CN205761133U - A kind of mechanism catching up with gas for adjacent diphenylamines mother solution deamination - Google Patents

A kind of mechanism catching up with gas for adjacent diphenylamines mother solution deamination Download PDF

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Publication number
CN205761133U
CN205761133U CN201620474880.0U CN201620474880U CN205761133U CN 205761133 U CN205761133 U CN 205761133U CN 201620474880 U CN201620474880 U CN 201620474880U CN 205761133 U CN205761133 U CN 205761133U
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China
Prior art keywords
reactor
gas
mother solution
motor
shaft
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Expired - Fee Related
Application number
CN201620474880.0U
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Chinese (zh)
Inventor
罗利忠
胡孝明
朱玉梅
储兵兵
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Anhui Dongzhi Guangxin Agrochemical Co Ltd
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Anhui Dongzhi Guangxin Agrochemical Co Ltd
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Priority to CN201620474880.0U priority Critical patent/CN205761133U/en
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Publication of CN205761133U publication Critical patent/CN205761133U/en
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/20Air quality improvement or preservation, e.g. vehicle emission control or emission reduction by using catalytic converters

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Abstract

nullA kind of mechanism catching up with gas for adjacent diphenylamines mother solution deamination,Including reactor、Nitrogen pot、Drive motor and shaft,Described reactor top center is provided with motor fixed rack,Motor fixed rack is provided with driving motor,Motor is driven to be connected with the shaft in reactor by variator,Shaft is sequentially provided with puddler from top to bottom、Many stirrer paddles and lower puddler,Described reactor inwall correspondence stirrer paddle is evenly distributed with multiple baffle plate arranged along vertical direction,Described reactor bottom interior wall tightens to be sticked and is equipped with ring pipe airway,Multiple jet thrust diagonally downward uniformly it is laid with inside annular airway,Described nitrogen pot top connects breather line,The outlet side of breather line connects with annular airway through reactor top and along reactor inwall,This utility model simple in construction,Can effectively absorb process ammonia,Avoid polluting environment,Improve nitric efficiency,Security performance is good.

