CN205774335U - A kind of small size coal high-temperature quick liquefaction reaction unit - Google Patents
A kind of small size coal high-temperature quick liquefaction reaction unit Download PDFInfo
- Publication number
- CN205774335U CN205774335U CN201620494642.6U CN201620494642U CN205774335U CN 205774335 U CN205774335 U CN 205774335U CN 201620494642 U CN201620494642 U CN 201620494642U CN 205774335 U CN205774335 U CN 205774335U
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- China
- Prior art keywords
- aeration tank
- reaction vessel
- temperature
- small size
- stop valve
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- Expired - Fee Related
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- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Abstract
This utility model relates to a kind of small size coal high-temperature quick liquefaction reaction unit, concrete technical scheme is, including gas cylinder, aeration tank, resonance agitator, tubular reaction vessel, high temperature heat source body and numeral temperature control instrument, Pressure gauge P1 and stop valve V1 it is provided with between gas cylinder and aeration tank, Pressure gauge P2 and stop valve V2 is set on aeration tank, the inflation/deflation of aeration tank can be realized by stop valve V1 and V2, described tubular reaction vessel is placed among described high temperature heat source body, can be realized and the resonance stirring of described tubular reaction vessel by resonance agitator, the reacting gas coming from described aeration tank can enter described tubular reaction vessel by stop valve V3, the temperature of described high temperature heat source body is measured by described numeral temperature control instrument.This utility model reaction unit, parts the most in acquisition, simple in construction, easy to operate, and overall price is compared the most much lower with the like product sold on market, and be applicable to the reaction between plurality of raw materials gas and liquid.
Description
Technical field
This utility model belongs to gas-liquid reaction equipment, particularly relates to a kind of small size coal high-temperature quick liquefaction reaction dress
Put.
Background technology
Hydrogenation reactor is a very important equipment in Organic Chemistry Laboratory and actual production process, is possible not only to
As the container of hydrogenation reaction, and can also be used for liquids and gases and need well-mixed occasion.Have in terms of chemical pharmacy
Purposes widely, can be as the infrastructure device of product development, organic chemical and pharmaceuticals research, it may also be used for quantitatively divide
The activity of catalyst in analysis industrial process.But on market, institute's product sold is not too expensive, it is simply that its purposes is less.
Summary of the invention
In order to solve above-mentioned technical problem, it is anti-that this utility model provides a kind of homemade small size coal high-temperature quick liquefaction
The device, concrete technical scheme is answered to be, a kind of small size coal high-temperature quick liquefaction reaction unit, it is characterised in that include gas cylinder, fill
Gas tank, resonance agitator, tubular reaction vessel, high-temperature salt bath and numeral temperature control instrument, be provided with Pressure gauge between gas cylinder and aeration tank
P1 and stop valve V1, aeration tank arranges Pressure gauge P2 and stop valve V2, can realize aeration tank by stop valve V1 and V2
Inflation/deflation, described tubular reaction vessel is placed among described high-temperature salt bath, can realize anti-with described tubular type by resonance agitator
Answering still resonance stirring, the reacting gas coming from described aeration tank can enter described tubular reaction vessel, institute by stop valve V3
The temperature stating high-temperature salt bath is measured by described numeral temperature control instrument.
Further, described high temperature heat source body is high-temperature salt bath.
Further, placing vibrating mass in described tubular reaction vessel, described vibrating mass can be at resonance agitator
Under effect, move up and down in described tubular reaction vessel.
Further, the volume of described tubular reaction vessel is 15～30mL, and the volume of described vibrating mass is described tubular type
0.1～0.3 times of reactor volume.
Further, described vibrating mass be shaped as bar-shaped or spherical.
This utility model one small size coal high-temperature quick liquefaction reaction unit, parts are easy to obtain, simple in construction,
Easy to operate, and overall price is compared the most much lower with the like product sold on market, is applicable to multiple former
Reaction between material gas and liquid.
Accompanying drawing explanation
Fig. 1 is this utility model one small size coal high-temperature quick liquefaction reaction unit schematic diagram.
Accompanying drawing acceptance of the bid note be described below: 1 gas cylinder, 2 aeration tanks, 3 resonance agitators, 4 tubular reaction vessels, 5 High Temperature Salt Bath Furnace,
6 numeral temperature control instruments.
Detailed description of the invention
This utility model provides a kind of homemade small size coal high-temperature quick liquefaction reaction unit, concrete technical scheme
For, a kind of slurry bed system resonance stirring reaction unit, it is characterised in that include that gas cylinder 1, aeration tank 2, resonance agitator 3, tubular type are anti-
Answer still 4, high temperature heat source body and numeral temperature control instrument 6, be provided with Pressure gauge P1 and stop valve V1 between gas cylinder 1 and aeration tank 2, inflation
Pressure gauge P2 and stop valve V2 is set on case 2, the inflation/deflation of aeration tank 2, described tubular type can be realized by stop valve V1 and V2
Reactor 4 is placed among described high temperature heat source body, can realize stirring with the resonance of described tubular reaction vessel 4 by resonance agitator 3
Mixing, the reacting gas coming from described aeration tank 2 can enter described tubular reaction vessel 4, described high-temperature hot by stop valve V3
The temperature of source body is measured by described numeral temperature control instrument 6.
