CN205809020U - A kind of sampling needle for thin-layer chromatography of band leg - Google Patents

A kind of sampling needle for thin-layer chromatography of band leg Download PDF

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Publication number
CN205809020U
CN205809020U CN201620785327.9U CN201620785327U CN205809020U CN 205809020 U CN205809020 U CN 205809020U CN 201620785327 U CN201620785327 U CN 201620785327U CN 205809020 U CN205809020 U CN 205809020U
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CN
China
Prior art keywords
pipe
needle
point sample
spotting
support ring
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201620785327.9U
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Chinese (zh)
Inventor
张彦坤
张蔓
李婷
沈宗尧
龚启勇
罗鸣
罗一鸣
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Harbin University of Science and Technology
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Harbin University of Science and Technology
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Priority to CN201620785327.9U priority Critical patent/CN205809020U/en
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Publication of CN205809020U publication Critical patent/CN205809020U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

A kind of sampling needle for thin-layer chromatography of band leg, the axial upper end of spotting needle pipe-in-pipe is provided with the opening of cavity and the ft connection making spotting needle pipe-in-pipe, spotting needle pipe-in-pipe lower axial end is provided with the perforate passed for point sample syringe needle, it is provided with screw thread outside spotting needle pipe-in-pipe, point sample needle tubing is arranged on inside spotting needle pipe-in-pipe, the perforate of point sample syringe needle crossing point sample needle tubing its lower end, the screw thread matched with spotting needle pipe-in-pipe outside screw it is provided with inside support ring, support ring is arranged on outside spotting needle pipe-in-pipe, support ring and spotting needle pipe-in-pipe are that screw thread spins, connect outside support ring and have support arm, leg has been connected up with support arm Vertical Square, spotting needle pipe-in-pipe is provided with observation window and measures chi.This sampling needle for thin-layer chromatography can solve the problem that point sample dynamics difficulty control problem, can prevent spotting needle from puncturing the coating layer on chromatographic sheet, by rotating support ring, controls the distance between point sample syringe needle and chromatographic sheet, it is ensured that point sample is accurate.

Description

A kind of sampling needle for thin-layer chromatography of band leg
Technical field
This utility model relates to chemical analysis instrument technical field, particularly relates to the thin layer chromatography point sample of a kind of band leg Pin.
Background technology
Thin layer chromatography is a kind of adsorption thin-layer chromatography partition method, and it utilizes each composition to same adsorbent ability not With, make during in flowing phase, (solvent) flow through fixing phase (adsorbent), continuous print produces that Adsorption and desorption is attached, adsorbs, more again Desorption, thus reach the purpose disconnected from each other of each composition.Thin layer chromatography is sharp separation and a small amount of material of qualitative analysis A kind of critically important experimental technique, be also used for follow the tracks of reaction process.
When thin-layer chromatographic analysis, need to use sample applicator to drop in thin layer chromatography board by detected sample, point sample diameter It is usually no more than 5mm.In the actual mechanical process of thin-layer chromatographic analysis, owing to lacking the firmly strong point, spotting needle easily stings Coating in broken thin layer chromatography board, spotting needle is easily shaken, unstable, inaccurate, causes point sample not meet the analysis of thin layer chromatography Requirement.
Summary of the invention
This utility model is for the problems referred to above, it is provided that the sampling needle for thin-layer chromatography of band leg, and this sampling needle for thin-layer chromatography holds Easily operate, be easily controlled point sample dynamics, it is simple to the distance between regulation point sample syringe needle and chromatographic sheet, point sample uniformly, accurately, Stable.
The technical scheme that the above-mentioned technical problem of this utility model solution is used is as follows:
A kind of sampling needle for thin-layer chromatography of band leg, including point sample needle tubing, point sample syringe needle, spotting needle pipe-in-pipe, support ring, Support arm, leg, the gimbal lever, observation window, measuring chi, the axial upper end of described spotting needle pipe-in-pipe is provided with and makes spotting needle pipe box The cavity of pipe and the opening of ft connection, spotting needle pipe-in-pipe lower axial end is provided with the perforate passed for point sample syringe needle, spotting needle Being provided with screw thread outside pipe-in-pipe, point sample needle tubing is arranged on inside spotting needle pipe-in-pipe, under point sample syringe needle crossing point sample needle tubing sleeve pipe The perforate of end, is provided with the screw thread matched with spotting needle pipe-in-pipe outside screw inside support ring, support ring is arranged on spotting needle Outside pipe-in-pipe, support ring and spotting needle pipe-in-pipe are that screw thread spins, and connecting outside support ring has support arm, are being perpendicular to support Being connected with leg upper end away from support ring end of support arm on arm direction, it is being perpendicular to leg lower end and the gimbal lever on leg direction Connecting, spotting needle pipe-in-pipe is provided with observation window and measures chi.
As preferably, described support ring is with support arm at grade.
As preferably, described support ring is arranged in spotting needle pipe-in-pipe, can dismantle.
This utility model has the advantages that the sampling needle for thin-layer chromatography of a kind of band leg can solve the problem that point sample dynamics Difficult control problem, support ring, support arm, leg cooperation under, can prevent spotting needle from puncturing the coating layer on chromatographic sheet, By rotating support ring or rotating point sample needle tubing sleeve pipe, control the distance between point sample syringe needle and chromatographic sheet, this thin layer color Spectrum spotting needle easily operates, is easily controlled point sample dynamics, it is simple to the distance between regulation point sample syringe needle and chromatographic sheet, point sample Do not shake, accurately, stable, uniform.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
In figure: 1-point sample needle tubing;2-point sample syringe needle;3-spotting needle pipe-in-pipe;4-support ring;5-support arm;6-leg;7- The gimbal lever;8-observation window;9-measures chi.
Detailed description of the invention
For making the purpose of this utility model, technical scheme and advantage of greater clarity, come in detail below in conjunction with accompanying drawing Embodiment of the present utility model is described.However, it should be understood that these describe the most exemplary, and it is not intended to limit this practicality Novel scope.Additionally, in the following description, the description to known features and technology is eliminated, to avoid unnecessarily obscuring Concept of the present utility model.
In describing the invention, it should be noted that term " " center ", " longitudinally ", " laterally ", " on ", D score, Orientation or the position relationship of the instruction such as "front", "rear", "left", "right", " vertically ", " level ", " top ", " end " " interior ", " outward " are Based on orientation shown in the drawings or position relationship, it is for only for ease of the description present invention and simplifies description rather than instruction or dark The device or the element that show indication must have specific orientation, with specific azimuth configuration and operation, therefore it is not intended that right The restriction of the present invention.
In describing the invention, it should be noted that unless otherwise clearly defined and limited, term " is installed ", " phase Even ", " connection " should be interpreted broadly, for example, it may be fixing connection, it is also possible to be to removably connect, or be integrally connected;Can To be mechanical connection, it is also possible to be electrical connection;Can be to be joined directly together, it is also possible to be indirectly connected to by intermediary, Ke Yishi The connection of two element internals.For the ordinary skill in the art, above-mentioned term can be understood as the case may be Concrete meaning in the present invention.
As it can be seen, the sampling needle for thin-layer chromatography of a kind of band leg, including point sample needle tubing 1, point sample syringe needle 2, point sample needle tubing Sleeve pipe 3, support ring 4, support arm 5, leg 6, the gimbal lever 7, observation window 8, measuring chi 9, described spotting needle pipe-in-pipe 3 is axial Upper end is provided with the opening of cavity and the ft connection making spotting needle pipe-in-pipe 3, and spotting needle pipe-in-pipe 3 lower axial end is provided with for point sample The perforate that syringe needle 2 passes, is provided with screw thread outside spotting needle pipe-in-pipe 3, it is internal that point sample needle tubing 1 is arranged on spotting needle pipe-in-pipe 3, point Sample syringe needle 2, through the perforate of point sample needle tubing sleeve pipe 3 lower end, is provided with inside support ring 4 and spotting needle pipe-in-pipe 3 outside screw phase The screw thread joined, support ring 4 is arranged on outside spotting needle pipe-in-pipe 3, and support ring 4 spins in screw thread with spotting needle pipe-in-pipe 3, supports Connect outside ring 4 and have support arm 5, be perpendicular to support arm 5 on support arm 5 direction away from support ring 4 end with leg 6 upper end even Connecing, be connected with the gimbal lever 7 being perpendicular to leg 6 lower end on leg 6 direction, spotting needle pipe-in-pipe 3 is provided with observation window 8 and measures Chi 9.When preparing point sample, by observation window 8 with measure chi 9 and accurately extract certain liquid to be detected.
Spotting needle pipe-in-pipe 3, support ring 4, support arm 5, leg 6, the preferred stainless steel material of the gimbal lever 7 are made, support ring 4, can be welding between support arm 5, leg 6, the gimbal lever 7, rivet or be mechanically connected.Observation window 8 is by glass material or transparent Engineering plastics are made.It is internal that point sample needle tubing 1 uses adhesive to be fixed on spotting needle pipe-in-pipe 3.
Support ring 4 with support arm 5 at grade, is preferably provided with two support arms 5, and two support arms are with support ring 4 Central point.
Support ring 4 is arranged in spotting needle pipe-in-pipe 3, when fixing point sample needle tubing sleeve pipe 3, by rotating support ring 4, point Relative distance between sample syringe needle 2 and the gimbal lever 7 changes, and during point sample, the gimbal lever 7 and thin layer chromatography board are in same In plane, rotate support ring 4 and can control the spacing of point sample syringe needle 2 and thin layer chromatography board, when rotating support ring 4, make support When ring 4 is away from point sample syringe needle 2, Distance Shortened between point sample syringe needle 2 and thin layer chromatography board, on the contrary distance increases;Or by band The sampling needle for thin-layer chromatography of foot is placed on the table, and thin layer chromatography board is placed on below point sample syringe needle 2, thin layer chromatography board and the gimbal lever 7 in approximately the same plane, rotate point sample needle tubing sleeve pipe 3 rise or fall, point sample syringe needle 2 rise with spotting needle pipe-in-pipe 3 or under Fall, thus regulate the spacing of point sample syringe needle 2 and thin layer chromatography board.Support ring 4 spins removable with spotting needle pipe-in-pipe 3 for screw thread Unload structure.Screw thread spins the distance that structure can be precisely controlled between point sample syringe needle 2 and thin layer chromatography board, ensures that point sample effect is Good, formed structure spotting needle can be played firm supporting role by support ring 4, support arm 5, leg 6, the gimbal lever 7, the most anti- Stop sample is shaken, point sample dynamics is uneven.
The foregoing describe embodiment of the present utility model, but described content only readily appreciates this utility model technology Scheme and the embodiment that uses, skilled person will appreciate that of the industry, this utility model is not restricted to the described embodiments, On the premise of without departing from this utility model spirit and scope, this utility model also has various changes and modifications, these changes In the range of both falling within claimed this utility model with improvement.This utility model claims scope by appended claim Book and equivalent thereof define.

