CN205774238U - A kind of remove impurity purification system of vitamin C glucoside - Google Patents
A kind of remove impurity purification system of vitamin C glucoside Download PDFInfo
- Publication number
- CN205774238U CN205774238U CN201620466825.7U CN201620466825U CN205774238U CN 205774238 U CN205774238 U CN 205774238U CN 201620466825 U CN201620466825 U CN 201620466825U CN 205774238 U CN205774238 U CN 205774238U
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- Prior art keywords
- pipeline
- permeate
- ultrafilter membrane
- membrane group
- glucoside
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- 239000012535 impurity Substances 0.000 title claims abstract description 27
- 229930182478 glucoside Natural products 0.000 title claims abstract description 23
- 238000000746 purification Methods 0.000 title claims abstract description 23
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Natural products OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 title claims abstract description 22
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 title claims abstract description 20
- 229930003268 Vitamin C Natural products 0.000 title claims abstract description 20
- 235000019154 vitamin C Nutrition 0.000 title claims abstract description 20
- 239000011718 vitamin C Substances 0.000 title claims abstract description 20
- -1 vitamin C glucoside Chemical class 0.000 title claims abstract description 20
- 239000012528 membrane Substances 0.000 claims abstract description 42
- 239000012466 permeate Substances 0.000 claims abstract description 37
- 239000007788 liquid Substances 0.000 claims abstract description 22
- 238000001802 infusion Methods 0.000 claims abstract description 14
- 230000008676 import Effects 0.000 claims abstract description 9
- MLSJBGYKDYSOAE-DCWMUDTNSA-N L-Ascorbic acid-2-glucoside Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O[C@@H]2[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O2)O)=C1O MLSJBGYKDYSOAE-DCWMUDTNSA-N 0.000 abstract description 9
- 239000000047 product Substances 0.000 abstract description 7
- 150000004676 glycans Chemical class 0.000 abstract description 3
- 239000005017 polysaccharide Substances 0.000 abstract description 3
- 229920001282 polysaccharide Polymers 0.000 abstract description 3
- 102000004169 proteins and genes Human genes 0.000 abstract description 3
- 108090000623 proteins and genes Proteins 0.000 abstract description 3
- 230000015572 biosynthetic process Effects 0.000 abstract description 2
- 239000000084 colloidal system Substances 0.000 abstract description 2
- 238000003786 synthesis reaction Methods 0.000 abstract description 2
- 238000000108 ultra-filtration Methods 0.000 abstract description 2
- 239000000243 solution Substances 0.000 description 20
- 238000000034 method Methods 0.000 description 6
- 230000000694 effects Effects 0.000 description 3
- 150000008131 glucosides Chemical class 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 230000008901 benefit Effects 0.000 description 2
- 239000008367 deionised water Substances 0.000 description 2
- 229910021641 deionized water Inorganic materials 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 241001597008 Nomeidae Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 235000010323 ascorbic acid Nutrition 0.000 description 1
- 239000011668 ascorbic acid Substances 0.000 description 1
- 229960005070 ascorbic acid Drugs 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000000385 dialysis solution Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 235000014593 oils and fats Nutrition 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
Abstract
This utility model discloses the remove impurity purification system of a kind of vitamin C glucoside, it batch can including being provided with temperature controller, and a circulation purifies pipeline, and a permeate gets rid of pipeline；Circulation purifies pipeline, it includes infusion pump, cartridge filter, booster pump and the ultrafilter membrane group being sequentially connected, ultrafilter membrane group has the import being connected with booster pump and two corresponding concentrated solution part, the concentrated solution outlet of permeate part and permeate outlets respectively, described infusion pump is connected with the liquid outlet of batch can, and the concentrated solution outlet of ultrafilter membrane group is connected with the inlet of batch can；Permeate gets rid of pipeline, and it is a pipeline, and this pipeline one section exports with the permeate of ultrafilter membrane group and is connected, and the other end is permeate outlet.This utility model uses antipollution high temperature ultrafiltration apparatus, removes the impurity such as the high molecular weight protein in AA2G synthesis liquid, polysaccharide, colloid, is carried product, improve the concentration of product simultaneously, substantially increase the quality of product.
