two (6) and three-dimensional valve (7)
First end connects, and the second end of three-dimensional valve (7) connects vacuum pipeline (11), the 3rd end connection air of three-dimensional valve (7).
The device of magnesium chloride, its feature is produced during vacuum mode the most according to claim 1 discharge titanium sponge production
It is: described reactor (9) is arranged in reduction furnace (10).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620894934.9U CN205874517U (en) | 2016-08-18 | 2016-08-18 | Produce device of magnesium chloride in vacuum mode emission titanium sponge production process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620894934.9U CN205874517U (en) | 2016-08-18 | 2016-08-18 | Produce device of magnesium chloride in vacuum mode emission titanium sponge production process |
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| Publication Number | Publication Date |
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| CN205874517U true CN205874517U (en) | 2017-01-11 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201620894934.9U Active CN205874517U (en) | 2016-08-18 | 2016-08-18 | Produce device of magnesium chloride in vacuum mode emission titanium sponge production process |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106048258A (en) * | 2016-08-18 | 2016-10-26 | 中航天赫（唐山）钛业有限公司 | Method and device for generating magnesium chloride in titanium sponge production process through vacuum discharging manner |
| CN109971979A (en) * | 2019-03-20 | 2019-07-05 | 洛阳双瑞万基钛业有限公司 | A kind of liner of two-maing ladle for titanium sponge production |
| CN114317966A (en) * | 2022-01-14 | 2022-04-12 | 新疆湘晟新材料科技有限公司 | Arrangement method of reduction distillation device and magnesium electrolytic cell device for titanium sponge production |
-
2016
- 2016-08-18 CN CN201620894934.9U patent/CN205874517U/en active Active
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106048258A (en) * | 2016-08-18 | 2016-10-26 | 中航天赫（唐山）钛业有限公司 | Method and device for generating magnesium chloride in titanium sponge production process through vacuum discharging manner |
| CN106048258B (en) * | 2016-08-18 | 2018-04-10 | 中航天赫（唐山）钛业有限公司 | The method and device of magnesium chloride is produced during vacuum mode discharge titanium sponge production |
| CN109971979A (en) * | 2019-03-20 | 2019-07-05 | 洛阳双瑞万基钛业有限公司 | A kind of liner of two-maing ladle for titanium sponge production |
| CN109971979B (en) * | 2019-03-20 | 2024-03-01 | 洛阳双瑞万基钛业有限公司 | Ladle liner for producing titanium sponge |
| CN114317966A (en) * | 2022-01-14 | 2022-04-12 | 新疆湘晟新材料科技有限公司 | Arrangement method of reduction distillation device and magnesium electrolytic cell device for titanium sponge production |
| CN114317966B (en) * | 2022-01-14 | 2023-08-18 | 新疆湘晟新材料科技有限公司 | Arrangement method of reduction distillation device and magnesium electrolytic tank device for producing titanium sponge |
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