Further, described high temperature heat source body is high-temperature salt bath 5.
Further, placing vibrating mass in described tubular reaction vessel 4, described vibrating mass can be in described resonance stirring
Under the effect of device 3, move up and down in described tubular reaction vessel 4.
A kind of preferably technical scheme is that the volume of described tubular reaction vessel 4 is 15～30mL, the body of described vibrating mass
Amass 0.1～0.3 times for described tubular reaction vessel 4 volume.
In above-described embodiment, described vibrating mass is rod iron or steel ball.
The using method that this utility model device is detailed is as follows.
1. take a certain amount of reactant liquor and a certain amount of catalyst, add in tubular reaction vessel 4, put into vibrating mass, close
Seal described tubular reaction vessel 4, first close stop valve V2, the most successively stop valve V3, V1 on aeration tank 2, open described gas cylinder
1, replace the air in tubular reaction vessel 4 with the reacting gas in described gas cylinder 1, be repeated 2 times ~ 3 times, then by tubular reaction vessel
In 4, pressure is adjusted to the setting value of reaction.
2. turn on the power, connect numeral temperature control instrument 6 and high-temperature salt bath 5 power supply, preheat described High Temperature Salt Bath Furnace 5.Treat high temperature
When in salt bath furnace 5, the salt temperature of solid-state rises to setting value, tubular reaction vessel 4 is rapidly inserted in described High Temperature Salt Bath Furnace 5, so
After open described resonance stirred reactor 3 and switch, and described resonance stirred reactor 3 voltage is transferred to desired value, reacts.
3., at the end of reaction, first close described resonance stirred reactor 3 and switch, more described tubular reaction vessel 4 is withdrawn institute
State High Temperature Salt Bath Furnace 5.Then described tubular reaction vessel 4 is placed in cold water so that it is be rapidly cooled to room temperature.
Close stop valve V1, V3 the most successively, slowly open stop valve V2 on aeration tank 2, make described tubular reaction vessel 4 intrinsic pressure
Power drops to normal pressure.
5. product is transferred in special container from described tubular reaction vessel 4, then by centrifugal for reaction afterproduct point
From, pipette the supernatant in color comparison tube, carry out chromatography.
This utility model device is applicable to the reaction between plurality of raw materials gas and liquid, is particularly adapted to institution of higher learning
Or the Routine Test Lab of R&D institution and coal liquefaction factory carries out research or the teaching use of coal high-temperature quick liquefaction.
Claims (5)
1. a small size coal high-temperature quick liquefaction reaction unit, it is characterised in that include gas cylinder (1), aeration tank (2), resonance
Agitator (3), tubular reaction vessel (4), high temperature heat source body and numeral temperature control instrument (6), arranged between gas cylinder (1) and aeration tank (2)
There is Pressure gauge P1 and stop valve V1, aeration tank (2) arranges Pressure gauge P2 and stop valve V2, can be real by stop valve V1 and V2
The inflation/deflation of existing aeration tank (2), described tubular reaction vessel (4) is placed among described high temperature heat source body, by resonance agitator (3)
Can realize and described tubular reaction vessel (4) resonance stirring, the reacting gas coming from described aeration tank (2) can be by cut-off
Valve V3 enters described tubular reaction vessel (4), and the temperature of described high temperature heat source body is measured by described numeral temperature control instrument (6).
Small size coal high-temperature quick liquefaction reaction unit the most according to claim 1, it is characterised in that described high temperature heat source
Body is high-temperature salt bath (5).
Small size coal high-temperature quick liquefaction reaction unit the most according to claim 1 and 2, it is characterised in that described tubular type
Placing vibrating mass in reactor (4), described vibrating mass can be under the effect of described resonance agitator (3), at described pipe
Formula reactor moves up and down in (4).
Small size coal high-temperature quick liquefaction reaction unit the most according to claim 3, it is characterised in that described pipe reaction
The volume of still (4) is 15～30mL, and the volume of described vibrating mass is 0.1～0.3 times of described tubular reaction vessel (4) volume.
Small size coal high-temperature quick liquefaction reaction unit the most according to claim 3, it is characterised in that described vibrating mass
Be shaped as bar-shaped or spherical.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620494642.6U CN205774335U (en) | 2016-05-27 | 2016-05-27 | A kind of small size coal high-temperature quick liquefaction reaction unit |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620494642.6U CN205774335U (en) | 2016-05-27 | 2016-05-27 | A kind of small size coal high-temperature quick liquefaction reaction unit |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205774335U true CN205774335U (en) | 2016-12-07 |
Family
ID=57407082
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620494642.6U Expired - Fee Related CN205774335U (en) | 2016-05-27 | 2016-05-27 | A kind of small size coal high-temperature quick liquefaction reaction unit |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205774335U (en) |
-
2016
- 2016-05-27 CN CN201620494642.6U patent/CN205774335U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20161207 Termination date: 20180527 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |