CN205839099U - A kind of this grade of internal circulation apparatus of extraction tank organic facies - Google Patents

A kind of this grade of internal circulation apparatus of extraction tank organic facies Download PDF

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Publication number
CN205839099U
CN205839099U CN201620625691.9U CN201620625691U CN205839099U CN 205839099 U CN205839099 U CN 205839099U CN 201620625691 U CN201620625691 U CN 201620625691U CN 205839099 U CN205839099 U CN 205839099U
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China
Prior art keywords
organic facies
cofferdam
plate
extraction tank
room
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Withdrawn - After Issue
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CN201620625691.9U
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Chinese (zh)
Inventor
曾阳庆
马朝扬
陈建彬
甘家毅
欧金宝
梁红梅
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CHINALCO JINYUAN RARE-EARTH Co Ltd
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CHINALCO JINYUAN RARE-EARTH Co Ltd
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Priority to CN201620625691.9U priority Critical patent/CN205839099U/en
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

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Abstract

This utility model provides a kind of this grade of internal circulation apparatus of extraction tank organic facies, including extraction tank body, described extraction tank body interior is separated into clarifying chamber by cell body dividing plate and mixing chamber overflow plate, mixing chamber and latent room, described latent room is positioned at bottom mixing chamber, it is provided with in described clarifying chamber and passes into upper level for aqueous phase and dive the aqueous phase cofferdam of room and pass into next stage for organic facies and dive the organic facies cofferdam of room, described organic facies cofferdam is separated into inter-stage organic facies cofferdam and interior circulation organic facies cofferdam by one piece of organic facies dividing plate, top, described interior circulation organic facies cofferdam is provided with organic facies flow control board, it is provided with, bottom described interior circulation organic facies cofferdam, the organic facies inner cycle channel connected with this grade of latent room.When this utility model preferably solves extract and separate, extraction section organic facies and aqueous phase stream are than too small problem, it is ensured that extraction process is properly functioning, reduce the extraction S amount of organic facies, reduce the acid and alkali consumption of extract and separate.

