CN205774956U - Integrated hollow fiber ceramic membrane device for spinning - Google Patents

Integrated hollow fiber ceramic membrane device for spinning Download PDF

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Publication number
CN205774956U
CN205774956U CN201620484220.0U CN201620484220U CN205774956U CN 205774956 U CN205774956 U CN 205774956U CN 201620484220 U CN201620484220 U CN 201620484220U CN 205774956 U CN205774956 U CN 205774956U
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China
Prior art keywords
spinning
hollow fiber
ceramic membrane
fiber ceramic
spinning head
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CN201620484220.0U
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Chinese (zh)
Inventor
闫啸
王松雪
王建明
陈顺权
苗晶
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Guangdong Carbon Neutralization Research Institute Shaoguan
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Shenzhen Institute of Advanced Technology of CAS
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Abstract

A kind of integrated hollow fiber ceramic membrane device for spinning, including: removable steelframe;Material liquid tank is arranged on removable steelframe, and it is provided with the first agitator, primary heater and the first Pressure gauge;Top offers the first charging aperture and the first air inlet, and bottom is provided with filter;Core flow container is arranged on removable steelframe, and it is provided with the second agitator, secondary heater and the second Pressure gauge, and top offers the second charging aperture and the second air inlet, and bottom is provided with effusion meter;Spinning head connects with material liquid tank and core flow container respectively;Coagulating tank is positioned at the bottom of removable steelframe, offers outlet bottom it;Fixing device is arranged between spinning head and coagulating tank, for regulating the air gap distance between spinning head and coagulating tank liquid level;Wrapping wire unit is arranged in coagulating tank, and is connected with spinning head by godet roller, and it includes two apart from adjustable synchronization wire wrapping wheel.Above-mentioned integrated hollow fiber ceramic membrane device for spinning easy can prepare straight film silk rapidly.

Description

Integrated hollow fiber ceramic membrane device for spinning
Technical field
This utility model relates to ceramic membrane device field, spins particularly to a kind of integrated hollow fiber ceramic membrane Silk device.
Background technology
It is high that ceramic membrane has mechanical strength, and chemical stability is good, and organic solvent-resistant is high temperature resistant, antibiosis materialization The advantages such as corrode, resistance to cleaning.Hollow fiber ceramic membrane has had again simple in construction concurrently, and unit volume filling is close Degree height, effective film area is big, the features such as pressure stability is high, device miniaturization.Hollow fiber ceramic membrane group Part takes up an area little, and energy consumption is low, and investment return is obvious, and prospect is the most wide.
The technology of preparing of the most conventional hollow fiber ceramic membrane mainly has dry-wet spinning, molte-salt synthesis spinning With reaction bonded forming technique etc..Wherein dry-wet spinning is with its low cost, and instrument size is flexible according to yield Controlled, by laboratory, the favor of factory.Hollow fiber ceramic membrane and the spinning side of doughnut organic membrane Method is essentially identical, therefore, market usually utilizes the spinning equipment system of common doughnut organic membrane Standby hollow fiber ceramic membrane.The spinning equipment of universal doughnut organic membrane cannot obtain directly easily and fast Film silk.
Utility model content
Based on this, it is necessary to provide a kind of integrated hollow fiber that easy can prepare straight film silk rapidly Ceramic membrane device for spinning.
A kind of integrated hollow fiber ceramic membrane device for spinning, including:
Removable steelframe;
Material liquid tank, is arranged on described removable steelframe, is used for holding casting solution, and described material liquid tank is arranged There are the first agitator, primary heater and the first Pressure gauge;The top of described material liquid tank offers the first charging Mouth and the first air inlet, the bottom of described material liquid tank is provided with filter;
Core flow container, is arranged on described removable steelframe, is used for holding core liquid, described core flow container is provided with Second agitator, secondary heater and the second Pressure gauge, the top of described core flow container offers the second charging aperture With the second air inlet, the bottom of described core flow container is provided with effusion meter;
Spinning head, connects with described material liquid tank and described core flow container respectively;
Coagulating tank, is positioned at the bottom of described removable steelframe, offers outlet bottom described coagulating tank;
Fixing device, is arranged between described spinning head and described coagulating tank, is used for regulating described spinning head And the air gap distance between described coagulating tank liquid level;And
Wrapping wire unit, is arranged in described coagulating tank, and is connected with described spinning head by godet roller, institute Stating wrapping wire unit and include two wire wrapping wheels synchronized, the distance between two described wire wrapping wheels is adjustable.
In one embodiment, described wire wrapping wheel is scalable wire wrapping wheel.
In one embodiment, described filter is disc-type filter.
In one embodiment, described spinning head is wet method spinning head.
In one embodiment, described primary heater and described secondary heater are equipped with thermostat.
In one embodiment, the bottom of described removable steelframe is provided with self-locking pulley.
In above-mentioned hollow fiber ceramic membrane device for spinning, this equipment by spinning, solidify, receive silk, immersion, Stretching, be dried etc. preparation technology be integrated in one in formula equipment, it is possible to prepare straight hollow fiber ceramic membrane, Improve the utilizability of the hollow fiber ceramic membrane prepared.
Accompanying drawing explanation
Fig. 1 is the structural representation of the integrated hollow fiber ceramic membrane device for spinning of an embodiment.
Detailed description of the invention
Understandable for enabling above-mentioned purpose of the present utility model, feature and advantage to become apparent from, below in conjunction with attached Detailed description of the invention of the present utility model is described in detail by figure.Elaborate much have in the following description Body details is so that fully understanding this utility model.But this utility model can be retouched at this to be much different from The alternate manner stated is implemented, and those skilled in the art can be in the case of this utility model intension Doing similar improvement, therefore this utility model is not limited by following public being embodied as.
Referring to Fig. 1, the integrated hollow fiber ceramic membrane device for spinning 100 of an embodiment, including moving Dynamic steelframe 10, material liquid tank 20, core flow container 30, spinning head 40, coagulating tank 50, fixing device 60 and around Silk unit 70.Material liquid tank 20, core flow container 30, spinning head 40, coagulating tank 50, fixing device 60 and around Silk unit 70 is arranged on removable steelframe 10.
Removable steelframe 10 is welded by stainless steel material.In one embodiment, removable steelframe 10 Bottom, equipped with band self-locking pulley 110, can be moved as required to different places.
In one embodiment, material liquid tank 20, substantially in cylindrical shape, is arranged on removable steelframe 10, For holding casting solution.The first agitator 210, primary heater 220 and first it is provided with on material liquid tank 20 Pressure gauge 230.The top of material liquid tank 20 offers the first charging aperture 240 and the first air inlet 250.Casting film Liquid adds to material liquid tank 20 from the first charging aperture 240, by the first agitator 210 by casting solution stirring all Even.By primary heater 220, casting solution is heated.In one embodiment, primary heater 220 On be provided with thermostat (not shown), the temperature in conveniently regulating and controlling material liquid tank 20.Enter by first QI KOU 250 is filled with nitrogen or other gases at high pressure, and the force value of material liquid tank 20 monitored by the first Pressure gauge 230, Thus regulate and control.To form high-pressure delivery casting solution.On the pipeline of the bottom of material liquid tank 20, valve is set 260 and filter 270, open or close valve 260 to control conveying and the disconnection of casting solution, by filtering Casting solution is filtered by device 270, it is to avoid large granular materials enters in spinning head 40, in one embodiment, Filter 270 is disc-type filter, and the screen material of disc-type filter can be metal or nonwoven Cloth, is filtered by in-depth filtration unit form, good filtration effect.
Core flow container 30, substantially in cylindrical shape, is arranged on removable steelframe 10, is used for holding core liquid.Core The second agitator 310, secondary heater 320 and the second Pressure gauge 330 it is provided with on flow container 30.Core flow container The top of 30 offers the second charging aperture 340 and the second air inlet 350, on the pipeline of the bottom of core flow container 30 It is provided with valve 360 and effusion meter 370, opens or closes valve 360 to control conveying and the disconnection of core liquid. Core liquid adds to core flow container 30 from the second charging aperture 340, by the second agitator 310 by the stirring of core liquid all Even.By secondary heater 320, core liquid is heated, from the second air inlet 350 be filled with nitrogen or other Gases at high pressure, are monitored the force value of core flow container 30, thus carry out pressure controlling by the second Pressure gauge 330, To form high-pressure delivery core liquid.The flow velocity of core liquid can be controlled by the effusion meter 370 bottom core flow container 30 System.
Spinning head 40 is arranged on below material liquid tank 20 and core flow container 30, by pipeline and material liquid tank 20 and Core flow container 30 connects.In one embodiment, spinning head 40 is wet method spinning head.
Coagulating tank 50 is fixed on the bottom of removable steelframe 10, offers outlet bottom coagulating tank 50 510。
Fixing device 60 is arranged between spinning head 40 and coagulating tank 50, is used for regulating spinning head 40 He Air gap distance between coagulating tank 50 liquid level.
Wrapping wire unit 70 is arranged in coagulating tank 60, and is connected with spinning head 40 by godet roller 710, Wrapping wire unit 70 also includes two wire wrapping wheels synchronized 720, and the distance between two wire wrapping wheels 720 is adjustable. Two wire wrapping wheel 720 transmissions synchronized are accurate, fricton-tight during work, have constant gear ratio, thus pass Dynamic steady.In one embodiment, wire wrapping wheel 720 is scalable wire wrapping wheel.
In process of production, casting solution adds from the first charging aperture 240, and core liquid adds from the second charging aperture 340 Enter, respectively casting solution and core liquid can be stirred all by first agitator the 210, second agitator 310 Even, carry out temperature control by primary heater 220 and secondary heater 320, adjusted by fixing device 60 Air gap distance between joint spinning head 40 and coagulating tank 50 liquid level, carries out spinning after feed liquid deaeration, Film silk enters coagulating tank 50, enters two wire wrapping wheels 720 by godet roller 710, completes the collection of film silk, Film silk is placed a period of time in coagulating tank 50, makes inversion of phases carry out completely, will by outlet 510 Coagulation bath bleeds off, and makes film silk be dried in atmosphere, is cut off from two ends by dried film silk and has just obtained directly The filming film silk of hollow fiber ceramic membrane, be sintered just can get straight hollow fiber ceramic membrane by film silk.
Embodiment described above only have expressed several embodiments of the present utility model, its describe more concrete and In detail, but therefore can not be interpreted as the restriction to this utility model the scope of the claims.It should be pointed out that, For the person of ordinary skill of the art, without departing from the concept of the premise utility, it is also possible to Making some deformation and improvement, these broadly fall into protection domain of the present utility model.Therefore, this utility model The protection domain of patent should be as the criterion with claims.