Description
Technical field
This utility model relates to the remove impurity purification system of a kind of vitamin C glucoside, divides by International Patent Classification (IPC) (IPC) and belongs to raw element C glucoside purification technique field.
Background technology
Vitamin C glucoside, has another name called ascorbic acid glucoside, is a kind of ascorbic derivant.Trade name is referred to as AA2G, and it possesses the formulation stability of brilliance, it is possible to inherently suppression variable color and degraded, remains all biological activity, to reach to highlight effect of whitening, resisting ultraviolet irradiation and defying age simultaneously.In the production process of AA2G, process for separating and purifying difficulty is relatively big, uses existing resin absorption technique, and the waste liquid of generation is more, and production cost is higher；In the most existing purifying technique, AA2G viscosity is high, the problem of membrane separation difficulty.
Therefore on the remove impurity purification system of existing raw element C glucoside, reach while how reducing waste liquid amount low cost and refining effect good etc. be current vitamin C glucoside remove impurity purification system structure in one of the important topic of research staff.
Utility model content
For the deficiencies in the prior art, this utility model provides the remove impurity purification system of a kind of vitamin C glucoside, and it mainly solves existing vitamin C glucoside and purifies the technical problem that production cost is higher.
For reaching above-mentioned purpose, this utility model is achieved through the following technical solutions:
A kind of remove impurity purification system of vitamin C glucoside, it batch can including being provided with temperature controller, a circulation purifies pipeline, and a permeate gets rid of pipeline, wherein:
Batch can, it is the tank body with liquid outlet and inlet；
Circulation purifies pipeline, it includes infusion pump, cartridge filter, booster pump and the ultrafilter membrane group being sequentially connected, wherein ultrafilter membrane group has the import being connected with booster pump and two corresponding concentrated solution part, the concentrated solution outlet of permeate part and permeate outlets respectively, described infusion pump is connected with the liquid outlet of batch can, the concentrated solution outlet of ultrafilter membrane group is connected with the inlet of batch can, and described circulation purifies and is additionally provided with butterfly valve and relief valve on pipeline；
Permeate gets rid of pipeline, and it is a pipeline, and this pipeline one section exports with the permeate of ultrafilter membrane group and is connected, and the other end is permeate outlet, and this permeate eliminating pipeline is additionally provided with butterfly valve and relief valve.
Further, it is respectively arranged with pressure transducer between described cartridge filter and infusion pump, booster pump.
Further, it is respectively arranged with pressure transducer at the import of described ultrafilter membrane group and concentrated solution outlet.
Further, it is provided with heat exchanger and flow transducer between concentrated solution outlet and the batch can of described ultrafilter membrane group.
Further, described cartridge filter is 5 microns of cartridge filters.
Further, described ultrafilter membrane group is 5000 molecular weight for retaining aperture.
Further, described permeate is got rid of pipeline and is also included a flow transducer.
Further, this remove impurity purification system also includes a feedback pipe, this feedback pipe includes switch valve and the feedback valve being dimly connected, and this feedback pipe one end is connected with the input of booster pump, and this feedback pipe other end purifies the concentrated solution outlet of ultrafilter membrane group in pipeline and is connected with circulation.
Further, described booster pump quantity is two, and is serially connected between two booster pumps.
Compared with prior art, advantage of the present utility model:
This utility model uses antipollution high temperature ultrafiltration apparatus, removes the impurity such as the high molecular weight protein in AA2G synthesis liquid, polysaccharide, colloid, is carried product, improve the concentration of product simultaneously, substantially increase the quality of product.
Accompanying drawing explanation
Fig. 1 is this utility model embodiment one structural representation；
Fig. 2 is this utility model embodiment two structural representation.