Description

A kind of this grade of internal circulation apparatus of extraction tank organic facies
Technical field
This utility model belongs to extraction equipment technical field, is specifically related to circulation dress in a kind of extraction tank this level of organic facies Put.
Background technology
During the cascade extraction of rare earth, it will usually have the amount of easily extraction component in rare earth feed liquid much smaller than difficult extraction group Point situation, realize separating two rare earth element components, at the theoretical flow ratio of extraction section organic facies and aqueous phase close to 1:1.But Being that organic facies is too small with the flow ratio of aqueous phase causes mixing chamber hydrops, causes organic facies circulation difficulty even to stop, finally makes extraction Process cannot be carried out.In order to ensure the operation smoothness of extraction tank, the stream of extraction section organic facies to be strengthened in actual production Ratio.The method of the flow ratio strengthening extraction section organic facies is to reduce the extraction S amount of organic facies or strengthen the extraction S amount of organic facies, but It is to use both approaches that following deficiency be individually present:
If the extraction S amount of reduction organic facies, need washing of addition sour less with acid regurgitation flow at washing section and stripping section, Cause aqueous phase out of proportion with organic facies flow, load organic phases with wash acid, acid regurgitation fails to be fully contacted reaction at mixing chamber, wash Wash and back extraction weak effect;
If strengthening the extraction S amount of organic facies, then needing to add at washing section and stripping section and more washing acid and acid regurgitation, making Strip liquor rare earth concentration is low, acidity is high, volume is big for one-tenth, and the trouble brought to later separation operation makes the consumption of bronsted lowry acids and bases bronsted lowry simultaneously Amount increases, and production cost increases.
Current Rare Earth Separation enterprise would generally select to strengthen the extraction S amount of organic facies, separates easily extraction component with realization and contains Measure less rare earth feed liquid, cause the increase of material consumption and energy consumption.Therefore, it is necessary to research organic facies and the extraction of the low flow ratio of aqueous phase Take segregation apparatus.
Utility model content
For solving above-mentioned technical problem, this utility model provides a kind of this grade of internal circulation apparatus of extraction tank organic facies.
This utility model is achieved by the following technical programs.
A kind of this grade of internal circulation apparatus of extraction tank organic facies that this utility model provides, including extraction tank body;Described extraction Taking groove body to be made up of cell body coaming plate, cell body base plate and cell body dividing plate, described extraction tank body interior is by cell body dividing plate and mixes Closing room overflow plate and be separated into clarifying chamber, mixing chamber and latent room, described latent room includes that dive room, next stage of this level dives room and upper level is dived Room, and be positioned at bottom mixing chamber, is provided with in described clarifying chamber and passes into upper level for aqueous phase and dive the aqueous phase cofferdam of room and confession Organic facies passes into next stage and dives the organic facies cofferdam of room, and described organic facies cofferdam separates staged by one piece of organic facies dividing plate Between organic facies cofferdam and interior circulation organic facies cofferdam, top, described interior circulation organic facies cofferdam is provided with organic facies Flow-rate adjustment Plate, is provided with the organic facies inner cycle channel connected with this grade of latent room, described clarifying chamber bottom described interior circulation organic facies cofferdam In organic facies overflow across inter-stage organic facies cofferdam and interior circulation organic facies cofferdam respectively and enter next stage and dive room and this level is dived room.
Described organic facies cofferdam is arranged on extraction tank body interior, and by coaming plate on passage and channel side coaming plate and cell body Baffle combination forms organic facies inner cycle channel.
Described organic facies flow control board and top, interior circulation organic facies cofferdam are connected by chute.
