CN205773405U - A kind of device manufacturing barium nitrate - Google Patents

A kind of device manufacturing barium nitrate Download PDF

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Publication number
CN205773405U
CN205773405U CN201620470223.9U CN201620470223U CN205773405U CN 205773405 U CN205773405 U CN 205773405U CN 201620470223 U CN201620470223 U CN 201620470223U CN 205773405 U CN205773405 U CN 205773405U
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China
Prior art keywords
reactor
nitric acid
swelling agent
reaction still
acid reaction
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Expired - Fee Related
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CN201620470223.9U
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Chinese (zh)
Inventor
陈准
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Individual
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Individual
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Abstract

The utility model discloses a kind of device manufacturing barium nitrate, including swelling agent reactor, nitric acid reaction still, evaporate expanded reactor, described swelling agent reactor, wherein swelling agent reactor discharging opening is connected with swelling agent input port by pipeline, pipeline between swelling agent reactor discharging opening and swelling agent input port is provided with pump, nitric acid reaction still discharging opening is by pipeline and the expanded reactor charging aperture of evaporation, and nitric acid reaction still discharging opening and the pipeline evaporated between expanded reactor charging aperture are provided with pump;This utility model is processed by three-step reaction and prepares barium nitrate, and raw material utilizes height, shortens barium nitrate manufacturing time short.

Description

A kind of device manufacturing barium nitrate
Technical field
This utility model belongs to mechanical field, a kind of device manufacturing barium nitrate.
Background technology
Barium nitrate, is dissolved in water, insoluble in ethanol.Decompose to give off oxygen during heating, have strong oxidizing property, with sulfur, phosphorus, Organic substance contact, friction or impact energy cause burning or blast.As oxidant, analytical reagent, it is used for barium salt processed, signal flare and fireworks, is additionally operable to potting enamel, medicine etc..Conventionally manufactured barium nitrate equipment and technique relative efficiency are low, and raw material availability is the highest.
Utility model content
The purpose of this utility model is to provide a kind of expansion effect good, saves the swelling agent reactor in response time.
The technical solution realizing this utility model purpose is:
nullA kind of device manufacturing barium nitrate,Including swelling agent reactor、Nitric acid reaction still、Evaporate expanded reactor,Described swelling agent reactor,Including swelling agent reactor housing、Stirring concentrator bowl、Swelling agent reactor shaft、Swelling agent reactor motor、Swelling agent reactor heating plate、Swelling agent reactor solid feed inlet,Described swelling agent reactor motor is fixed on swelling agent reactor case top by support,Swelling agent reactor motor is connected with swelling agent reactor shaft upper end,Stirring concentrator bowl is suspended in swelling agent reactor housing by swelling agent reactor shaft,Swelling agent reactor heating plate it is provided with in swelling agent reactor housing,Swelling agent reactor case top is provided with swelling agent reactor feeding-in solid body mouth and swelling agent reactor air vent,Swelling agent reactor housing upper end sidewall is provided with swelling agent reactor water inlet,Swelling agent reactor housing bottom is provided with swelling agent reactor discharging opening,Swelling agent reactor discharging opening is provided with valve,The cylinder of described stirring concentrator bowl is open top cylinder,Cylinder lateral wall is provided with some holes,Cylinder inboard wall is fixing connects mixing baffle,Cylinder is connected by support and swelling agent reactor shaft lower end are fixing;
nullDescribed nitric acid reaction still,Including nitric acid reaction still shell body、Stirring vane、Nitric acid reaction still shaft、Nitric acid reaction still motor、Add heat pipe、Nitric acid pump,Described nitric acid reaction still motor is fixed on nitric acid reaction still case top by support,Nitric acid reaction still motor is connected with nitric acid reaction still shaft upper end,Stirring vane is suspended in nitric acid reaction still shell body by nitric acid reaction still shaft,Nitric acid reaction still closure periphery is provided with and adds heat pipe,Nitric acid reaction still case top is provided with nitric acid reaction still air vent、Nitric acid reaction still feeding-in solid body mouth、Swelling agent input port、Nitric acid reaction still observation panel,Nitric acid reaction still shell body upper end sidewall is provided with nitric acid reaction still water inlet,Nitric acid reaction still housing bottom is provided with nitric acid reaction still discharging opening,Nitric acid reaction still discharging opening is provided with valve,Nitric acid pump is connected with nitric acid tank and nitric acid reaction still case top respectively by pipeline,Described stirring vane includes longitudinal blade and cross blade,Wherein longitudinal blade and horizontal plane,Cross blade and horizontal plane are provided with angle,Cross blade one end is fixing with nitric acid reaction still shaft to be connected,The cross blade other end is fixing with longitudinal blade to be connected;
nullThe expanded reactor of described evaporation,Including evaporating expanded reactor housing、Anchor formula blade、Evaporate expanded reactor shaft、Evaporate expanded reactor motor、Evaporate expanded reactor heating plate,Described evaporation expanded reactor motor is fixed on the expanded reactor case top of evaporation by support,Evaporate expanded reactor motor and be connected with evaporating expanded reactor shaft upper end,Anchor formula blade is suspended in the expanded reactor housing of evaporation by evaporating expanded reactor shaft,Evaporate expanded reactor closure periphery and be provided with the expanded reactor heating plate of evaporation,Evaporate expanded reactor case top and be provided with the expanded reactor air vent of evaporation、Evaporate expanded reactor charging aperture、Evaporate expanded reactor observation panel,Evaporate expanded reactor housing bottom and be provided with the expanded reactor discharging opening of evaporation,Evaporate expanded reactor discharging opening and be provided with valve,Described anchor formula blade and evaporate and be provided with brush between expanded reactor inner walls,Brush is fixed on anchor formula blade surface;
Wherein swelling agent reactor discharging opening is connected with swelling agent input port by pipeline, pipeline between swelling agent reactor discharging opening and swelling agent input port is provided with pump, nitric acid reaction still discharging opening is by pipeline and the expanded reactor charging aperture of evaporation, and nitric acid reaction still discharging opening and the pipeline evaporated between expanded reactor charging aperture are provided with pump.
This utility model compared with prior art, its remarkable advantage:
(1) device of this utility model manufacture barium nitrate is processed by three-step reaction and prepares barium nitrate, and raw material utilizes high, shortens barium nitrate manufacturing time short.
(2) the stirring concentrator bowl sidewall of swelling agent reactor of the present utility model is provided with hole, solid material and liquid charging stock mutually impact under the mixing baffle of stirring concentrator bowl, solid is finally dissolved in liquid, under the jet and pressure of liquid, produce expanded reaction, finally flow out from concentrator bowl hole after reaction.
(3) nitric acid reaction still of the present utility model uses cross blade and longitudinal blade to rotate, and makes the liquid in nitric acid reaction still produce horizontal mobility and longitudinal flow, makes nitric acid be fully contacted with other raw material in housing.
(4) being provided with brush between anchor formula blade and the inner walls of the expanded reactor of evaporation of the present utility model, when effectively preventing evaporation from drying, solid, powdery thing is set on the inwall evaporating expanded reactor.
Below in conjunction with the accompanying drawings this utility model swelling agent reactor is described in further detail.
Accompanying drawing explanation
Fig. 1 is the structural representation that this utility model manufactures the device of barium nitrate.
Fig. 2 is swelling agent reactor structural representation of the present utility model.
Fig. 3 is the plan structure schematic diagram of this utility model swelling agent reactor stirring concentrator bowl.
Fig. 4 is nitric acid reaction still structural representation of the present utility model.
Fig. 5 is the stirring vane structural representation of this utility model nitric acid reaction still.
Fig. 6 is evaporation of the present utility model expanded reactor structural representation.
Detailed description of the invention
As shown in figs 1 to 6:
A kind of device manufacturing barium nitrate, including swelling agent reactor 1, nitric acid reaction still 2, evaporates expanded reactor 3,
nullAs shown in Fig. 2-Fig. 3,Described swelling agent reactor 1,Including swelling agent reactor housing 11、Stirring concentrator bowl 12、Swelling agent reactor shaft 13、Swelling agent reactor motor 14、Swelling agent reactor heating plate 15、Swelling agent reactor solid feed inlet 16,Described swelling agent reactor motor 14 is fixed on swelling agent reactor housing 11 top by support,Swelling agent reactor motor 14 is connected with swelling agent reactor shaft 13 upper end,Stirring concentrator bowl 12 is suspended in swelling agent reactor housing 11 by swelling agent reactor shaft 13,Swelling agent reactor heating plate 15 it is provided with in swelling agent reactor housing 11,Swelling agent reactor housing 11 top is provided with swelling agent reactor feeding-in solid body mouth 16 and swelling agent reactor air vent 111,Swelling agent reactor housing 11 upper end sidewall is provided with swelling agent reactor water inlet 113,Swelling agent reactor discharging opening 17 it is provided with bottom swelling agent reactor housing 11,Swelling agent reactor discharging opening 17 is provided with valve;The cylinder 121 of described stirring concentrator bowl 12 is open top cylinder, and cylinder 121 sidewall is provided with some holes, the fixing mixing baffle 122 that connects of cylinder 121 inwall, and cylinder 121 is connected by support and swelling agent reactor shaft 13 lower end are fixing;
nullAs shown in fig. 4-5,Described nitric acid reaction still 2,Including nitric acid reaction still shell body 21、Stirring vane 22、Nitric acid reaction still shaft 23、Nitric acid reaction still motor 24、Add heat pipe 25、Nitric acid pump 26,Described nitric acid reaction still motor 24 is fixed on nitric acid reaction still shell body 21 top by support,Nitric acid reaction still motor 24 is connected with nitric acid reaction still shaft 23 upper end,Stirring vane 22 is suspended in nitric acid reaction still shell body 21 by nitric acid reaction still shaft 23,Nitric acid reaction still shell body 21 periphery is provided with and adds heat pipe 25,Nitric acid reaction still shell body 21 top is provided with nitric acid reaction still air vent 211、Nitric acid reaction still feeding-in solid body mouth 212、Swelling agent input port 213、Nitric acid reaction still observation panel 214,Nitric acid reaction still shell body 21 upper end sidewall is provided with nitric acid reaction still water inlet 215,Nitric acid reaction still discharging opening 27 it is provided with bottom nitric acid reaction still shell body 21,Nitric acid reaction still discharging opening 27 is provided with valve,Nitric acid pump 26 is connected with nitric acid tank and nitric acid reaction still shell body 21 top respectively by pipeline,Described stirring vane 22 includes longitudinal blade 221 and cross blade 222,Wherein longitudinal blade 221 and horizontal plane,Cross blade 222 and horizontal plane are provided with angle,Cross blade 222 one end is fixing with nitric acid reaction still shaft 23 to be connected,Cross blade 222 other end is fixing with longitudinal blade 221 to be connected;
nullAs shown in Figure 6,The expanded reactor of described evaporation 3,Including evaporating expanded reactor housing 31、Anchor formula blade 32、Evaporate expanded reactor shaft 33、Evaporate expanded reactor motor 34、Evaporate expanded reactor heating plate 35,Described evaporation expanded reactor motor 34 is fixed on expanded reactor housing 31 top of evaporation by support,Evaporate expanded reactor motor 34 and be connected with evaporating expanded reactor shaft 33 upper end,Anchor formula blade 32 is suspended in the expanded reactor housing 31 of evaporation by evaporating expanded reactor shaft 33,Evaporate expanded reactor housing 31 periphery and be provided with the expanded reactor heating plate 35 of evaporation,Evaporate expanded reactor housing 31 top and be provided with the expanded reactor air vent 311 of evaporation、Evaporate expanded reactor charging aperture 312、Evaporate expanded reactor observation panel 313,Evaporate and bottom expanded reactor housing 31, be provided with the expanded reactor discharging opening 36 of evaporation,Evaporate expanded reactor discharging opening 36 and be provided with valve,Described anchor formula blade 32 and evaporate and be provided with brush 321 between expanded reactor housing 31 inwall,Brush 321 is fixed on anchor formula blade 32 surface.
Described swelling agent reactor housing 11 appearance and nitric acid reaction still shell body 21 appearance are equipped with heat-insulation layer.
Described heat-insulation layer uses aluminium silicate wool.
Described nitric acid reaction still observation panel 214 and the expanded reactor observation panel 313 of evaporation all use quartz visor.
The operation principle of the device of this utility model manufacture barium nitrate:
By water inlet water filling in swelling agent reactor housing, water in swelling agent reactor housing reaches design temperature by heater plate, swelling agent reactor driven by motor stirring concentrator bowl high speed rotating, solid, powdery raw material is repeatedly pulverized in entrance stirring concentrator bowl through the crushing blade of solid feed inlet, solid material and liquid charging stock mutually impact under the mixing baffle of stirring concentrator bowl, solid is finally dissolved in liquid, expanded reaction is produced under the jet and pressure of liquid, the final swelling agent input port being discharged into nitric acid reaction still from swelling agent reactor discharging opening after reaction.
By water inlet water filling in nitric acid reaction still shell body, solid material is added by nitric acid reaction still feeding-in solid body mouth, in kettle, the required swelling agent of reaction is injected by swelling agent input port, by nitric acid pump by nitric acid in nitric acid tank in suction nitric acid reaction still, liquid in reactor reaches design temperature by nitric acid reaction still heater plate, nitric acid reaction still driven by motor stirring vane rotates, cross blade and longitudinal blade rotate, the liquid in nitric acid reaction still is made to produce horizontal mobility and longitudinal flow, nitric acid is made to be fully contacted intensified response effect with other raw material in housing, end reaction terminates, reacted product is discharged from going out nitric acid reaction still material mouth.
The liquid charging stock reacted through nitric acid reaction still enters in the housing evaporating expanded reactor by evaporating expanded reactor charging aperture, anchor formula blade rotates under the drive of motor, uniform temperature is kept in the heating lower house of heating plate, under the high-speed stirred of anchor formula blade, liquid charging stock produces expanded reaction, and liquid slowly becomes powdery solid under high temperature dries the effect of evaporation and stirring, it is set on inner wall of kettle when there being part powdery solid, on anchor formula blade, it is brushed down from inner wall of kettle by brush, end reaction thing powdery barium nitrate is discharged from nitric acid reaction still shell discharging opening.

