CN205759871U - A kind of left-handed resin tower with d-camphorsulfonic acid of the most quickly recovery - Google Patents
A kind of left-handed resin tower with d-camphorsulfonic acid of the most quickly recovery Download PDFInfo
- Publication number
- CN205759871U CN205759871U CN201620521123.4U CN201620521123U CN205759871U CN 205759871 U CN205759871 U CN 205759871U CN 201620521123 U CN201620521123 U CN 201620521123U CN 205759871 U CN205759871 U CN 205759871U
- Authority
- CN
- China
- Prior art keywords
- double
- camphorsulfonic acid
- deck
- plate
- flow
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
This utility model relates to a kind of left-handed resin tower with d-camphorsulfonic acid of the most quickly recovery.During left (right) rotation camphorsulfonic acid splits DL-phenylglycine, just can not apply mechanically after certain batch when splitting mother liquid recycle.Tower body of the present utility model has two charging apertures in upper end, it is provided with discharging opening in the lower end of tower body, arranging at least four bilayer flow-stopping plate in described tower body from top to bottom, the double-deck deflector of odd column is inclined to set, and the double-deck deflector of even column is for being horizontally disposed with.Have, on the upper plate of the double-deck flow-stopping plate being obliquely installed and lower plate, the perforate being symmetrical set, the upper plate of the double-deck flow-stopping plate be arrangeding in parallel and lower plate have the hole being uniformly interspersed.It is notable that this utility model splits the recovering effect of left (right) rotation camphorsulfonic acid in mother solution for DL-phenylglycine, and production capacity up to 10t/h greatly reduces production cost, also made outstanding contributions for environmental protection work simultaneously.
Description
Technical field
This utility model relates to a kind of left-handed resin tower with d-camphorsulfonic acid of the most quickly recovery.
Background technology
During left (right) rotation camphorsulfonic acid splits DL-phenylglycine, just can not apply mechanically after certain batch when splitting mother liquid recycle.This splits a left side (right) the rotation camphorsulfonic acid containing 5%-8% in mother solution.If directly discharge can increase burden to cesspool, once sewage disposal process is made a fault and be will result in serious environmental protection problem；If reclaiming a left side (right) camphorsulfonic acid by concentrating fractionation mother solution, energy consumption is big, cycle length, cost are high, does not meets the call of current " energy-saving and emission-reduction ", concentrates in addition and often can not get a qualified left side (right) rotation camphorsulfonic acid.
Utility model content
The purpose of this utility model is to solve above-mentioned technical problem, and provides a kind of and the most quickly reclaim the left-handed and resin tower of d-camphorsulfonic acid, can rapidly and efficiently reclaim the left-handed and d-camphorsulfonic acid split in mother solution, reduce cost, reduce environmental pollution.
The technical solution adopted in the utility model is: a kind of left-handed resin tower with d-camphorsulfonic acid of the most quickly recovery, it is characterized in that the tower body of described resin tower has two charging apertures in upper end, it is provided with discharging opening in the lower end of tower body, at least four bilayer flow-stopping plate is set in described tower body from top to bottom, the double-deck deflector of odd column is inclined to set, and the double-deck deflector of even column is for being horizontally disposed with.Have, on the upper plate of the double-deck flow-stopping plate being obliquely installed and lower plate, the perforate being symmetrical set, the upper plate of the double-deck flow-stopping plate be arrangeding in parallel and lower plate have the hole being uniformly interspersed.
Described tower body arranges four double-deck flow-stopping plates, and first double-deck flow-stopping plate is 45 degree of placements, and second double-deck flow-stopping plate is 135 degree of placements.
Described tower body is cylinder, and described flow-stopping plate is circular slab or elliptical flat-plate.
Described charging aperture includes a big charging aperture and a little charging aperture.
Described charging aperture is distributed in both sides, top, and described discharging opening is arranged on center bottom.
This utility model uses RXZ-108 resin, the PH that DL-phenylglycine splits mother solution is controlled, resin tower uses the double-deck flow-stopping plate possessing perforate, and then by DL-phenylglycine split mother solution and the eluent time of staying in tower and liquid form controls within requiring, and then obtain satisfied absorption, dissociation effect.It is notable that this utility model splits the recovering effect of left (right) rotation camphorsulfonic acid in mother solution for DL-phenylglycine, and production capacity up to 10t/h greatly reduces production cost, also made outstanding contributions for environmental protection work simultaneously.
Accompanying drawing explanation
Fig. 1 structural representation of the present utility model.
Detailed description of the invention
Below this utility model is further described:
As it is shown in figure 1, resin tower is overall in class cylinder, the both sides, top of resin tower 4 have small one and large one two charging apertures 1, and center bottom has a discharging opening 5.Four double-deck flow-stopping plates 3, perforate on flow-stopping plate is had in resin tower.From top to bottom: first double-deck flow-stopping plate is 45 ° of placements, and the position of opening of two-layer flow-stopping plate is distributed in heterodoxy；Second double-deck flow-stopping plate horizontal positioned, two-layer flow-stopping plate uniform pore openings and the interlaced distribution of perforate；The 135 degree of placements of 3rd double-deck flow-stopping plate, two-layer flow-stopping plate position of opening is distributed in heterodoxy；4th double-deck flow-stopping plate horizontal positioned, two-layer flow-stopping plate uniform pore openings and the interlaced distribution of perforate.Sphere in resin tower is RXZ-108 resin 2, is dispersed between double-deck flow-stopping plate, can flow freely.