Described mixing chamber is surrounded by mixing chamber overflow plate, mixing chamber base plate and cell body dividing plate, and in the middle part of mixing chamber base plate It is provided with cylindrical hole.
It is provided with reinforcement bottom described mixing chamber base plate.
Described extraction tank is the most internal is additionally provided with reinforcing plate between cell body dividing plate.
Described aqueous phase cofferdam is made up of cofferdam plate in aqueous phase periphery weir plate and aqueous phase, and wherein in aqueous phase, cofferdam plate is positioned at aqueous phase Inside peripheral weir plate, and plate top in cofferdam is provided with aqueous phase overflow pipe in aqueous phase, cofferdam in aqueous phase periphery weir plate with aqueous phase Plate lower end arranges overfall.
The height in described inter-stage organic facies cofferdam is identical with the height of mixing chamber overflow plate.
The low 2-5cm of height in the aspect ratio inter-stage organic facies cofferdam in described interior circulation organic facies cofferdam.
The height of described organic facies flow control board is 4-8cm.
The beneficial effects of the utility model are:
This utility model simple in construction, convenient operation and control, when preferably solving extract and separate extraction section organic facies with Aqueous phase stream is than too small problem, it is ensured that extraction process is properly functioning, reduces the extraction S amount of organic facies, reduces extract and separate Acid and alkali consumption.
Compared with prior art, in the case of the low flow ratio of organic facies and aqueous phase, extraction tank can be properly functioning;In easy extraction group During the Rare Earth Separation that point content is relatively low, improve the extraction section organic facies extract and separate efficiency to easily extracting component;Can reduce Organic facies extraction S amount, reduce the acid and alkali consumption of extract and separate, the minimizing of organic facies flow simultaneously can reduce washing section and The extraction equipment size of stripping section, reduces equipment and the input of material.
Accompanying drawing explanation
Fig. 1 is planar structure schematic diagram of the present utility model;
Fig. 2 is the A-A direction view of Fig. 1;
Fig. 3 is the B-B direction view of Fig. 1;
Fig. 4 is the C-C direction view of Fig. 1;
Fig. 5 is profile perspective view of the present utility model;
Fig. 6 is internal perspective view of the present utility model;
Fig. 7 is end position solid cut-away diagram of the present utility model;
Fig. 8 is medium position solid cut-away diagram of the present utility model;
Fig. 9 is the perspective view in organic facies cofferdam in this utility model;
Figure 10 is the polycrystalline substance schematic diagram of Fig. 9;
Figure 11 is the structural representation in aqueous phase cofferdam in this utility model.
In figure: 1-extraction tank body, 2-clarifying chamber, 3-mixing chamber, 4-dives room, 5-organic facies cofferdam, 6-aqueous phase cofferdam, 7- Inter-stage organic facies cofferdam, circulation organic facies cofferdam, 9-organic facies dividing plate, 10-reinforcing plate, 11-cell body coaming plate, 12-cell body in 8- Base plate, 13-cell body dividing plate, 31-mixing chamber overflow plate, 32-mixing chamber base plate, this level of 41-dives room, and 42-next stage is dived room, 43- Upper level is dived room, 61-aqueous phase periphery weir plate, cofferdam plate in 62-aqueous phase, 63-aqueous phase overflow pipe, 64-overfall, 81-organic facies Flow control board, 82-chute, 83-organic facies inner cycle channel, 321-cylindrical hole, 322-reinforcement, coaming plate on 831-passage, 832-channel side coaming plate.
Detailed description of the invention
The technical solution of the utility model is described further below, but claimed scope is not limited to described.
A kind of this grade of internal circulation apparatus of extraction tank organic facies, including extraction tank body 1;Described extraction tank body 1 is by cell body Coaming plate 11, cell body base plate 12 and cell body dividing plate 13 form, and described extraction tank body 1 is internal to be overflow by cell body dividing plate 13 and mixing chamber Stream plate 31 is separated into clarifying chamber 2, mixing chamber 3 and latent room 4, and described latent room 4 includes that dive room 41, next stage of this level is dived room 42 and upper The latent room 43 of level, and is positioned at bottom mixing chamber 3, is provided with and passes into upper level for aqueous phase and dive the water of room 43 in described clarifying chamber 2 Phase cofferdam 6 and pass into next stage for organic facies and dive the organic facies cofferdam 5 of room 42, described organic