Claims (4)

  1. null1. the device manufacturing barium nitrate,It is characterized in that,Including swelling agent reactor (1)、Nitric acid reaction still (2)、Evaporate expanded reactor (3),Described swelling agent reactor (1),Including swelling agent reactor housing (11)、Stirring concentrator bowl (12)、Swelling agent reactor shaft (13)、Swelling agent reactor motor (14)、Swelling agent reactor heating plate (15)、Swelling agent reactor solid feed inlet (16),Described swelling agent reactor motor (14) is fixed on swelling agent reactor housing (11) top by support,Swelling agent reactor motor (14) is connected with swelling agent reactor shaft (13) upper end,Stirring concentrator bowl (12) is suspended in swelling agent reactor housing (11) by swelling agent reactor shaft (13),Swelling agent reactor heating plate (15) it is provided with in swelling agent reactor housing (11),Swelling agent reactor housing (11) top is provided with swelling agent reactor feeding-in solid body mouth (16) and swelling agent reactor air vent (111),Swelling agent reactor housing (11) upper end sidewall is provided with swelling agent reactor water inlet (113),Swelling agent reactor housing (11) bottom is provided with swelling agent reactor discharging opening (17),Swelling agent reactor discharging opening (17) is provided with valve,The cylinder (121) of described stirring concentrator bowl (12) is open top cylinder,Cylinder (121) sidewall is provided with some holes,Cylinder (121) inwall is fixing connects mixing baffle (122),Cylinder (121) is connected by support and swelling agent reactor shaft (13) lower end are fixing;
    nullDescribed nitric acid reaction still (2),Including nitric acid reaction still shell body (21)、Stirring vane (22)、Nitric acid reaction still shaft (23)、Nitric acid reaction still motor (24)、Add heat pipe (25)、Nitric acid pump (26),Described nitric acid reaction still motor (24) is fixed on nitric acid reaction still shell body (21) top by support,Nitric acid reaction still motor (24) is connected with nitric acid reaction still shaft (23) upper end,Stirring vane (22) is suspended in nitric acid reaction still shell body (21) by nitric acid reaction still shaft (23),Nitric acid reaction still shell body (21) periphery is provided with and adds heat pipe (25),Nitric acid reaction still shell body (21) top is provided with nitric acid reaction still air vent (211)、Nitric acid reaction still feeding-in solid body mouth (212)、Swelling agent input port (213)、Nitric acid reaction still observation panel (214),Nitric acid reaction still shell body (21) upper end sidewall is provided with nitric acid reaction still water inlet (215),Nitric acid reaction still shell body (21) bottom is provided with nitric acid reaction still discharging opening (27),Nitric acid reaction still discharging opening (27) is provided with valve,Nitric acid pump (26) is connected with nitric acid tank and nitric acid reaction still shell body (21) top respectively by pipeline,Described stirring vane (22) includes longitudinal blade (221) and cross blade (222),Wherein longitudinal blade (221) and horizontal plane,Cross blade (222) and horizontal plane are provided with angle,Cross blade (222) one end is fixing with nitric acid reaction still shaft (23) to be connected,Cross blade (222) other end is fixing with longitudinal blade (221) to be connected;
    nullThe expanded reactor of described evaporation (3),Including evaporating expanded reactor housing (31)、Anchor formula blade (32)、Evaporate expanded reactor shaft (33)、Evaporate expanded reactor motor (34)、Evaporate expanded reactor heating plate (35),Described evaporation expanded reactor motor (34) is fixed on expanded reactor housing (31) top of evaporation by support,Evaporate expanded reactor motor (34) and be connected with evaporating expanded reactor shaft (33) upper end,Anchor formula blade (32) is suspended in the expanded reactor housing (31) of evaporation by evaporating expanded reactor shaft (33),Evaporate expanded reactor housing (31) periphery and be provided with the expanded reactor heating plate (35) of evaporation,Evaporate expanded reactor housing (31) top and be provided with the expanded reactor air vent (311) of evaporation、Evaporate expanded reactor charging aperture (312)、Evaporate expanded reactor observation panel (313),Evaporate expanded reactor housing (31) bottom and be provided with the expanded reactor discharging opening (36) of evaporation,Evaporate expanded reactor discharging opening (36) and be provided with valve,It is provided with brush (321) between described anchor formula blade (32) and expanded reactor housing (31) inwall of evaporation,Brush (321) is fixed on anchor formula blade (32) surface;
    Wherein swelling agent reactor discharging opening (17) is connected with swelling agent input port (213) by pipeline, pipeline between swelling agent reactor discharging opening (17) and swelling agent input port (213) is provided with pump, nitric acid reaction still discharging opening (27) is provided with pump by pipeline with the expanded reactor charging aperture (312) of evaporation, nitric acid reaction still discharging opening (27) and the pipeline evaporated between expanded reactor charging aperture (312).
  2. A kind of device manufacturing barium nitrate the most according to claim 1, it is characterised in that: described swelling agent reactor housing (11) appearance and nitric acid reaction still shell body (21) appearance are equipped with heat-insulation layer.
  3. A kind of device manufacturing barium nitrate the most according to claim 2, it is characterised in that: described heat-insulation layer uses aluminium silicate wool.
  4. A kind of device manufacturing barium nitrate the most according to claim 1, it is characterised in that: described nitric acid reaction still observation panel (214) and the expanded reactor observation panel (313) of evaporation all use quartz visor.
CN201620470223.9U 2016-05-23 2016-05-23 A kind of device manufacturing barium nitrate Expired - Fee Related CN205773405U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201620470223.9U CN205773405U (en) 2016-05-23 2016-05-23 A kind of device manufacturing barium nitrate

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201620470223.9U CN205773405U (en) 2016-05-23 2016-05-23 A kind of device manufacturing barium nitrate

Publications (1)

Publication Number Publication Date
CN205773405U true CN205773405U (en) 2016-12-07

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201620470223.9U Expired - Fee Related CN205773405U (en) 2016-05-23 2016-05-23 A kind of device manufacturing barium nitrate

Country Status (1)

Country Link
CN (1) CN205773405U (en)

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20161207

Termination date: 20170523