Detailed description of the invention
Clearer for the purpose making this utility model implement, technical scheme and advantage, below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is further described in more detail.In the accompanying drawings, the most same or similar label represents same or similar element or has the element of same or like function.Described embodiment is a part of embodiment of the present invention rather than whole embodiments.The embodiment described below with reference to accompanying drawing is exemplary, it is intended to is used for explaining the present invention, and is not considered as limiting the invention.Based on the embodiment in the present invention, the every other embodiment that those of ordinary skill in the art are obtained under not making creative work premise, broadly fall into the scope of protection of the invention.
In the description of the technical program, it will be appreciated that, term " " center ", " longitudinally ", " laterally ", " front ", " afterwards ", " left ", " right ", " vertically ", " level ", " push up ", " end " " interior ", orientation or the position relationship of the instruction such as " outward " are based on orientation shown in the drawings or position relationship, it is for only for ease of the description present invention and simplifies description, rather than indicate or imply that the device of indication or element must have specific orientation, with specific azimuth configuration and operation, therefore it is not intended that limiting the scope of the invention, the utility model is described in further detail below in conjunction with the accompanying drawings:
Embodiment one: refer to shown in Fig. 1, the remove impurity purification system of a kind of vitamin C glucoside, it batch can A including being provided with temperature controller, a circulation purifies pipeline, and a permeate gets rid of pipeline.
Referring to shown in Fig. 1, batch can A, it is the tank body with liquid outlet and inlet.Specifically: on this batch can A, temperature controller is installed；The technical scheme more having a choosing is: the inlet of described batch can A is offered and can be added deionized water feed liquid is carried out dilute filling opening.
Refer to shown in Fig. 1, circulation purifies pipeline, it includes infusion pump P001, cartridge filter B, booster pump P002 and ultrafilter membrane group C being sequentially connected, wherein ultrafilter membrane group C has the import being connected with booster pump and two corresponding concentrated solution part, the concentrated solution outlet of permeate part and permeate outlets respectively, described infusion pump P001 is connected with the liquid outlet of batch can A, the concentrated solution outlet of ultrafilter membrane group C is connected with the inlet of batch can, and described circulation purifies and is additionally provided with butterfly valve V and relief valve on pipeline.Specifically: described cartridge filter B is 5 microns of cartridge filters, it is respectively arranged with pressure transducer PG between described cartridge filter B and infusion pump P001, booster pump P002, described ultrafilter membrane group C is 5000 molecular weight for retaining aperture, it is respectively arranged with pressure transducer PG at the import of described ultrafilter membrane group C and concentrated solution outlet, between concentrated solution outlet and the batch can of described ultrafilter membrane group C, is provided with heat exchanger and flow transducer FI；Wherein said pressure transducer PG can be Pressure gauge, and flow transducer FI can be flow meter.
Referring to shown in Fig. 1, permeate gets rid of pipeline, and it is a pipeline, this pipeline one section exports with the permeate of ultrafilter membrane group C and is connected, the other end is permeate outlet, and this permeate eliminating pipeline is additionally provided with butterfly valve V and relief valve, and described permeate is got rid of pipeline and also included a flow transducer FI.Specifically, described flow transducer FI is provided with flow meter.
Referring to shown in Fig. 1, the concrete remove impurity of said structure purifies principle and technique is as follows:
AA2G solution is placed in the batch can A being provided with temperature controller, and this batch can A just can carry out walking material when temperature reaches 50 ~ 60 degrees Celsius the speed of filtration (high temperature can improve) through being heated to, and first starts dehvery pump P001, restarts booster pump P002；Feed liquid is by dehvery pump P001(lift=30 ~ 40m) conveying, first pass through 5 microns of cartridge filter B and remove most suspended substances matter in feed liquid, ultrafilter membrane group C is played a protective role, is used for detecting blocking state of filter equipped with Pressure gauge before and after described cartridge filter B；Send into after feed liquid intensified pump P002 supercharging that high temperature resistant (common ultrafilter membrane heatproof is the highest 45 DEG C, high temperature resistance diaphragm is up to 75 DEG C) ultrafilter membrane group C in, in ultrafilter membrane group C, ultrafilter membrane retains aperture is 5000 molecular weight, liquid after ultrafilter membrane group C is divided into two parts, permeate is got rid of pipeline through permeate and is constantly discharged, concentrated solution constantly circulates in circulation purifies pipeline, concentrated liquid purifies pipeline in circulation and returns in batch can A, carrying out along with process, AA2G content in feed liquid constantly enters in permeate and discharges, macromolecular polysaccharide in feed liquid simultaneously, protein, the impurity such as oils and fats are constantly from being trapped, serve the effect of remove impurity；When walking material and proceeding to a certain degree, by adding deionized water in batch can A feed liquid, feed liquid is diluted, AA2G is made more to penetrate in dialysis solution, thus improve the product yield of AA2G, the scheme more having a choosing is: whole remove impurity purification system is provided with the temperature control system of control strict to temperature: when system temperature is too high, and heat exchanger logical cooling water cools down；(too low causing viscosity of sludge too high, cause fouling membrane, and filter efficiency declines) when temperature is too low, heat exchanger leads to steam and heats.
Embodiment two: refer to shown in Fig. 2, the remove impurity purification system of a kind of vitamin C glucoside, it batch can A including being provided with temperature controller, a circulation purifies pipeline, and a permeate gets rid of pipeline, and feedback pipe.
Referring to shown in Fig. 2, the batch can A of temperature controller, it is identical with embodiment one structure that a permeate gets rid of pipeline, is not repeating；Described circulation purifies pipeline and includes that (described booster pump quantity is two, and is serially connected between two booster pumps P002, P003 for infusion pump P001 being sequentially connected, cartridge filter B, booster pump.) and ultrafilter membrane group C, wherein ultrafilter membrane group C has the import being connected with booster pump P002 and two corresponding concentrated solution part, the concentrated solution outlet of permeate part and permeate outlets respectively, described infusion pump P001 is connected with the liquid outlet of batch can A, the concentrated solution outlet of ultrafilter membrane group C is connected with the inlet of batch can, and described circulation purifies and is additionally provided with butterfly valve V and relief valve on pipeline.Specifically: described cartridge filter B is 5 microns of cartridge filters, it is respectively arranged with pressure transducer between described cartridge filter B and infusion pump P001, booster pump P002, described ultrafilter membrane group C is 5000 molecular weight for retaining aperture, it is respectively arranged with pressure transducer at the import of described ultrafilter membrane group C and concentrated solution outlet, between concentrated solution outlet and the batch can A of described ultrafilter membrane group C, is provided with heat exchanger and flow transducer；Wherein said pressure transducer can be Pressure gauge, and flow transducer can be flow meter.
Referring to shown in Fig. 2, feedback pipe, it includes switch valve and the feedback valve LS being dimly connected, and this feedback pipe one end is connected with the input of booster pump P003, and this feedback pipe other end purifies the concentrated solution outlet of ultrafilter membrane group C in pipeline and is connected with circulation.
Described above, only utilize modification, change that the embodiment of this origination techniques content, any those skilled in the art use this creation to be done, all belong to the scope of the claims of this creation opinion, and be not limited to those disclosed embodiments.
Claims (9)
1. the remove impurity purification system of a vitamin C glucoside, it is characterised in that: it batch can including being provided with temperature controller, a circulation purifies pipeline, and a permeate gets rid of pipeline, wherein:
Batch can, it is the tank body with liquid outlet and inlet；
Circulation purifies pipeline, it includes infusion pump, cartridge filter, booster pump and the ultrafilter membrane group being sequentially connected, wherein ultrafilter membrane group has the import being connected with booster pump and two corresponding concentrated solution part, the concentrated solution outlet of permeate part and permeate outlets respectively, described infusion pump is connected with the liquid outlet of batch can, the concentrated solution outlet of ultrafilter membrane group is connected with the inlet of batch can, and described circulation purifies and is additionally provided with butterfly valve and relief valve on pipeline；
Permeate gets rid of pipeline, and it is a pipeline, and this pipeline one section exports with the permeate of ultrafilter membrane group and is connected, and the other end is permeate outlet, and this permeate eliminating pipeline is additionally provided with butterfly valve and relief valve.
The remove impurity purification system of a kind of vitamin C glucoside the most according to claim 1, it is characterised in that: it is respectively arranged with pressure transducer between described cartridge filter and infusion pump, booster pump.
The remove impurity purification system of a kind of vitamin C glucoside the most according to claim 2, it is characterised in that: it is respectively arranged with pressure transducer at the import of described ultrafilter membrane group and concentrated solution outlet.
The remove impurity purification system of a kind of vitamin C glucoside the most according to claim 2, it is characterised in that: it is provided with heat exchanger and flow transducer between concentrated solution outlet and the batch can of described ultrafilter membrane group.
The remove impurity purification system of a kind of vitamin C glucoside the most according to claim 2, it is characterised in that: described cartridge filter is 5 microns of cartridge filters.
The remove impurity purification system of a kind of vitamin C glucoside the most according to claim 1, it is characterised in that: described ultrafilter membrane group is 5000 molecular weight for retaining aperture.
The remove impurity purification system of a kind of vitamin C glucoside the most according to claim 1, it is characterised in that: described permeate is got rid of pipeline and is also included a flow transducer.
8. according to the remove impurity purification system of a kind of vitamin C glucoside described in claim 1 to 7 any one, it is characterized in that: this remove impurity purification system also includes a feedback pipe, this feedback pipe includes switch valve and the feedback valve being dimly connected, this feedback pipe one end is connected with the input of booster pump, and this feedback pipe other end purifies the concentrated solution outlet of ultrafilter membrane group in pipeline and is connected with circulation.
The remove impurity purification system of a kind of vitamin C glucoside the most according to claim 8, it is characterised in that: described booster pump quantity is two, and is serially connected between two booster pumps.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620466825.7U CN205774238U (en) | 2016-05-20 | 2016-05-20 | A kind of remove impurity purification system of vitamin C glucoside |
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| CN201620466825.7U CN205774238U (en) | 2016-05-20 | 2016-05-20 | A kind of remove impurity purification system of vitamin C glucoside |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109012195A (en) * | 2018-09-20 | 2018-12-18 | 佛山市海天（江苏）调味食品有限公司 | A kind of ultrafiltration system and its operating method |
| CN111111292A (en) * | 2020-01-15 | 2020-05-08 | 福州三合元生物科技有限公司 | Edulcoration purification device of vitamin C glucoside |
-
2016
- 2016-05-20 CN CN201620466825.7U patent/CN205774238U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109012195A (en) * | 2018-09-20 | 2018-12-18 | 佛山市海天（江苏）调味食品有限公司 | A kind of ultrafiltration system and its operating method |
| CN111111292A (en) * | 2020-01-15 | 2020-05-08 | 福州三合元生物科技有限公司 | Edulcoration purification device of vitamin C glucoside |
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| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: A purification system of vitamin C glucoside Effective date of registration: 20200812 Granted publication date: 20161207 Pledgee: Bank of China Limited Xiamen hi tech Park sub branch Pledgor: QINHAO MEMBRANE TECHNOLOGY(XIAMEN)CO., Ltd. Registration number: Y2020980004900 |
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| PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20231212 Granted publication date: 20161207 Pledgee: Bank of China Limited Xiamen hi tech Park sub branch Pledgor: QINHAO MEMBRANE TECHNOLOGY(XIAMEN)CO., Ltd. Registration number: Y2020980004900 |