facies cofferdam 5 is had by one piece Machine phase dividing plate 9 is separated into inter-stage organic facies cofferdam 7 and interior circulation organic facies cofferdam 8, and top, described interior circulation organic facies cofferdam 8 sets It is equipped with organic facies flow control board 81, is provided with organic with what this grade of latent room 41 connected bottom described interior circulation organic facies cofferdam 8 Phase inner cycle channel 83, the organic facies in described clarifying chamber 2 overflows across inter-stage organic facies cofferdam 7 and interior circulation organic facies cofferdam respectively 8 enter next stage dives room 42 and this level is dived room 41.Using the technical program, the organic facies of clarifying chamber 2 overflows across inter-stage organic facies and encloses Weir 7 and interior circulation organic machine cofferdam 8 respectively enter entrance next stage and dive room 42 and this level is dived room 41, organic by circulation in mobile The organic facies flow control board 81 at top, phase cofferdam 8 can realize the organic facies circular flow at this grade.Organic facies flow is adjusted When joint plate moves to interior circulation organic facies cofferdam Close All, organic facies not inner circulating reflux can be realized.There is simple in construction, operation Feature easy to control, when preferably solving extract and separate, extraction section organic facies and aqueous phase stream are than too small problem, it is ensured that extraction Take process properly functioning, reduce the extraction S amount of organic facies, reduce the acid and alkali consumption of extract and separate.This device is applied in reality In can have some levels, i.e. internal to be separated into several by cell body dividing plate 13 and mixing chamber overflow plate 31 clear for extraction tank body 1 Clear room 2, mixing chamber 3 and latent room 4, the technical program is as a example by three grades, i.e. clarifying chamber 2, mixing chamber 3 and latent room 4 is respectively three, Three latent rooms 4 are respectively dive room 41, next stage of this level and dive room 42 and upper level is dived room 43;In production application according to actual needs Can be level Four, Pyatyi, six grades etc..Concrete progression is decided according to the actual requirements.
It is internal that described organic facies cofferdam 5 is arranged on extraction tank body 1, and by coaming plate 831 and channel side coaming plate on passage 832 form organic facies inner cycle channel 83 with cell body dividing plate 13 combination.
Described organic facies flow control board 81 and top, interior circulation organic facies cofferdam 8 are connected by chute 82.So, It is easy to the circular flow of this grade of slidable adjustment.
Described mixing chamber 3 is surrounded by mixing chamber overflow plate 31, mixing chamber base plate 32 and cell body dividing plate 13, and at the bottom of mixing chamber Cylindrical hole 321 it is provided with in the middle part of plate 32.So, the organic facies under latent room 4 and aqueous phase pass through under the effect of the draft of stirring paddle Cylindrical hole 321 enters mixing chamber 3 and enters hybrid extraction.
It is provided with reinforcement 322 bottom described mixing chamber base plate 32.When actual fabrication, reinforcement 322 is designed to T-shaped Structure, and T-shaped head infall is positioned at cylindrical hole 321 center, thus pretend being formed effectively to add bottom mixing chamber 3 With.
Between cell body dividing plate 13, reinforcing plate 10 it is additionally provided with in described extraction tank body 1.Prevent dividing plate 13 in extraction It is deformed in groove body 1 and affects extraction quality.
Described aqueous phase cofferdam 6 is made up of cofferdam plate 62 in aqueous phase periphery weir plate 61 and aqueous phase, wherein cofferdam plate 62 in aqueous phase It is positioned at inside aqueous phase periphery weir plate 61, and cofferdam plate 62 top is provided with aqueous phase overflow pipe 63 in aqueous phase, in the outer cofferdam of aqueous phase Plate 61 arranges overfall 64 with cofferdam plate 62 lower end in aqueous phase.
The height in described inter-stage organic facies cofferdam 7 is identical with the height of mixing chamber overflow plate 31.
The low 2-5cm of height in the aspect ratio inter-stage organic facies cofferdam 7 in described interior circulation organic facies cofferdam 8.Use this size, This grade of capacity of returns of organic facies is favorably strengthened in application process.
The height of described organic facies flow control board 81 is 4-8cm.In actual use, it is possible to shelter from organic facies completely ?.