Claims (6)

1. an integrated hollow fiber ceramic membrane device for spinning, it is characterised in that including:
Removable steelframe;
Material liquid tank, is arranged on described removable steelframe, is used for holding casting solution, and described material liquid tank is arranged There are the first agitator, primary heater and the first Pressure gauge;The top of described material liquid tank offers the first charging Mouth and the first air inlet, the bottom of described material liquid tank is provided with filter;
Core flow container, is arranged on described removable steelframe, is used for holding core liquid, described core flow container is provided with Second agitator, secondary heater and the second Pressure gauge, the top of described core flow container offers the second charging aperture With the second air inlet, the bottom of described core flow container is provided with effusion meter;
Spinning head, connects with described material liquid tank and described core flow container respectively;
Coagulating tank, is positioned at the bottom of described removable steelframe, and the bottom of described coagulating tank offers water outlet Mouthful;
Fixing device, is arranged between described spinning head and described coagulating tank, is used for regulating described spinning head And the air gap distance between described coagulating tank liquid level;And
Wrapping wire unit, is arranged in described coagulating tank, and is connected with described spinning head by godet roller, institute Stating wrapping wire unit and include two wire wrapping wheels synchronized, the distance between two described wire wrapping wheels is adjustable.
Integrated hollow fiber ceramic membrane device for spinning the most according to claim 1, it is characterised in that Described wire wrapping wheel is scalable wire wrapping wheel.
Integrated hollow fiber ceramic membrane device for spinning the most according to claim 1, it is characterised in that Described filter is disc-type filter.
Integrated hollow fiber ceramic membrane device for spinning the most according to claim 1, it is characterised in that Described spinning head is wet method spinning head.
Integrated hollow fiber ceramic membrane device for spinning the most according to claim 1, it is characterised in that Described primary heater and described secondary heater are equipped with thermostat.
Integrated hollow fiber ceramic membrane device for spinning the most according to claim 1, it is characterised in that The bottom of described removable steelframe is provided with self-locking pulley.
CN201620484220.0U 2016-05-25 2016-05-25 Integrated hollow fiber ceramic membrane device for spinning Active CN205774956U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201620484220.0U CN205774956U (en) 2016-05-25 2016-05-25 Integrated hollow fiber ceramic membrane device for spinning

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201620484220.0U CN205774956U (en) 2016-05-25 2016-05-25 Integrated hollow fiber ceramic membrane device for spinning

Publications (1)

Publication Number Publication Date
CN205774956U true CN205774956U (en) 2016-12-07

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201620484220.0U Active CN205774956U (en) 2016-05-25 2016-05-25 Integrated hollow fiber ceramic membrane device for spinning

Country Status (1)

Country Link
CN (1) CN205774956U (en)

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Effective date of registration: 20230103

Address after: 512029 Building 42, Huangshaping Innovation Park, Guanshaocheng Phase I, Wujiang District, Shaoguan City, Guangdong Province

Patentee after: Guangdong Carbon Neutralization Research Institute (Shaoguan)

Address before: 1068 No. 518055 Guangdong city in Shenzhen Province, Nanshan District City Xili University School Avenue

Patentee before: SHENZHEN INSTITUTES OF ADVANCED TECHNOLOGY