CN205853163U - A kind of polyarylate resin pelletizing production line - Google Patents

A kind of polyarylate resin pelletizing production line Download PDF

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Publication number
CN205853163U
CN205853163U CN201620592441.XU CN201620592441U CN205853163U CN 205853163 U CN205853163 U CN 205853163U CN 201620592441 U CN201620592441 U CN 201620592441U CN 205853163 U CN205853163 U CN 205853163U
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Prior art keywords
reactor
discharge nozzle
polyarylate resin
tank
production line
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CN201620592441.XU
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Chinese (zh)
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宋才生
任华平
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Bo Sheng Novel Material Science And Technology Ltd Of Jiangyin City
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Bo Sheng Novel Material Science And Technology Ltd Of Jiangyin City
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Abstract

This utility model relates to a kind of polyarylate resin pelletizing production line, including the reactor set gradually, the first washing mechanism, concentration tank, centrifuge, at rear washing tank, baking oven and granulating mechanism;Reactor includes reactor body, reaction stirring paddle it is configured with in reaction kettle body, at least provided with a discharge nozzle below reactor body, top formula ball valve it is configured with in discharge nozzle, when material reacts in reactor, discharge nozzle is positioned at the tube chamber blocking etc. of below reactor by upper top formula ball valve.This utility model is able to ensure that polyarylate normal operation of whole production process from raw material to final products, optimizes each portion and produces, and makes the final products polyarylate granule prepared have higher degree of purity, stability, it is achieved that the continuous granulation of polyarylate resin produces.

Description

A kind of polyarylate resin pelletizing production line
Technical field
This utility model relates to polyarylate resin pelletizing production line.
Background technology
Polyarylate (PAR) is a kind of high transparency amorphous thermoplastic special engineering plastics, its glass transition temperature (Tg) About 194 DEG C, the heat distortion temperature 174 under big load~175 DEG C, can at 184 DEG C life-time service, the dimensional stability of goods Hydroscopicity good, nontoxic, low, high case hardness, resistance to ultraviolet shielded property are excellent, have high hot strength and toughness, It is widely used in the fields such as aviation, automobile, electronic apparatus, LED illumination, medical apparatus and instruments and energy traffic.
The patent of invention of Authorization Notice No. CN103965452B discloses the phase transfer catalysis interfacial polycondensation of a kind of polyarylate Method preparation and process for separation and purification, belong to the new method of aromatic copolyester refining and edulcoration, is particularly suitable for the contracting of phase transfer catalysis interface Poly-method synthesis aromatic copolyester, goes out, through deionized water wash, the sodium chloride that dereaction produces, and the machinery being filtered to remove in resin liquid is miscellaneous The resin separating-purifying of smart resin liquid, pulverizing and the solvent recovery reutilization technology prepared after matter.
Polyarylate is to impurity, process conditions sensitivity in preparation process, and the equipment therefore reacting used is also required to work and adapts to Property improve and just can ensure that normal production and the quality of final products.
Utility model content
The purpose of this utility model is to provide a kind of polyarylate resin pelletizing production line, the spy produced for polyarylate resin Different requirement, improves the quality of product.
The technical scheme in the invention for solving the above technical problem is: a kind of polyarylate resin pelletizing production line, bag Include set gradually reactor, the first washing mechanism, concentration tank, centrifuge, at rear washing tank, baking oven and granulating mechanism.
Preferably, reactor includes reactor body, is configured with reaction stirring paddle, below reactor body in reaction kettle body At least provided with a discharge nozzle, in described discharge nozzle, it is configured with top formula ball valve, in the state that material reacts in reactor Under, discharge nozzle is positioned at the tube chamber blocking of below reactor by described upper top formula ball valve;
Above-mentioned first washing mechanism includes that emulsion defecator and washing tank, described emulsion defecator arrange described reaction After still, before washing tank, first pass through the filtration of described defecator from reactor emulsion material out and be then re-fed into washing Washing in tank;
Above-mentioned concentration tank includes tank body, and tank body is provided with air entry, is configured with stirring paddle and crushing knife, tank body in tank body Lower section, at least provided with a discharge nozzle, is configured with top formula ball valve in described discharge nozzle, when material is in tank body, Discharge nozzle is positioned at the tube chamber blocking of below tank body by described upper top formula ball valve;
Above-mentioned centrifuge includes that centrifugal chamber, described centrifugal chamber are configured with water inlet pipe, and described centrifugal chamber inwall is provided with filter screen, The mesh number of described filter screen is between 400~600 mesh;
Relatively reasonably arranging is that reactor has cooling jacket, reduces the fluctuation of temperature in polymerization process.
Preferably, described crushing knife is zigzag.
Further, granulating mechanism includes melting granulator, and is arranged on the Devolatilization device of this melting granulator front end, institute Stating Devolatilization device and include disengagement chamber, the front-end configuration of this disengagement chamber has air-flow feeding port, described disengagement chamber to be configured with heating arrangement, Disengagement chamber cavity top uniformly offers bleeding point, the external exhaust tube of bleeding point, and material is blown from into separation from air-flow feeding port Chamber, the volatile matter contained in material is heated to rise and arranges outside bleeding point, and the powder in material falls, it is achieved to material before pelletize Devolatilization.
Above-mentioned heating arrangement is the heater strip of heating mantle or spiral winding.
Compared with prior art, the utility model has the advantage of: provide polyarylate resin pelletizing production line, it is possible to really Protect polyarylate normal operation of whole production process from raw material to final products, optimize each portion and produce, make the final products prepared Polyarylate granule has higher degree of purity, stability, it is achieved that the continuous granulation of polyarylate resin produces.
Accompanying drawing explanation
Fig. 1 is the structural representation of polyarylate resin pelletizing production line in this utility model embodiment;
Fig. 2 is the structural representation of reactor in this utility model embodiment;
Fig. 3 is the structural representation of the first washing mechanism in this utility model embodiment;
Fig. 4 is the structural representation of concentration tank in this utility model embodiment;
Fig. 5 is the structural representation of centrifuge in this utility model embodiment;
Fig. 6 is the structural representation of granulating mechanism in this utility model embodiment.
Detailed description of the invention
Below in conjunction with accompanying drawing embodiment, this utility model is described in further detail.
Polyarylate resin pelletizing production line in the present embodiment, including reactor the 1, first washing mechanism 2 set gradually, Concentration tank 3, centrifuge 4, at rear washing tank 5, baking oven 6 and granulating mechanism 7.
Reactor 1 includes reactor body 1.1, is configured with reaction stirring paddle 1.2, reactor body in reaction kettle body 1.1 At least provided with a discharge nozzle 1.3 below 1.1, it is configured with top formula ball valve 1.4 in described discharge nozzle 1.3, at material in instead Answering in still under the state of reaction, discharge nozzle 1.3 is positioned at the tube chamber blocking of below reactor by described upper top formula ball valve 1.4.Relatively close The setting of reason is that described reactor has cooling jacket 1.5, contributes to controlling reaction temperature, reduces the fluctuation of reaction temperature.
The reactor of said structure, by arranging top formula ball valve, in reaction in the discharge nozzle of reactor body bottom portion During, on this, formula ball valve in top can will be located in the discharge nozzle tube chamber of below reactor and blocks, and prevents the material in reactor from existing Discharge nozzle inner accumulated, helps to ensure that the whole effecting reaction of all materials.
Washing mechanism 2 is for washing polyarylate resin emulsion head product, after being arranged on reactor 1, including breast Liquid defecator 2.2 and washing tank 2.3, after described emulsion defecator 2.2 arranges described reactor 1, washing tank 2.3 it Before, first pass through described defecator 2.2 from reactor 1 emulsion material out and filter and be then re-fed in washing tank 2.3 washing, Defecator 2.2 uses filter screen filtration preferably to filter gauze.
The washing mechanism of said structure, is first filtered to remove mechanical admixture to emulsion material out from reactor, Then it is re-fed into washing tank washing, eliminates first to wash at present and filter a difficult problem for filtration difficulty present in the mode of production afterwards, no Only help to improve filter effect, and improve production efficiency.
Concentration tank 3 includes tank body 3.1, tank body 3.1 is provided with air entry, is configured with stirring paddle 3.2 in described tank body 3.1 With crushing knife 3.5, at least provided with a discharge nozzle 3.3 below tank body 3.1, in described discharge nozzle 3.3, it is configured with top formula ball Valve 3.4, when material is in tank body 3.1, discharge nozzle 3.3 is positioned at the pipe of below tank body by described upper top formula ball valve 3.4 Chamber blocks to prevent material from blocking in discharge nozzle 3.Described crushing knife 3.5 is zigzag, prevents material at concentration process Middle caking.
Above-mentioned concentration tank is prevented from material caking in concentration process by arranging crushing knife, it addition, upper top formula ball valve energy Enough prevent material from luming in discharge nozzle, it is ensured that the granular material discharging finally obtained is smooth and easy.
Centrifuge 4 is that the material after desolvation is further dried acquisition powder, including centrifugal chamber a, described centrifugal chamber a Being configured with water inlet pipe 4.1, described centrifugal chamber a inwall is provided with filter screen 4.2, and the mesh number of filter screen 4.2 is between 400~600 mesh.Pass through Configure water inlet pipe to centrifugal chamber, at the centrifugal initial stage, by water inlet pipe to centrifugal chamber inner water-supply, then coordinate centrifuge to arrange suitably Rotating speed, makes the sodium chloride dissolution as far as possible of remnants and throws away with water, is stripped of in powder the sodium chloride of remnants, dried object further Also product has been purified while material.
Granulating mechanism 7 includes melting granulator 7.1, and is arranged on the Devolatilization device 8 of this melting granulator 7.1 front end, institute Stating Devolatilization device 8 and include disengagement chamber 8.1, the front-end configuration of this disengagement chamber 8.1 has air-flow feeding port 8.2, described disengagement chamber 8.1 to join Being equipped with heating arrangement, disengagement chamber 8.1 cavity top uniformly offers bleeding point 8.3, the external exhaust tube of bleeding point 8.3, material from Air-flow feeding port 8.2 is blown from into disengagement chamber 8.1, and the volatile matter contained in material is heated rising through the outer row of bleeding point 8.3, material In powder fall, it is achieved devolatilization to material before pelletize.Heating arrangement is the heater strip being spirally wound on disengagement chamber periphery 8.4。
The granulating mechanism of said structure arranges Devolatilization device in the front end of melting granulator, and material is carried out degree of depth devolatilization, The moisture being blended in material, trace solvent etc. are removed further, thus improves the degree of purity of material, contribute to obtaining more The polyarylate granule of high-quality.
This utility model is able to ensure that polyarylate normal operation of whole production process from raw material to final products, optimizes each Portion produces, and makes the final products polyarylate granule prepared have higher degree of purity, stability, it is achieved that the company of polyarylate resin Continuous pelletize produces.

Claims (5)

1. a polyarylate resin pelletizing production line, it is characterised in that: the reactor that includes setting gradually, the first washing mechanism, Concentration tank, centrifuge, at rear washing tank, baking oven and granulating mechanism;
Described reactor includes reactor body, is configured with reaction stirring paddle, at least sets below reactor body in reaction kettle body It is equipped with a discharge nozzle, in described discharge nozzle, is configured with top formula ball valve, when material reacts in reactor, described Discharge nozzle is positioned at the tube chamber blocking of below reactor by upper top formula ball valve;
Described first washing mechanism include emulsion defecator and washing tank, described emulsion defecator arrange described reactor it Afterwards, before washing tank, first pass through described defecator from reactor emulsion material out and filter and be then re-fed in washing tank Washing;
Described concentration tank includes tank body, and tank body is provided with air entry, is configured with stirring paddle and crushing knife, below tank body in tank body At least provided with a discharge nozzle, in described discharge nozzle, it is configured with top formula ball valve, when material is in tank body, described Discharge nozzle is positioned at the tube chamber blocking of below tank body by upper top formula ball valve;
Described centrifuge includes that centrifugal chamber, described centrifugal chamber are configured with water inlet pipe, and described centrifugal chamber inwall is provided with filter screen, described The mesh number of filter screen is between 400~600 mesh.
Polyarylate resin pelletizing production line the most according to claim 1, it is characterised in that: described reactor has cooling folder Set.
Polyarylate resin pelletizing production line the most according to claim 1, it is characterised in that: described crushing knife is zigzag.
Polyarylate resin pelletizing production line the most according to claim 1, it is characterised in that: described granulating mechanism includes melting Comminutor, and it is arranged on the Devolatilization device of this melting granulator front end, described Devolatilization device includes disengagement chamber, before this disengagement chamber End is configured with air-flow feeding port, and described disengagement chamber is configured with heating arrangement, and disengagement chamber cavity top uniformly offers bleeding point, takes out The external exhaust tube of QI KOU, material is blown from into disengagement chamber from air-flow feeding port, and the volatile matter contained in material is heated rising through taking out Arranging outside QI KOU, powder in material falls, it is achieved devolatilization to material before pelletize.
Polyarylate resin pelletizing production line the most according to claim 4, it is characterised in that: described heating arrangement is heating mantle Or the heater strip of spiral winding.
CN201620592441.XU 2016-06-17 2016-06-17 A kind of polyarylate resin pelletizing production line Active CN205853163U (en)

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CN201620592441.XU CN205853163U (en) 2016-06-17 2016-06-17 A kind of polyarylate resin pelletizing production line

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Application Number Priority Date Filing Date Title
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107871438A (en) * 2017-11-22 2018-04-03 河南莱帕克化工设备制造有限公司 Polystyrene resin produces line training device
CN109107221A (en) * 2018-08-21 2019-01-01 金发科技股份有限公司 A kind of liquid-solid extraction purification devices and purification process
CN109731537A (en) * 2018-12-31 2019-05-10 江苏麒祥高新材料有限公司 A kind of complexes of binder resin processing

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107871438A (en) * 2017-11-22 2018-04-03 河南莱帕克化工设备制造有限公司 Polystyrene resin produces line training device
CN109107221A (en) * 2018-08-21 2019-01-01 金发科技股份有限公司 A kind of liquid-solid extraction purification devices and purification process
CN109731537A (en) * 2018-12-31 2019-05-10 江苏麒祥高新材料有限公司 A kind of complexes of binder resin processing

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