Description

A kind of mechanism catching up with gas for adjacent diphenylamines mother solution deamination
Technical field
This utility model relates to pesticide processing apparatus field, specifically a kind of female for adjacent diphenylamines Loss of thick fluid ammonia catches up with the mechanism of gas.
Background technology
O-phenylenediamine is main pesticide and dyestuff intermediate, is the former of production pesticide carbendazim Material.Containing a large amount of ammonias in adjacent diphenylamines mother solution, during mother solution with feed separation, workshop Being ammonia taste everywhere, uncontrollable discharge ratio is more serious, in order to improve workshop condition, reduces inorganization Discharge, reduces potential safety hazard, it will usually with nitrogen by the ammonia aeration in mother solution, reduce discharge. The deamination effect of existing deamination mechanism is bad, easily has too many residual in o-phenylenediamine mother solution Ammonia, the by-product produced when being so easily caused late phase reaction is more, and pollutes environment, peace Full property is poor;It addition, existing deamination mechanism can not effectively absorb process ammonia mostly, can only drive out of Ammonia, the most still pollutes the environment.
Utility model content
The purpose of this utility model is to provide a kind of simple in construction, it is possible to absorption processes ammonia, Avoiding polluting environment, improve nitric efficiency, what security performance was good is used for adjacent diphenylamines mother solution deamination Catch up with the mechanism of gas, with the problem solving to propose in above-mentioned background technology.
For achieving the above object, the following technical scheme of this utility model offer:
A kind of mechanism catching up with gas for adjacent diphenylamines mother solution deamination, including reactor, nitrogen pot, Driving motor and shaft, described reactor top center is provided with motor fixed rack, and motor is solid Fixed rack is provided with driving motor, drives motor by variator with the shaft in reactor even Connecing, shaft is sequentially provided with puddler, many stirrer paddles and lower puddler from top to bottom, Described reactor inwall correspondence stirrer paddle be evenly distributed with multiple along vertical direction arrange Baffle plate, described reactor bottom interior wall tightens to be sticked and is equipped with ring pipe airway, annular airway Inner side is uniformly laid with multiple jet thrust diagonally downward, and described nitrogen pot top connects ventilation Pipeline, the outlet side of breather line through reactor top and is led along reactor inwall with annular Trachea connects, and reactor top side is provided with charging aperture and exhaustor, and the exhaustor other end is stretched Entering gas treatment bottom portion to arrange, gas treatment case is connected by dropping pipe dropping tank, described Drainage conduit it is provided with bottom reactor.
As further program of the utility model, described exhaustor is provided with exhaust solenoid valve Door.
As further program of the utility model, it is close to be arranged on gear in the middle part of described breather line On plate side.
As further program of the utility model, described dropping pipe is provided with drip switch Valve.
As further program of the utility model, described gas treatment upper box part side is provided with out QI KOU.
Compared with prior art, the beneficial effects of the utility model are: be passed through by breather line Nitrogen, owing to nitrogen is noble gas, insoluble in the mother solution in reactor, by uniform cloth It is located at the jet thrust inside annular airway bottom reactor, is passed through nitrogen, it is ensured that nitrogen can Ammonia in whole reactor is driven out of, catches up with gas effect comprehensive;Shaft sets the most successively There are upper puddler, many stirrer paddles and lower puddler, reactor inwall correspondence stirrer paddle Sheet is evenly distributed with multiple baffle plate arranged along vertical direction, and mother solution is in the effect of stirrer paddle Baffle plate in lower rotation, and knock-on reaction still inwall, it is possible to being prevented effectively from mother solution can be along with stirring Oar spins inside kettle so that the ammonia in mother solution is discharged more rapid, improves nitric efficiency; By dropping pipe, the acid solution in dropping tank is joined in gas treatment case, be used for absorbing ammonia Generate ammonium salt fertilizer, not only reduce entreprise cost, also avoid waste gas discharge to cause air Pollute.This utility model simple in construction, it is possible to effectively absorption processes ammonia, it is to avoid pollute environment, Improving nitric efficiency, security performance is good.
Accompanying drawing explanation
Fig. 1 is the structural representation of a kind of mechanism catching up with gas for adjacent diphenylamines mother solution deamination.
In figure: 1-reactor, 2-support, 3-variator, 4-motor fixed rack, 5-baffle plate, 6-nitrogen pot, 7-drives motor, 8-exhaustor, 9-exhaust solenoid valve door, 10-charging aperture, The upper puddler of 11-, 12-stirrer paddle, 13-annular airway, 14-drainage conduit, under 15- Puddler, 16-jet thrust, 17-breather line, 18-drips tank, and 19-drips pipe, and 20-goes out QI KOU, 21-gas treatment case.
Detailed description of the invention
Below in conjunction with the accompanying drawing in this utility model embodiment, in this utility model embodiment Technical scheme be clearly and completely described, it is clear that described embodiment be only this The a part of embodiment of utility model rather than whole embodiments.Based in this utility model Embodiment, those of ordinary skill in the art are obtained under not making creative work premise Every other embodiment, broadly falls into the scope of this utility model protection.
Refer to Fig. 1, in this utility model embodiment, a kind of for adjacent diphenylamines mother solution deamination Catch up with the mechanism of gas, including the reactor 1 being arranged on support 2, nitrogen pot 6, drive motor 7 and shaft, described reactor 1 top center is provided with motor fixed rack 4, and motor is fixed Support 4 is provided with driving motor 7, drives motor 7 by variator 3 and reactor 1 Shaft connects, and shaft is sequentially provided with puddler 11, many stirrer paddles from top to bottom Sheet 12 and lower puddler 15, described reactor 1 inwall correspondence stirrer paddle 12 uniformly divides Being furnished with multiple baffle plate 5 arranged along vertical direction, described reactor 1 bottom interior wall tightens and is sticked Be equipped with ring pipe airway 13, be uniformly laid with inside annular airway 13 multiple diagonally downward Jet thrust 16, described nitrogen pot 6 top connect have breather line 17, breather line 17 Outlet side connects with annular airway 13 through reactor 1 top and along reactor 1 inwall, Reactor 1 top side is provided with charging aperture 10 and exhaustor 8, and exhaustor 8 other end is stretched Enter bottom gas treatment case 21 arrange, gas treatment case 21 by dropping pipe 19 connect have drip Add tank 18, bottom described reactor 1, be provided with drainage conduit 14.
In this utility model embodiment, described exhaustor 8 is provided with exhaust solenoid valve door 9, uses Control the discharge of gas in reactor 1.
In this utility model embodiment, it is close to be arranged on baffle plate 5 in the middle part of described breather line 17 On side, impact suffered by breather line 17 when significantly reducing stirring.
In this utility model embodiment, described dropping pipe 19 is provided with drip switch valve, uses In the dropping situation controlling acid solution.
In this utility model embodiment, described gas treatment case 21 top side is provided with gas outlet 20。
Operation principle of the present utility model is: be passed through nitrogen by breather line 17, due to nitrogen Gas is noble gas, insoluble in the mother solution in reactor 1, leads by being uniformly laid in annular Jet thrust 16 inside trachea 13 is passed through nitrogen bottom reactor 1, it is ensured that nitrogen can be by Ammonia in whole reactor 1 is driven out of, catches up with gas effect comprehensive;Shaft sets the most successively There are upper puddler 11, many stirrer paddles 12 and lower puddler 15, reactor 1 inwall pair Answering stirrer paddle 12 to be evenly distributed with multiple baffle plate 5 arranged along vertical direction, mother solution exists Rotate under the effect of stirrer paddle 12, and the baffle plate 5 on knock-on reaction still 1 inwall, energy Enough it is prevented effectively from mother solution to spin inside kettle along with stirring paddle so that the ammonia row in mother solution Go out more rapid, improve nitric efficiency;By dropping pipe 19 by the acid solution in dropping tank 18 Join in gas treatment case 21, be used for absorbing ammonia and generate ammonium salt fertilizer, not only reduce Entreprise cost, also avoids waste gas discharge to cause the pollution of air.
It is obvious to a person skilled in the art that this utility model is not limited to above-mentioned exemplary reality Execute the details of example, and in the case of without departing substantially from spirit or essential attributes of the present utility model, This utility model can be realized in other specific forms.Therefore, no matter from the point of view of which point, Embodiment all should be regarded as exemplary, and be nonrestrictive, model of the present utility model Enclose and limited by claims rather than described above, it is intended that will fall in claim All changes in the implication of equivalency and scope are included in this utility model.Should will not weigh Any reference during profit requires is considered as limiting involved claim.
Moreover, it will be appreciated that although this specification is been described by according to embodiment, but not Each embodiment only comprises an independent technical scheme, and this narrating mode of description is only Being only for clarity sake, those skilled in the art should be using description as an entirety, each reality Executing the technical scheme in example can also be through appropriately combined, and formation it will be appreciated by those skilled in the art that Other embodiments.