Claims (3)

1. a sampling needle for thin-layer chromatography for band leg, including point sample needle tubing (1), point sample syringe needle (2), spotting needle pipe-in-pipe (3), Support ring (4), support arm (5), leg (6), the gimbal lever (7), observation window (8), measure chi (9), it is characterised in that: described point The axial upper end of sample needle tubing sleeve pipe (3) is provided with the opening of cavity and the ft connection making spotting needle pipe-in-pipe (3), spotting needle pipe box Pipe (3) lower axial end is provided with the perforate passed for point sample syringe needle (2), and spotting needle pipe-in-pipe (3) outside is provided with screw thread, point sample needle tubing (1) being arranged on spotting needle pipe-in-pipe (3) internal, point sample syringe needle (2) is through the perforate of point sample needle tubing sleeve pipe (3) lower end, support ring (4) inner side is provided with the screw thread matched with spotting needle pipe-in-pipe (3) outside screw, and support ring (4) is arranged on spotting needle pipe-in-pipe (3) outside, support ring (4) spins in screw thread with spotting needle pipe-in-pipe (3), and support ring (4) outside connects support arm (5), It is perpendicular to holding away from support ring (4) of support arm (5) on support arm (5) direction be connected with leg (6) upper end, is perpendicular to leg (6) on direction, leg (6) lower end is connected with the gimbal lever (7), and spotting needle pipe-in-pipe (3) is provided with observation window (8) and measures chi (9).
The sampling needle for thin-layer chromatography of a kind of band leg the most according to claim 1, it is characterised in that: described support ring (4) with support arm (5) at grade.
The sampling needle for thin-layer chromatography of a kind of band leg the most according to claim 1, it is characterised in that: described support ring (4) it is arranged in spotting needle pipe-in-pipe (3), can dismantle.
CN201620785327.9U 2016-07-25 2016-07-25 A kind of sampling needle for thin-layer chromatography of band leg Expired - Fee Related CN205809020U (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
CN201620785327.9U CN205809020U (en) 2016-07-25 2016-07-25 A kind of sampling needle for thin-layer chromatography of band leg

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105954458A (en) * 2016-07-25 2016-09-21 哈尔滨理工大学 Thin-layer chromatography sample application needle with supporting feet
CN110082473A (en) * 2019-05-16 2019-08-02 广州市鹭江远科技有限公司 A kind of spot sample device for aflatoxins detection based on thin layer chromatography

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105954458A (en) * 2016-07-25 2016-09-21 哈尔滨理工大学 Thin-layer chromatography sample application needle with supporting feet
CN105954458B (en) * 2016-07-25 2018-05-04 哈尔滨理工大学 A kind of sampling needle for thin-layer chromatography with leg
CN110082473A (en) * 2019-05-16 2019-08-02 广州市鹭江远科技有限公司 A kind of spot sample device for aflatoxins detection based on thin layer chromatography

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20161214

Termination date: 20170725

CF01 Termination of patent right due to non-payment of annual fee