Processing procedure is as follows: closed by resin tower lower end drain hole, treatment fluid is squeezed into flooding RXZ-108 resin in resin tower, RXZ-108 resin is carried out pretreatment, DL-phenylglycine is split mother solution and squeezes into resin tower from heavy caliber charging aperture, stop charging to drain hole feed liquid band color.Eluent is squeezed into resin tower from the small-bore charging aperture of resin tower, is repeated twice, obtain left (right) rotation camphorsulfonic acid liquid.Concentrating under reduced pressure, reclaims eluent and waits to reuse, and obtains a qualified left side (right) rotation camphorsulfonic acid.
Listed above is only specific embodiment of the utility model, and this utility model is not limited to above example, it is also possible to have many deformation.All deformation that those of ordinary skill in the art can directly derive from this utility model disclosure or associate, are all considered as protection domain of the present utility model.
Claims (5)
1. one kind is the most quickly reclaimed the left-handed and resin tower of d-camphorsulfonic acid, it is characterized in that the tower body of described resin tower has two charging apertures in upper end, it is provided with discharging opening in the lower end of tower body, at least four bilayer flow-stopping plate is set in described tower body from top to bottom, the double-deck deflector of odd column is inclined to set, the double-deck deflector of even column is for being horizontally disposed with, have, on the upper plate of the double-deck flow-stopping plate being obliquely installed and lower plate, the perforate being symmetrical set, the upper plate of the double-deck flow-stopping plate be arrangeding in parallel and lower plate have the hole being uniformly interspersed.
A kind of left-handed resin tower with d-camphorsulfonic acid of the most quickly recovery the most according to claim 1, it is characterised in that described tower body arranges four double-deck flow-stopping plates, and first double-deck flow-stopping plate is 45 degree of placements, and second double-deck flow-stopping plate is 135 degree of placements.
A kind of left-handed resin tower with d-camphorsulfonic acid of the most quickly recovery the most according to claim 2, it is characterised in that described tower body is cylinder, and described flow-stopping plate is circular slab or elliptical flat-plate.
A kind of left-handed resin tower with d-camphorsulfonic acid of the most quickly recovery the most according to claim 3, it is characterised in that described charging aperture includes a big charging aperture and a little charging aperture.
A kind of left-handed resin tower with d-camphorsulfonic acid of the most quickly recovery the most according to claim 4, it is characterised in that described charging aperture is distributed in both sides, top, and described discharging opening is arranged on center bottom.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620521123.4U CN205759871U (en) | 2016-05-31 | 2016-05-31 | A kind of left-handed resin tower with d-camphorsulfonic acid of the most quickly recovery |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620521123.4U CN205759871U (en) | 2016-05-31 | 2016-05-31 | A kind of left-handed resin tower with d-camphorsulfonic acid of the most quickly recovery |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205759871U true CN205759871U (en) | 2016-12-07 |
Family
ID=58135447
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620521123.4U Active CN205759871U (en) | 2016-05-31 | 2016-05-31 | A kind of left-handed resin tower with d-camphorsulfonic acid of the most quickly recovery |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205759871U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107746091A (en) * | 2017-11-07 | 2018-03-02 | 广州栋方生物科技股份有限公司 | A kind of method for reducing camphor content in borneol water |
-
2016
- 2016-05-31 CN CN201620521123.4U patent/CN205759871U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107746091A (en) * | 2017-11-07 | 2018-03-02 | 广州栋方生物科技股份有限公司 | A kind of method for reducing camphor content in borneol water |
| CN107746091B (en) * | 2017-11-07 | 2020-04-17 | 广州栋方生物科技股份有限公司 | Method for reducing camphor content in borneol water |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103397194A (en) | Method for recycling nickel from nickel-containing wastewater | |
| CN106430783A (en) | Ternary precursor waste water treatment system and treating method thereof | |
| CN105110544A (en) | Method for treating wastewater with dilute alkali by aid of macroporous resin | |
| CN205759871U (en) | A kind of left-handed resin tower with d-camphorsulfonic acid of the most quickly recovery | |
| CN101708908B (en) | Novel method for treating electroplating chromium-containing wastewater and recovering metal ions | |
| CN202151529U (en) | Recycling device for titanium white postprocessing washing liquid | |
| CN204982071U (en) | Waste cupric liquor copper recovery device | |
| CN109665593A (en) | Ion exchange resin adsorbs the Processes and apparatus that DTRO produces water ammonia nitrogen | |
| CN106865833A (en) | Electrodialysis membrane recovery process for acidic wastewater in viscose fiber spinning | |
| CN103628064A (en) | Recycling system of acid etching liquid | |
| CN207405061U (en) | A kind of vertical sludge filter press | |
| CN205575732U (en) | Modularization electricity flocculation waste water treatment equipment | |
| CN204607581U (en) | A kind of acid-restoring plant of lead acid cell | |
| CN203525387U (en) | Sludge-water separation mechanism for sludge treatment | |
| CN208482100U (en) | A kind of waste water environmental protection and energy saving purifier | |
| CN203307186U (en) | Oily sludge treatment device | |
| CN202107584U (en) | Water-saving device for electroplating production line | |
| CN206334440U (en) | One kind precipitation sheet frame pressure-filtering deslagging system | |
| CN105565544A (en) | Method for recycling nickel | |
| CN110790441A (en) | Device and method for recovering copper from copper-containing waste liquid | |
| CN203333417U (en) | Nickel plating wastewater on-line treater | |
| CN211226469U (en) | Ion exchange equipment for sewage treatment | |
| CN204939214U (en) | Waste Water Treatment | |
| CN202717848U (en) | Recycling system of acid etching liquid | |
| CN202724866U (en) | Precipitation filter for processing waste diluting agent |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |