CN205749360U - A kind of freeze dryer eutectic point eutectic point test equipment - Google Patents
A kind of freeze dryer eutectic point eutectic point test equipment Download PDFInfo
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- CN205749360U CN205749360U CN201620308262.9U CN201620308262U CN205749360U CN 205749360 U CN205749360 U CN 205749360U CN 201620308262 U CN201620308262 U CN 201620308262U CN 205749360 U CN205749360 U CN 205749360U
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Abstract
The utility model discloses a kind of freeze dryer eutectic point eutectic point test equipment, test storehouse including eutectic point and be arranged on the eutectic point test storehouse below eutectic point test storehouse, described eutectic point test storehouse includes the dry storehouse in hollow cylindrical and is arranged on and adds hot plate within dry storehouse, material disc it is provided with in hot plate in described adding, eutectic point test pen it is provided with in this material disc, described dry storehouse top is provided with upper cover, it is provided with lower cover bottom described dry storehouse, it is provided with stainless steel faceplate below described lower cover, described eutectic point test position in storehouse is below described stainless steel faceplate, it is provided with material disc in described eutectic point test storehouse, eutectic point test pen it is provided with in this material disc, described eutectic point test periphery, storehouse is provided with vaporizer.This utility model is capable of vacuum, freezing, is dried, simultaneously material eutectic point, temperature of eutectic point can be detected and be analyzed again；And automatically according to " eutectic point " " eutectic point " temperature, lyophilizing technique is arranged temperature control.
Description
Technical field
This utility model relates to a kind of freeze dryer eutectic point eutectic point test equipment.
Background technology
At present, domestic freeze dryer the most all criteria of right and wrong products.What major part manufacturer was walked is imitated road, some factory
Family, while using advanced foreign technology, has been also carried out bigger improvement.As: have employed special guiding device in heating plate,
Make the uniform flow of fluid in plate, it is ensured that heating the most even stable；Water vessel can realize alternately catching water and melting at work
Ice, in water vessel coil pipe, Ammonia refrigeration mode is changed into ammoniacal liquor phase-change-free refrigeration by traditional ammoniacal liquor freezing by change of state, makes water vessel dish
Homogeneous temperature in pipe, frosting is functional.For freeze dryer, these design, improve and optimize, and simply supplement in lyophilizing
Heat sublimation, catch aqueous, improve lyophilizing efficiency；But the lyophilizing mass action for material is the most little.
Ensure quality of material, improve material activity and reproducibility, keep to greatest extent by the cytoactive of dry material with
And by the color of dry material, shape and nutritional labeling, and rehydration performance is good.Lyophylized food be use modern dehydration technique with
Integrating of processes be convenient, health care, the high-quality pollution-free food of pure natural, it is to avoid conventional dehydration method is brought
Variable color, rotten, spoiled, ingredients from lossing, the defect such as cannot reduce.Reduce energy consumption, it is ensured that freeze-drying prods quality is inexorable trend.
The unique counterweight realizing this target controls temperature of charge exactly.The i.e. eutectic point temperature of eutectic point of material.
At present, the instrument volume of domestic and international lyophilizing function tester material eutectic point is big, power consumption is high, somewhat expensive, startup survey
Examination cost is high, supports waste huge.Independent eutectic point MELTING POINT TESTER together, price is the most all at several ten thousand yuan of even hundreds of thousands
The impact of unit, the most restricted cold heating-up temperature and equipment, limitation is too big, and neither one equipment can have eutectic simultaneously
The dual-use function that point is tested with eutectic point.The vacuum freezings such as the medicine of 95%, food, biological product, scientific research, biological preparation
It is dried and all cannot realize the technology lyophilizing that effective temperature controls.All of lyophilizing technique is the most all to grope in constantly experiment
Optimal freeze temperature. a large amount of labor intensive and material resources. vacuum lyophilization is also all in the primary stage.Numerous businessmans is to eutectic
Point eutectic point test is the most all felt frustrated.
Utility model content
The purpose of this utility model is to provide a kind of freeze dryer eutectic point eutectic point test equipment, it is possible to improve existing skill
The problem that art exists, it is achieved vacuum, freezing, be dried, material " eutectic point ", " eutectic point " temperature can be detected again simultaneously
With analysis；And automatically according to " eutectic point " " eutectic point " temperature, lyophilizing technique is arranged temperature control, keep quilt to greatest extent
The cytoactive of dry material and by the color of dry material, shape and rehydration and nutritional labeling, is the most domestic or even state
Market, border all do not have can lyophilization realize the most simultaneously " eutectic point " " eutectic point " test analysis comprehensive vacuum freezing do
Dry analysis system, simple to operate, economical and practical.
This utility model is achieved through the following technical solutions:
A kind of freeze dryer eutectic point eutectic point test equipment, tests storehouse including eutectic point and is arranged under eutectic point test storehouse
The eutectic point test storehouse of side, described eutectic point test storehouse includes the dry storehouse in hollow cylindrical and is arranged on inside dry storehouse
Add hot plate, be provided with material disc in hot plate in described adding, in this material disc, be provided with eutectic point test pen, described
Dry storehouse top is provided with upper cover, is provided with lower cover bottom described dry storehouse, is provided with stainless below described lower cover
Steel facing, described eutectic point test position in storehouse, below described stainless steel faceplate, is arranged in described eutectic point test storehouse
There is material disc, in this material disc, be provided with eutectic point test pen, described eutectic point test periphery, storehouse is provided with vaporizer,
Described eutectic point test storehouse is provided with vacuum orifice, described stainless steel faceplate is provided with through hole and makes described freezing
Dry storehouse is connected with described eutectic point test storehouse, is provided with discharge outlet, described below described eutectic point test storehouse
Stainless steel faceplate is provided above test point.
Further, on described upper cover lower surface, it is provided with annular recess for this utility model is better achieved,
Described annular recess is embedded with sealing ring, and the upper surface of described dry storehouse can be embedded in described annular recess.
Further, on the upper surface of described lower cover, it is provided with annular recess for this utility model is better achieved,
Being embedded with sealing ring at this annular recess, the lower surface of described dry storehouse can be embedded in described annular recess.
Further, it is bolted to described dry storehouse for heating dish described in the utility model is better achieved
(101) inner side.
Further, on described dry storehouse, it is provided with temperature sensor for this utility model is better achieved.
Further, described in the utility model the metal that hot plate includes setting gradually from top to bottom is added for being better achieved
Layer, zone of heating and thermal insulation layer.
Solution is not to condense when a certain fixed temperature or melt, but condenses in a certain temperature range or molten
Solving, the temperature starting to separate out crystal when cooled is referred to as the freezing point of solution, and the temperature that solution all condenses is called the solidifying of solution
Solid point.It is the most also simultaneously the beginning temperature (both fusing points) melted, for solution, is also solute and temperature that solvent melts jointly,
It is called again eutectic point.The freezing point of visible solution and eutectic point differ.Eutectic point is only solution and the most all congeals into solid
Temperature.In freezing process, only determine whether fully charge is impossible to product, along with states of matter from apparent and variations in temperature
The change of change electrical property, particularly change in resistance can reflect the process freezed.Because solution is ionic conduction, freeze to lead
Causing solion transfixion, solution resistance rate significantly increases.And resistivity will be remarkably decreased in the presence of having a small amount of liquid.Therefore
The resistivity measuring product will can determine that the eutectic point of product.
Temperature resistance curve is when being changed into solid-state by liquid, and the resistance of determinand changes, and record temperature-resistance is bent
Line, the catastrophe point of this curve is i.e. freezing point, and automatically demonstrates eutectic temperature value.Under certain pressure intensity, temperature-resistance is bent
Line is liquid when solid transition, and the resistance of determinand changes, and records temperature resistance curve, and the catastrophe point of this curve is i.e.
Fusing point.The same temperature of eutectic point automatically showing material.Eutectic point and eutectic point are to determining that freezing scope is extremely important.
Further, for this utility model is better achieved, described eutectic point test includes that dry storehouse and being arranged on freezes
Add hot plate in dry storehouse, be provided with material disc in hot plate in described adding, in this material disc, be provided with eutectic point test pen,
Described dry storehouse top is provided with upper cover, is provided with lower cover bottom described dry storehouse, arranges below described lower cover
There is stainless steel faceplate.
Further, for this utility model is better achieved, described eutectic point test include eutectic point test storehouse and with
The compressor that described eutectic point test storehouse is connected, described eutectic point test system is positioned under described stainless steel faceplate
Side, is provided with vaporizer in described eutectic point test periphery, storehouse, is provided with breather valve on described eutectic point test storehouse,
Described eutectic point test storehouse, is provided with vacuum orifice, on described stainless steel faceplate on described eutectic point test storehouse
Being provided with through hole makes described dry storehouse be connected with described eutectic point test storehouse, sets below described eutectic point test storehouse
Being equipped with discharge outlet, described dry storehouse lower end inside is provided with vaporizer, and described vacuum system includes being connected to described taking out
Vacuum pump on vacuum port, described vacuum pump is connected with described vacuum orifice, in described connection by connecting pipeline
It is provided with filter on pipeline, the connection pipeline between described filter and described vacuum pump is provided with vacuum conditions
Valve.
Further, for this utility model is better achieved, described eutectic point eutectic point analysis includes being arranged on described
Stainless steel faceplate above test point, in described material disc, be provided with test pen, described test pen by circuit with
Described display operating system is connected.
This utility model compared with prior art, has the advantages that
(1) this utility model is by using freeze dryer cold-trap to freeze, and dividing plate heats, and studies through for many years, reform and innovation, will
The analysis test of eutectic point and eutectic point is together with instrument perfection set, it is achieved the most all have no idea to realize small-sized lyophilizing
Machine eutectic point eutectic point analysis and testing technology.Substantially increase work efficiency, saving fund, reduce use space and resource wave
Take.
(2) this utility model is by using refrigeration system, heating system, vacuum system and eutectic point eutectic point analysis system
System, it is achieved vacuum, freezing, be dried, simultaneously material " eutectic point ", " eutectic point " temperature can be detected and analyze again, it is achieved
System is analyzed in the comprehensive vacuum lyophilization of " eutectic point " " eutectic point " test analysis, simple to operate, economical and practical.
Accompanying drawing explanation
In order to be illustrated more clearly that the technical scheme of this utility model embodiment, will use required in embodiment below
Accompanying drawing be briefly described, it will be appreciated that the following drawings illustrate only some embodiment of the present utility model, the most should be by
Regard the restriction to scope as, for those of ordinary skill in the art, on the premise of not paying creative work, also may be used
To obtain other relevant accompanying drawings according to these accompanying drawings.
Fig. 1 is this utility model embodiment 1 overall structure schematic diagram；
Fig. 2 is that this utility model embodiment 1 adds hot plate structural representation；
Fig. 3 is this utility model embodiment 3 overall structure schematic block diagram.
Fig. 4 is this utility model embodiment 3 overall structure schematic diagram；
Fig. 5 is this utility model eutectic point eutectic point test philosophy figure；
Fig. 6 is this utility model embodiment 3 eutectic point test function analysis chart；
Fig. 7 is this utility model embodiment 3 eutectic point test function analysis chart；
Fig. 8 is this utility model embodiment 4 overall structure schematic block diagram.
Wherein: 101. dry storehouses, 102. add hot plate, 103. upper covers, 104. lower covers, 105. stainless steel faceplates, 106. eutectics
Point test storehouse, 107. vaporizers, 109. vacuum orifices, 110. annular recess, 111. test points, 113. metal levels, 114. heating
Layer, 115. thermal insulation layers, 116. vacuum pumps, 117. filters, 118. vacuum breakers.
Detailed description of the invention
Below in conjunction with specific embodiment, this utility model is described in further detail, but embodiment party of the present utility model
Formula is not limited to this.
Embodiment 1:
As shown in Figure 1, 2, a kind of freeze dryer eutectic point eutectic point test equipment, test storehouse including eutectic point and be arranged on altogether
Eutectic point test storehouse 106 below fusing point test storehouse, described eutectic point test storehouse includes the dry storehouse 101 in hollow cylindrical
And be arranged on and add hot plate 102 within dry storehouse 101, it is provided with material disc in hot plate 102, in this material disc in described adding
It is provided with eutectic point test pen, described dry storehouse 101 top is provided with upper cover 103, sets bottom described dry storehouse 101
Being equipped with lower cover 104, be provided with stainless steel faceplate 105 below described lower cover 104, described eutectic point test storehouse 106 is positioned at
Below described stainless steel faceplate 105, in described eutectic point test storehouse 106, it is provided with material disc, sets in this material disc
It is equipped with eutectic point test pen, described eutectic point test periphery, storehouse 106 is provided with vaporizer 107, surveys at described eutectic point
Examination is provided with vacuum orifice 109 on storehouse 106, is provided with through hole and makes described dry storehouse 101 on described stainless steel faceplate 105
It is connected with described eutectic point test storehouse 106, below described eutectic point test storehouse 106, is provided with discharge outlet, described
Stainless steel faceplate 105 be provided above test point 111.
Material is placed in the material disc above heating plate, by connecting vacuum pump on vacuum orifice, can make altogether
Keep certain vacuum in brilliant some test storehouse and dry storehouse, by eutectic point test storehouse, material is lowered the temperature, make material exist
Quick freezing under low temperature, then heats material by adding hot plate, makes the ice crystal in material go out by the way of distillation,
And make residual moisture discharge with vapor form by vaporizer.
Embodiment 2:
The present embodiment is on the basis of embodiment 1, in the present embodiment, in order to enable upper cover preferably close relative to dry storehouse
Envelope, keeps certain vacuum, it is preferable that be provided with annular recess on described upper cover 103 lower surface in making dry storehouse
110, it is embedded with sealing ring at described annular recess 110, the upper surface of described dry storehouse 101 can be embedded into described ring
In shape groove 110.
In the present embodiment, in order to enable lower cover preferably to seal relative to dry storehouse, make to keep in dry storehouse certain true
Reciprocal of duty cycle, it is preferable that be provided with annular recess 110 on the upper surface of described lower cover 104, is embedded with at this annular recess 110
Sealing ring, the lower surface of described dry storehouse 101 can be embedded in described annular recess 110.
The dismounting of structure for convenience, in the present embodiment, it is preferable that the described hot plate 102 that adds is bolted to described
Inside dry storehouse 101.Support can be set adding in hot plate, conveniently be fixed in dry storehouse, in the present embodiment, further
Preferably, use aluminium alloy to make supporting structure, supporting structure is fixedly connected in dry storehouse, heating dish is bolted to
On supporting structure.
Detect temperature for convenience, in the present embodiment, it is preferable that on described dry storehouse 101, be provided with temperature sensing
Device.
Make heating more uniform, in the present embodiment, it is preferable that the described hot plate 102 that adds includes from top to bottom for convenience
Metal level 113, zone of heating 114 and the thermal insulation layer 115 set gradually.By using above-mentioned setting, it is possible to make performance more smooth
Smooth, make different layers add between hot plate and do not interfere with each other mutually, convenient control temperature, make to be uniformly heated.
Test pen is put in material by this utility model, and refrigeration system put into by material, the while of material refrigeration, and central processing unit
Record temperature and resistance, calculate eutectic point or eutectic point temperature.Material vacuum lyophilization, eutectic point eutectic point test with
Same equipment completes.Economic, practical, simple, quick.It it is currently the only vacuum lyophilization eutectic point eutectic point test
Completion system.
Embodiment 3:
The mensuration of eutectic point measures frequently with electric-resistivity method, but unfixing equipment, measure the accuracy of the data obtained
And repeatability cannot ensure.Expense is the highest, and difficulty is the biggest.And it is unstable not to be suitable for properties, normal pressure is normal
Yielding determinand under temperature.
In the present embodiment, as shown in Figure 3, Figure 4, a kind of freeze dryer eutectic point eutectic point test system, including display operation
System and the eutectic point test system being connected with display operating system respectively, eutectic point test system, program control system, system
Cooling system, heating system, vacuum system.
In the present embodiment, disclose the preferred structure of a kind of eutectic point test system, it is preferable that described eutectic point test
Service system include dry storehouse 101 and be arranged in dry storehouse 101 add hot plate 102, be provided with in hot plate 102 in described adding
Material disc, is provided with eutectic point test pen in this material disc, is provided with upper cover 103, in institute at described dry storehouse 101 top
It is provided with lower cover 104 bottom the dry storehouse 101 stated, below described lower cover 104, is provided with stainless steel faceplate 105.
In the present embodiment, also disclose the preferred structure of a kind of eutectic point test system, described eutectic point test system
Testing storehouse 106 and the compressor being connected with described eutectic point test storehouse 106 including eutectic point, described eutectic point test is
System is positioned at below described stainless steel faceplate 105, is provided with vaporizer 107, in institute in described eutectic point test periphery, storehouse 106
It is provided with breather valve, in described eutectic point test storehouse 106, in described eutectic point test on the eutectic point test storehouse 106 stated
Be provided with vacuum orifice 109 on storehouse 106, described stainless steel faceplate 105 is provided with through hole make described dry storehouse 101 with
Described eutectic point test storehouse 106 is connected, and is provided with discharge outlet below described eutectic point test storehouse 106, and described freezes
Dry storehouse 101 lower end inside is provided with vaporizer 107, and described vacuum system includes being connected on described vacuum orifice 109
Vacuum pump 116, described vacuum pump 116 is connected with described vacuum orifice 109, in described connection by connecting pipeline
It is provided with filter 117 on pipeline, the connection pipeline between described filter 117 and described vacuum pump 116 is arranged
There is vacuum breaker 118.
As it is shown in figure 5, freeze first with refrigeration system, program control system record temperature, curve；Open eutectic point
Eutectic point analyzes system, when temperature and resistance are undergone mutation, and temperature when program control system records sudden change and resistance, aobvious
Show that operating system demonstrates eutectic temperature；Carry out eutectic point test, open refrigeration system and freeze, utilize eutectic point congruent melting
Point analysis system detection material, material to be measured be placed on specimen disc (adding hot plate) insert eutectic point test storehouse carry out freezing；
Material is frozen to-40 DEG C, open eutectic point eutectic point test system and test switch, obtain eutectic point test function analysis chart, as
Shown in Fig. 6；Click eutectic point is tested；Opening heating system, utilization adds hot plate and starts to heat, the material in container when material adds
When hot temperature is undergone mutation, program control system record temperature of eutectic point, display operating system demonstrates test result, such as Fig. 7
Shown in.
Embodiment 4:
The present embodiment is on the basis of embodiment 3, in the present embodiment, by using filter and regulation valve, it is possible to make thing
Moisture in material is discharged by vacuum pump, compares existing structure, by using regulating valve structure, it is possible to avoid material by vacuum pump
Take away, it is to avoid loss of material, avoid vacuum pump to block simultaneously.
Preferably, in the present embodiment, described eutectic point eutectic point is analyzed system and is included being arranged on described surface stainless steel
Test point 111 above plate 105, is provided with test pen in described material disc, and described test pen passes through circuit with described
Display operating system be connected.
In the present embodiment, it is further preferred that remotely controlling of also including being connected with described display operating system is
System, humidity warning system, heating defrosting system and noble gas backfill system.
As shown in Figure 8, it is preferable that described humidity warning system includes being arranged within described dry storehouse 101
Humidity sensor, described humidity sensor is connected with described display operating system by circuit, described noble gas
Backfill system includes the noble gas communicating pipe being connected with described dry storehouse, sets outside described noble gas communicating pipe
It is equipped with booster pump.
The foregoing is only preferred embodiment of the present utility model, be not limited to this utility model, for this
For the technical staff in field, this utility model can have various modifications and variations.All in spirit of the present utility model and principle
Within, any modification, equivalent substitution and improvement etc. made, within should be included in protection domain of the present utility model.
Claims (6)
1. a freeze dryer eutectic point eutectic point test equipment, it is characterised in that: include eutectic point test storehouse and be arranged on congruent melting
Eutectic point test storehouse (106) below some test storehouse, described eutectic point test storehouse includes the dry storehouse in hollow cylindrical
(101) and be arranged on dry storehouse (101) internal add hot plate (102), be provided with material disc in described adding in hot plate (102),
In this material disc, it is provided with eutectic point test pen, is provided with upper cover (103), described at described dry storehouse (101) top
Dry storehouse (101) bottom be provided with lower cover (104), described lower cover (104) lower section is provided with stainless steel faceplate (105),
Described eutectic point test storehouse (106) is positioned at described stainless steel faceplate (105) lower section, in described eutectic point test storehouse
(106) it is provided with material disc in, in this material disc, is provided with eutectic point test pen, at described eutectic point test storehouse (106)
Periphery is provided with vaporizer (107), is provided with vacuum orifice (109), described on described eutectic point test storehouse (106)
Being provided with through hole on stainless steel faceplate (105) makes described dry storehouse (101) be connected with described eutectic point test storehouse (106)
Logical, described eutectic point test storehouse (106) lower section is provided with discharge outlet, is provided above at described stainless steel faceplate (105)
There is test point (111).
A kind of freeze dryer eutectic point eutectic point test equipment the most according to claim 1, it is characterised in that: described upper
Lid is provided with annular recess (110) on (103) lower surface, is embedded with sealing ring at described annular recess (110), and described freezes
The upper surface in dry storehouse (101) can be embedded in described annular recess (110).
A kind of freeze dryer eutectic point eutectic point test equipment the most according to claim 1 and 2, it is characterised in that: described
Lower cover (104) upper surface on be provided with annular recess (110), be embedded with sealing ring at this annular recess (110), described
The lower surface of dry storehouse (101) can be embedded in described annular recess (110).
A kind of freeze dryer eutectic point eutectic point test equipment the most according to claim 1 and 2, it is characterised in that: described
Add hot plate (102) and be bolted to described dry storehouse (101) inner side.
A kind of freeze dryer eutectic point eutectic point test equipment the most according to claim 1 and 2, it is characterised in that: described
Dry storehouse (101) on be provided with temperature sensor.
A kind of freeze dryer eutectic point eutectic point test equipment the most according to claim 1 and 2, it is characterised in that: described
Add metal level (113), zone of heating (114) and thermal insulation layer (115) that hot plate (102) includes setting gradually from top to bottom.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620308262.9U CN205749360U (en) | 2016-04-14 | 2016-04-14 | A kind of freeze dryer eutectic point eutectic point test equipment |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201620308262.9U CN205749360U (en) | 2016-04-14 | 2016-04-14 | A kind of freeze dryer eutectic point eutectic point test equipment |
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| CN205749360U true CN205749360U (en) | 2016-11-30 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105784753A (en) * | 2016-04-14 | 2016-07-20 | 王劲松 | Freeze-dryer eutectic point and co-melting point testing equipment and system |
-
2016
- 2016-04-14 CN CN201620308262.9U patent/CN205749360U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105784753A (en) * | 2016-04-14 | 2016-07-20 | 王劲松 | Freeze-dryer eutectic point and co-melting point testing equipment and system |
| CN105784753B (en) * | 2016-04-14 | 2018-12-28 | 王劲松 | A kind of freeze dryer eutectic point eutectic point test equipment and its test macro |
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