CN205856569U - A kind of high purity metal calcium stagewise retort - Google Patents
A kind of high purity metal calcium stagewise retort Download PDFInfo
- Publication number
- CN205856569U CN205856569U CN201620887939.9U CN201620887939U CN205856569U CN 205856569 U CN205856569 U CN 205856569U CN 201620887939 U CN201620887939 U CN 201620887939U CN 205856569 U CN205856569 U CN 205856569U
- Authority
- CN
- China
- Prior art keywords
- retort
- connecting cylinder
- curved slab
- stagewise
- high purity
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Manufacture And Refinement Of Metals (AREA)
- Muffle Furnaces And Rotary Kilns (AREA)
Abstract
This utility model belongs to calcium metal purification technique field, discloses a kind of high purity metal calcium stagewise retort, causes, in the through hole and lower surface of cold plate, the problem that purity is low for solving existing retort due to impurities left.This utility model includes heating furnace, described heating furnace is placed with retort, the inner bottom part of described retort is provided with the crucible for placing material, the epimere of described retort is provided with for removing vacuum line with external vacuum system is connected, the top of described retort connects bell body, described bell body includes bell body, the lower surface of described bell body connects the connecting cylinder having cylindrically, described connecting cylinder extend in retort, the lower end of described connecting cylinder is hinged with curved slab, it is provided with for driving curved slab to carry out rotational drive motor on the outer wall of described connecting cylinder, in described curved slab, cold plate is installed.
Description
Technical field
This utility model belongs to calcium metal purification technique field, is specifically related to a kind of high purity metal calcium stagewise distillation
Stove.
Background technology
In numerous high-purity rare metal preparations, high-purity calcium is as preferable reducing agent, and its purity directly affects
The purity of products obtained therefrom, and then affect its final utilization performance.During particularly prepared by the production at some material, high-purity calcium is more
It is that there is indispensable status.In prior art, the technical literature about retort is the most more, such as Application No.
The patent of invention of 201410001261.5 discloses a kind of high-purity calcium vacuum distillation purification device and method thereof, and this device includes adding
Distillation reaction tank in hot stove, heating furnace, the crucible being placed on distillation reaction pot bottom and crucible cover with holes, thick calcium is positioned over
In crucible, distillation reaction tank upper end arranges the vacuum line that goes in order to connect vacuum system, and cross sectional shape is for falling " convex " shape
Retort bell, bell top arranges water collar, and the convex surface lower end of bell is provided with cold plate, and it is convex that cold plate is exposed at bell
Some apertures it are uniformly distributed on outer outside lower end, face；Heating furnace is to use resistance wire indirectly to heat, have heat insulation function
Two sections of heating furnaces；Vacuum system is made up of two stage pump, and primary pump is rotary vane mechanical pump, and two stage pump is oil diffusion pump；Cold plate
Outer be uniformly distributed aperture, small aperture be not less than 10mm, little hole number be not less than 16；It is uniformly distributed little on crucible cover
Hole, small aperture is not less than 10mm, and little hole number is not less than 20；Between distillation reaction tank and retort bell, sealing is set
Circle.
This device compare before retort, although can improve the purity of calcium metal, but in use, due to
Low boiling, high saturated vapor pressure impurity are condensate at bell lower surface after the aperture of cold plate, and the condensation of last calcium metal is cold
Coagulating on cold plate, the design of this structure makes still can residual part on the aperture hole wall of cold plate and the lower surface of cold plate
Divide impurity, cause calcium metal purity the highest, have impact on the further lifting of calcium metal purity.
Utility model content
This utility model is led due to impurities left to solve existing retort in the through hole and lower surface of cold plate
Cause the problem that purity is low, and a kind of high purity metal calcium stagewise retort is provided.
For solving above-mentioned technical problem, this utility model be the technical scheme is that
A kind of high purity metal calcium stagewise retort, including heating furnace, is placed with retort in described heating furnace, described
The inner bottom part of retort is provided with the crucible for placing material, the epimere of described retort be provided with for external vacuum system
What system connected removes vacuum line, and the top of described retort connects bell body, it is characterised in that described bell body includes bell
Body, the lower surface of described bell body connects the connecting cylinder having cylindrically, and described connecting cylinder extend in retort, described connection
The lower end of cylinder is hinged with curved slab, the outer wall of described connecting cylinder is provided with for driving curved slab to carry out rotating driving electric
Machine, is provided with cold plate in described curved slab.
Further, described curved slab includes shell body and inner housing, and described inner housing is sheathed the most also
Form the cooling cavity sealed.
Further, the both sides of described curved slab are connected on connecting cylinder through hollow rotating shaft, and described hollow rotating shaft with
Cooling cavity connection, described connecting cylinder is arranged with the bearing block for installing hollow rotating shaft.
Further, described hollow rotating shaft one end is through bearing block and is arranged with annular sleeve, described annular sleeve and hollow turn
Being provided with sealing ring between axle, described annular sleeve connects with outside water source through pipeline.
Further, the outer circle wall of described hollow rotating shaft being provided with gear ring, the output shaft of described driving motor connects
There is driving gear intermeshing with gear ring.
Further, described heating furnace is provided with first paragraph heater strip spaced apart from each other and second segment heater strip.
Further, the upper end of described crucible is provided with crucible cover, and described crucible cover offers through hole.
Compared with prior art, this utility model has the advantages that
High purity metal calcium stagewise retort of the present utility model, during pre-distillation, low boiling, high saturated steaming
Vapour pressure impurity, under the guide functions of curved slab, rises to the lower surface of bell along curved slab；During distillation, driving
Under the induced effect of galvanic electricity machine, curved slab rotates so that the calcium metal of politics and law condenses on cold plate.During whole, cold
Solidifying plate is all not exposed to low boiling, high saturated vapor pressure impurity, therefore, it is possible to improve the purity of calcium metal.
This utility model in use, even if low boiling, high saturated vapor pressure impurity from curved slab and connecting cylinder it
Between space through can always rise condense on the lower surface of bell, therefore also will not touch cold under the effect of curved slab
Solidifying plate, therefore, this utility model can improve the purity of calcium metal.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model；
Fig. 2 is the connecting cylinder in bell body of the present utility model and curved slab attachment structure schematic diagram；
Labelling in figure: 1, heating furnace, 2, retort, 3, crucible, 4, bell body, 5, remove vacuum line, 6, first paragraph heating
Silk, 7, second segment heater strip, 8, crucible cover, 41, bell, 42, connecting cylinder, 43, inner housing, 44, shell body, 45, cooling cavity,
46, bearing block, 47, hollow rotating shaft, 48, gear ring, 49, driving gear, 410, drive motor, 411, annular sleeve, 412, cold plate.
Detailed description of the invention
Below in conjunction with embodiment, the utility model will be further described, and described embodiment is only that this practicality is new
The a part of embodiment of type, is not whole embodiments.Based on the embodiment in this utility model, the ordinary skill people of this area
Member obtained under not making creative work premise other used by embodiment, broadly fall into protection model of the present utility model
Enclose.
In conjunction with accompanying drawing, high purity metal calcium stagewise retort of the present utility model includes heating furnace 1, described heating furnace 1
In be placed with retort 2, the inner bottom part of described retort 2 is provided with the crucible 3 for placing material, described retort 2 upper
Section is provided with removes vacuum line 5 for be connected with external vacuum system, goes vacuum management 5 to connect with outside vacuum system,
For in use to carrying out in retort 2 being dehydrated degassing processing, the top of described retort 2 connects bell body 4, institute
State bell body and include bell body 41, accelerate low boiling, high saturated vapor pressure impurity for the ease of in use carrying out cooling
Condensation, the upper end of bell body 41 is also equipped with cooling recirculation system, and wherein cooling recirculation system belongs to prior art products, this
The technical staff in field can be appreciated and understood that, does not repeats them here.The lower surface of described bell body 41 connects to be had cylindrically
Connecting cylinder 42, described connecting cylinder 42 extend in retort 2, and the lower end of described connecting cylinder 42 is hinged with curved slab, described company
Connect and be provided with on the outer wall of cylinder 42 for driving curved slab to carry out rotational drive motor 410, be provided with in described curved slab
Cold plate 412.
Further, described curved slab includes that shell body 44 and inner housing 43, described inner housing 43 are set in shell body 44
Inside and form the cooling cavity 45 of sealing, the both sides of described curved slab are connected on connecting cylinder through hollow rotating shaft, and institute
State hollow rotating shaft 47 to connect with cooling cavity 45, described connecting cylinder 42 is arranged with the bearing block for installing hollow rotating shaft 47
46, wherein the hollow rotating shaft of curved slab both sides is respectively as water inlet pipe and outlet pipe, cools down for curved slab, thus accelerates
The cooling of cold plate 412, improves the condensation time of calcium metal.
Further, described hollow rotating shaft 47 one end is through bearing block 46 and is arranged with annular sleeve 411, i other words, hollow
Rotating shaft one end connects with cooling cavity 45, and the other end connects with annular sleeve, arranges between described annular sleeve 411 and hollow rotating shaft 47
Having sealing ring, described annular sleeve 411 connects with outside water source through pipeline, ensure that hollow rotating shaft 47 by arranging annular sleeve
Normal rotation in the case of can be by cooling liquid in cooling cavity, and the design of sealing ring, enabling current
Overflow between hollow rotating shaft and annular sleeve.
As a kind of preferably mode of this utility model, the outer circle wall of described hollow rotating shaft 47 is provided with gear ring 48,
The output shaft of described driving motor 510 connects driving gear 49 intermeshing with gear ring 48.Wherein, in order to prevent evaporation
Metal condensation is to gear ring, driving gear and driving motor, as a kind of preferably mode of this utility model, drives motor, actively
The periphery of gear and gear ring is coated with sealing cover body, improves practicality of the present utility model.
Further, described heating furnace 1 is provided with first paragraph heater strip 6 spaced apart from each other and second segment heater strip 7, passes through
First paragraph heating wire and second segment are set and accelerate silk, it is simple to the technique controlling distillation, thus ensure in different phase different
Temperature.
Further, the upper end of described crucible 2 is provided with crucible cover 8, and described crucible cover 8 offers through hole, it is simple to fall
The evaporation rate of low metal, it is ensured that being smoothed out of distillation.
Embodiment one
The high purity metal calcium stagewise retort of the present embodiment, including heating furnace, is placed with reaction in described heating furnace
Tank, the inner bottom part of described retort is provided with the crucible for placing material, and the epimere of described retort is provided with for outward
What portion's vacuum system connected removes vacuum line, and the top of described retort connects has bell body, described bell body to include bell body,
The lower surface of described bell body connects the connecting cylinder having cylindrically, and described connecting cylinder extend in retort, described connecting cylinder
Lower end be hinged with curved slab, the outer wall of described connecting cylinder is provided with for drive curved slab carry out rotate drive electricity
Machine, is provided with cold plate in described curved slab.
Embodiment two
The high purity metal calcium stagewise retort of the present embodiment, including heating furnace, is placed with reaction in described heating furnace
Tank, the inner bottom part of described retort is provided with the crucible for placing material, and the epimere of described retort is provided with for outward
What portion's vacuum system connected removes vacuum line, and the top of described retort connects has bell body, described bell body to include bell body,
The lower surface of described bell body connects the connecting cylinder having cylindrically, and described connecting cylinder extend in retort, described connecting cylinder
Lower end be hinged with curved slab, the outer wall of described connecting cylinder is provided with for drive curved slab carry out rotate drive electricity
Machine, is provided with cold plate in described curved slab；Described curved slab includes that shell body and inner housing, described inner housing are set in shell
The inside of body also forms the cooling cavity of sealing.
Embodiment three
The high purity metal calcium stagewise retort of the present embodiment, including heating furnace, is placed with reaction in described heating furnace
Tank, the inner bottom part of described retort is provided with the crucible for placing material, and the epimere of described retort is provided with for outward
What portion's vacuum system connected removes vacuum line, and the top of described retort connects has bell body, described bell body to include bell body,
The lower surface of described bell body connects the connecting cylinder having cylindrically, and described connecting cylinder extend in retort, described connecting cylinder
Lower end be hinged with curved slab, the outer wall of described connecting cylinder is provided with for drive curved slab carry out rotate drive electricity
Machine, is provided with cold plate in described curved slab；Described curved slab includes that shell body and inner housing, described inner housing are set in shell
The inside of body also forms the cooling cavity of sealing；The both sides of described curved slab are connected on connecting cylinder through hollow rotating shaft, and institute
State hollow rotating shaft to connect with cooling cavity, described connecting cylinder is arranged with the bearing block for installing hollow rotating shaft.
Embodiment four
The high purity metal calcium stagewise retort of the present embodiment, including heating furnace, is placed with reaction in described heating furnace
Tank, the inner bottom part of described retort is provided with the crucible for placing material, and the epimere of described retort is provided with for outward
What portion's vacuum system connected removes vacuum line, and the top of described retort connects has bell body, described bell body to include bell body,
The lower surface of described bell body connects the connecting cylinder having cylindrically, and described connecting cylinder extend in retort, described connecting cylinder
Lower end be hinged with curved slab, the outer wall of described connecting cylinder is provided with for drive curved slab carry out rotate drive electricity
Machine, is provided with cold plate in described curved slab；Described curved slab includes that shell body and inner housing, described inner housing are set in shell
The inside of body also forms the cooling cavity of sealing；The both sides of described curved slab are connected on connecting cylinder through hollow rotating shaft, and institute
State hollow rotating shaft to connect with cooling cavity, described connecting cylinder is arranged with the bearing block for installing hollow rotating shaft；Described hollow
Rotating shaft one end is through bearing block and is arranged with annular sleeve, is provided with sealing ring, described ring between described annular sleeve and hollow rotating shaft
Shape set connects with outside water source through pipeline.
Embodiment five
The high purity metal calcium stagewise retort of the present embodiment, including heating furnace, is placed with reaction in described heating furnace
Tank, the inner bottom part of described retort is provided with the crucible for placing material, and the epimere of described retort is provided with for outward
What portion's vacuum system connected removes vacuum line, and the top of described retort connects has bell body, described bell body to include bell body,
The lower surface of described bell body connects the connecting cylinder having cylindrically, and described connecting cylinder extend in retort, described connecting cylinder
Lower end be hinged with curved slab, the outer wall of described connecting cylinder is provided with for drive curved slab carry out rotate drive electricity
Machine, is provided with cold plate in described curved slab；Described curved slab includes that shell body and inner housing, described inner housing are set in shell
The inside of body also forms the cooling cavity of sealing；The both sides of described curved slab are connected on connecting cylinder through hollow rotating shaft, and institute
State hollow rotating shaft to connect with cooling cavity, described connecting cylinder is arranged with the bearing block for installing hollow rotating shaft；Described hollow
Rotating shaft one end is through bearing block and is arranged with annular sleeve, is provided with sealing ring, described ring between described annular sleeve and hollow rotating shaft
Shape set connects with outside water source through pipeline；Gear ring it is provided with on the outer circle wall of described hollow rotating shaft, described driving motor
Output shaft connects driving gear intermeshing with gear ring.
Embodiment six
On the basis of any of the above-described embodiment, described heating furnace is provided with first paragraph heater strip spaced apart from each other and
Two-stage nitration heater strip.
Embodiment seven
On the basis of any of the above-described embodiment, the upper end of described crucible is provided with crucible cover, and described crucible cover is opened
It is provided with through hole.
Claims (7)
1. a high purity metal calcium stagewise retort, including heating furnace, is placed with retort in described heating furnace, described instead
The inner bottom part answering tank is provided with the crucible for placing material, the epimere of described retort be provided with for external vacuum system
Connect removes vacuum line, and the top of described retort connects bell body, it is characterised in that described bell body includes bell
Body, the lower surface of described bell body connects the connecting cylinder having cylindrically, and described connecting cylinder extend in retort, described connection
The lower end of cylinder is hinged with curved slab, the outer wall of described connecting cylinder is provided with for driving curved slab to carry out rotating driving electric
Machine, is provided with cold plate in described curved slab.
High purity metal calcium stagewise retort the most according to claim 1, it is characterised in that described curved slab includes shell
Body and inner housing, described inner housing is sheathed within the outer shell and form the cooling cavity of sealing.
High purity metal calcium stagewise retort the most according to claim 2, it is characterised in that the both sides warp of described curved slab
Hollow rotating shaft is connected on connecting cylinder, and described hollow rotating shaft with cooling cavity connect, described connecting cylinder is arranged with for
The bearing block of hollow rotating shaft is installed.
High purity metal calcium stagewise retort the most according to claim 3, it is characterised in that described hollow rotating shaft one end is worn
Crossing bearing block and be arranged with annular sleeve, being provided with sealing ring between described annular sleeve and hollow rotating shaft, described annular sleeve is through pipeline
Connect with outside water source.
High purity metal calcium stagewise retort the most according to claim 4, it is characterised in that the cylindrical of described hollow rotating shaft
Being provided with gear ring on perisporium, the output shaft of described driving motor connects driving gear intermeshing with gear ring.
High purity metal calcium stagewise retort the most according to claim 1, it is characterised in that described heating furnace is provided with phase
The first paragraph heater strip separated mutually and second segment heater strip.
High purity metal calcium stagewise retort the most according to claim 1, it is characterised in that the upper end of described crucible is arranged
There is crucible cover, described crucible cover offers through hole.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620887939.9U CN205856569U (en) | 2016-08-16 | 2016-08-16 | A kind of high purity metal calcium stagewise retort |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620887939.9U CN205856569U (en) | 2016-08-16 | 2016-08-16 | A kind of high purity metal calcium stagewise retort |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205856569U true CN205856569U (en) | 2017-01-04 |
Family
ID=57594524
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620887939.9U Active CN205856569U (en) | 2016-08-16 | 2016-08-16 | A kind of high purity metal calcium stagewise retort |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205856569U (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108249676A (en) * | 2018-02-11 | 2018-07-06 | 叶利萍 | Micro quantity organic pollutant enriching apparatus in a kind of new type water |
| CN108331546A (en) * | 2018-02-11 | 2018-07-27 | 义乌市绿美生物科技有限公司 | A kind of novel oilfield chemicals equipment |
| CN109055768A (en) * | 2018-02-24 | 2018-12-21 | 虔东稀土集团股份有限公司 | A method of it preparing the vacuum drying oven of High purity samarium metal and its prepares High purity samarium metal |
-
2016
- 2016-08-16 CN CN201620887939.9U patent/CN205856569U/en active Active
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108249676A (en) * | 2018-02-11 | 2018-07-06 | 叶利萍 | Micro quantity organic pollutant enriching apparatus in a kind of new type water |
| CN108331546A (en) * | 2018-02-11 | 2018-07-27 | 义乌市绿美生物科技有限公司 | A kind of novel oilfield chemicals equipment |
| CN108331546B (en) * | 2018-02-11 | 2018-11-20 | 义乌市绿美生物科技有限公司 | A kind of novel oilfield chemicals equipment |
| CN109055768A (en) * | 2018-02-24 | 2018-12-21 | 虔东稀土集团股份有限公司 | A method of it preparing the vacuum drying oven of High purity samarium metal and its prepares High purity samarium metal |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN205856569U (en) | A kind of high purity metal calcium stagewise retort | |
| CN107893782A (en) | A kind of water pump cooling structure | |
| CN205317003U (en) | Rotary kiln surface radiant heat steam generator | |
| CN202698811U (en) | Steam cooker with separable inner liner | |
| CN205462178U (en) | High efficiency is reation kettle for rosin production | |
| CN208658820U (en) | A kind of steam chafing dish energy gathering cap air pressure valve | |
| CN206486490U (en) | A kind of rose liquid alembic of indirectly heat | |
| CN113058534B (en) | Chemical equipment temperature control equipment with alarm device | |
| CN204794572U (en) | Liquid cooling electric machine cooling ware | |
| CN209055766U (en) | A kind of Mobile phone screen defoaming machine with circulation heating structure | |
| CN202046906U (en) | Distilled water machine | |
| CN206391596U (en) | A kind of production concentration tank for treating AIDS-treating medicine | |
| CN211871448U (en) | High concentration waste liquid treatment evaporation reactor | |
| CN206768428U (en) | Heat exchanger component for middle model machine | |
| CN216592248U (en) | Heat conduction oil heating type insulation can | |
| CN106917648B (en) | The cylinder heat insulation structural of steam turbine | |
| CN214388942U (en) | Energy-saving type distillation kettle | |
| CN218131804U (en) | Preparation kettle with heat preservation function | |
| CN108144389A (en) | Coal production steam dust removing device | |
| CN104653486A (en) | High-temperature resistant fan for furnace | |
| CN203956088U (en) | A kind of transferred-arc plasma electric furnace with steam systematic function | |
| CN203584481U (en) | Steam sucking and cooling system for turbine steam seal for sugar factory | |
| CN210635732U (en) | Purification device of regenerated graphite | |
| CN202039049U (en) | Tea tree oil extracting device | |
| CN211875990U (en) | Energy-saving consumption-reducing type boiler continuous blowdown waste heat recovery device |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20220628 Address after: 614902 No.5, south section of Xingye Road, Jianong Town, Shawan District, Leshan City, Sichuan Province Patentee after: Sichuan JINGDING Technology Co.,Ltd. Address before: 614216 in maker dream factory, No.5, Xingxi Road, Fuxi Town, Emeishan City, Leshan City, Sichuan Province Patentee before: MOUNT EMEI CITY ELEMENTS AND NEW MATERIALS TECHNOLOGY CO.,LTD. |
|
| TR01 | Transfer of patent right |