Claims (5)

1. catch up with a mechanism for gas for adjacent diphenylamines mother solution deamination, including reactor, nitrogen pot, Drive motor and shaft, it is characterised in that described reactor top center is provided with motor and fixes Support, motor fixed rack is provided with driving motor, drives motor by variator and reactor Interior shaft connects, and shaft is sequentially provided with puddler, many stirrer paddles from top to bottom Sheet and lower puddler, described reactor inwall correspondence stirrer paddle is evenly distributed with multiple along lead Nogata is to the baffle plate arranged, and described reactor bottom interior wall tightens to be sticked and is equipped with ring pipe inducing QI Pipe, is uniformly laid with multiple jet thrust diagonally downward, described nitrogen pot inside annular airway Top connects breather line, and the outlet side of breather line is through reactor top and along reaction Still inwall connects with annular airway, and reactor top side is provided with charging aperture and exhaustor, The exhaustor other end stretches into gas treatment bottom portion and arranges, and gas treatment case is connected by dropping pipe There is dropping tank, bottom described reactor, be provided with drainage conduit.
A kind of machine catching up with gas for adjacent diphenylamines mother solution deamination the most according to claim 1 Structure, it is characterised in that described exhaustor is provided with exhaust solenoid valve door.
A kind of machine catching up with gas for adjacent diphenylamines mother solution deamination the most according to claim 1 Structure, it is characterised in that be close in the middle part of described breather line be arranged on baffle plate side.
A kind of machine catching up with gas for adjacent diphenylamines mother solution deamination the most according to claim 1 Structure, it is characterised in that be provided with drip switch valve on described dropping pipe.
A kind of machine catching up with gas for adjacent diphenylamines mother solution deamination the most according to claim 1 Structure, it is characterised in that described gas treatment upper box part side is provided with gas outlet.
CN201620474880.0U 2016-05-19 2016-05-19 A kind of mechanism catching up with gas for adjacent diphenylamines mother solution deamination Expired - Fee Related CN205761133U (en)

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Application Number Priority Date Filing Date Title
CN201620474880.0U CN205761133U (en) 2016-05-19 2016-05-19 A kind of mechanism catching up with gas for adjacent diphenylamines mother solution deamination

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109663467A (en) * 2019-02-25 2019-04-23 临沂华毅医药股份有限公司 A kind of aminating reaction object optimization device and method of ortho-aminobenzoic acid
CN109969631A (en) * 2019-04-08 2019-07-05 南京威安新材料科技有限公司 A kind of solid catalyst shipping container
CN113651700A (en) * 2021-08-06 2021-11-16 安徽东至广信农化有限公司 Deamination process of o-phenylenediamine mother liquor
CN115445249A (en) * 2022-10-09 2022-12-09 铜陵华兴精细化工有限公司 Solution deamination equipment for sodium persulfate processing

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109663467A (en) * 2019-02-25 2019-04-23 临沂华毅医药股份有限公司 A kind of aminating reaction object optimization device and method of ortho-aminobenzoic acid
CN109969631A (en) * 2019-04-08 2019-07-05 南京威安新材料科技有限公司 A kind of solid catalyst shipping container
CN113651700A (en) * 2021-08-06 2021-11-16 安徽东至广信农化有限公司 Deamination process of o-phenylenediamine mother liquor
CN115445249A (en) * 2022-10-09 2022-12-09 铜陵华兴精细化工有限公司 Solution deamination equipment for sodium persulfate processing
CN115445249B (en) * 2022-10-09 2023-08-18 铜陵华兴精细化工有限公司 Solution deamination equipment for sodium persulfate processing

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CF01 Termination of patent right due to non-payment of annual fee
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Granted publication date: 20161207

Termination date: 20210519