Claims (10)

1. this grade of internal circulation apparatus of an extraction tank organic facies, it is characterised in that: include extraction tank body (1), described extraction tank Body (1) is made up of cell body coaming plate (11), cell body base plate (12) and cell body dividing plate (13), and described extraction tank body (1) is internal logical Cross cell body dividing plate (13) and mixing chamber overflow plate (31) is separated into clarifying chamber (2), mixing chamber (3) and latent room (4), described latent room (4) include that dive room (41), next stage of this level dives room (42) and upper level is dived room (43), and be positioned at mixing chamber (3) bottom, described clear It is provided with in clear room (2) and passes into upper level for aqueous phase and dive the aqueous phase cofferdam (6) of room (43) and passing into down for organic facies One-level is dived the organic facies cofferdam (5) of room (42), and described organic facies cofferdam (5) is separated into inter-stage by one piece of organic facies dividing plate (9) Organic facies cofferdam (7) and interior circulation organic facies cofferdam (8), described interior circulation organic facies cofferdam (8) top is provided with organic phase fluid Amount adjustable plate (81), described interior circulation organic facies cofferdam (8) bottom is followed in being provided with the organic facies that room (41) of diving with this level connects Ring passage (83), the organic facies in described clarifying chamber (2) overflows across inter-stage organic facies cofferdam (7) and interior circulation organic facies cofferdam respectively (8) enter next stage and dive room (42) and this level is dived room (41).
2. this grade of internal circulation apparatus of extraction tank organic facies as claimed in claim 1, it is characterised in that: described organic facies cofferdam (5) extraction tank body (1) it is arranged on internal, and by coaming plate (831) on passage and channel side coaming plate (832) and cell body dividing plate (13) combination forms organic facies inner cycle channel (83).
3. this grade of internal circulation apparatus of extraction tank organic facies as claimed in claim 1, it is characterised in that: described organic facies flow is adjusted Joint plate (81) and interior circulation organic facies cofferdam (8) top are connected by chute (82).
4. this grade of internal circulation apparatus of extraction tank organic facies as claimed in claim 1, it is characterised in that: described mixing chamber (3) by Mixing chamber overflow plate (31), mixing chamber base plate (32) and cell body dividing plate (13) surround, and arrange at mixing chamber base plate (32) middle part There is cylindrical hole (321).
5. this grade of internal circulation apparatus of extraction tank organic facies as claimed in claim 4, it is characterised in that: described mixing chamber base plate (32) bottom is provided with reinforcement (322).
6. this grade of internal circulation apparatus of extraction tank organic facies as claimed in claim 1, it is characterised in that: described extraction tank body (1) it is positioned between cell body dividing plate (13) and is additionally provided with reinforcing plate (10).
7. this grade of internal circulation apparatus of extraction tank organic facies as claimed in claim 1, it is characterised in that: described aqueous phase cofferdam (6) Being made up of cofferdam plate (62) in aqueous phase periphery weir plate (61) and aqueous phase, wherein in aqueous phase, cofferdam plate (62) is positioned at aqueous phase periphery weir plate (61) inner side, and in aqueous phase, cofferdam plate (62) top is provided with aqueous phase overflow pipe (63), at aqueous phase periphery weir plate (61) and water Plate (62) lower end, mutually interior cofferdam arranges overfall (64).
8. this grade of internal circulation apparatus of extraction tank organic facies as claimed in claim 1, it is characterised in that: described inter-stage organic facies is enclosed The height on weir (7) is identical with the height of mixing chamber overflow plate (31).
9. this grade of internal circulation apparatus of extraction tank organic facies as claimed in claim 1, it is characterised in that: described interior circulation organic facies The low 2-5cm of height of aspect ratio inter-stage organic facies cofferdam (7) in cofferdam (8).
10. this grade of internal circulation apparatus of extraction tank organic facies as claimed in claim 3, it is characterised in that: described organic facies flow The height of adjustable plate (81) is 4-8cm.
CN201620625691.9U 2016-06-22 2016-06-22 A kind of this grade of internal circulation apparatus of extraction tank organic facies Withdrawn - After Issue CN205839099U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201620625691.9U CN205839099U (en) 2016-06-22 2016-06-22 A kind of this grade of internal circulation apparatus of extraction tank organic facies

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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105907996A (en) * 2016-06-22 2016-08-31 中铝广西有色金源稀土有限公司 Organic phase corresponding stage reflux device of extraction tank
CN109680168A (en) * 2019-02-22 2019-04-26 广东富远稀土新材料股份有限公司 Rare earth extraction separation reflux organic phase constant-current stabilizer

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105907996A (en) * 2016-06-22 2016-08-31 中铝广西有色金源稀土有限公司 Organic phase corresponding stage reflux device of extraction tank
CN105907996B (en) * 2016-06-22 2018-02-13 中铝广西有色金源稀土有限公司 A kind of this grade of reflux of extraction tank organic phase
CN109680168A (en) * 2019-02-22 2019-04-26 广东富远稀土新材料股份有限公司 Rare earth extraction separation reflux organic phase constant-current stabilizer
CN109680168B (en) * 2019-02-22 2023-04-07 广东省富远稀土有限公司 Rare earth extraction separation reflux organic phase current stabilizer

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Granted publication date: 20161228

Effective date of abandoning: 20180213

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