CN205731263U - A kind of device for preparing indole azoles - Google Patents
A kind of device for preparing indole azoles Download PDFInfo
- Publication number
- CN205731263U CN205731263U CN201620713631.2U CN201620713631U CN205731263U CN 205731263 U CN205731263 U CN 205731263U CN 201620713631 U CN201620713631 U CN 201620713631U CN 205731263 U CN205731263 U CN 205731263U
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- China
- Prior art keywords
- ice bath
- pond
- azoles
- water
- semiconductor cooler
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- Filtration Of Liquid (AREA)
- Devices That Are Associated With Refrigeration Equipment (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
This utility model discloses a kind of device for preparing indole azoles, including magnetic stirring apparatus, ice bath device, three neck round bottom flask, constant pressure funnel and thermometer, described ice bath device includes housing, ice bath pond, semiconductor cooler, water-cooled pond, temperature sensor, microprocessor and display module, described ice bath pond, described semiconductor cooler, described water-cooled pond and described microprocessor are located in described housing, the refrigeration end of described semiconductor cooler is located in described ice bath pond, and the end that heats of described semiconductor cooler is located in described water-cooled pond；Described temperature sensor is located in described ice bath pond, and described display module is located on the outer wall of described housing.This utility model, without increasing or change ice cube and reducing experiment energy consumption, is conducive to keeping temperature of reaction system stable, reduces the amount of labour of experimenter.
Description
Technical field
This utility model relates to chemical experiment field, is used for preparing indole pyroles chemical combination more particularly, to one
The device of thing.
Background technology
During using existing experimental provision to prepare indole azoles, need flask is placed in ice bath
In, due to the thawing of ice cube, need the most on the rocks, but also need to emit the water at low temperature in ice bath device, and be used for making
The water of ice temperature under normal circumstances can be higher than the temperature of the water at low temperature in ice bath device, and this has resulted in the energy consumption in experimentation
Increase.And when experiment is carried out, due to the consumption of ice cube, need in ice-water bath, constantly increase ice cube, if during reaction
Between long, need constantly ice making and trash ice, which increase the amount of labour of experimenter, and once increase the ice cube time relatively
Evening, it is possible to cause the failure of an experiment or products collection efficiency relatively low.
Utility model content
Because in this, this utility model purpose is that offer is a kind of without increasing or change ice cube and reducing experiment energy
The device for preparing indole azoles of consumption, is conducive to keeping temperature of reaction system stable, reduces experimenter
The amount of labour.
For reaching above-mentioned purpose, this utility model uses following technical proposals: one is used for preparing indole pyroles
The device of compound, including magnetic stirring apparatus, ice bath device, three neck round bottom flask, constant pressure funnel and thermometer, described ice bath device
Including housing, ice bath pond, semiconductor cooler, water-cooled pond, temperature sensor, microprocessor and display module, described ice bath pond,
Described semiconductor cooler, described water-cooled pond and described microprocessor are located in described housing, the system of described semiconductor cooler
Cold end is located in described ice bath pond, and the end that heats of described semiconductor cooler is located in described water-cooled pond；Described temperature sensor
Being located in described ice bath pond, described display module is located on the outer wall of described housing；The signal output part of described temperature sensor
Communicate to connect with the signal input part of described microprocessor, the signal output part of described microprocessor and the letter of described display module
The communication connection of number input；The liquid outlet of described constant pressure funnel is located in a bottleneck of described three neck round bottom flask, and described three
Mouth round-bottomed flask is located in described ice bath pond, and described ice bath device is located on described magnetic stirring apparatus；The lower end of described thermometer
It is located in described three neck round bottom flask, in described three neck round bottom flask, is provided with magnet rotor.
The above-mentioned device for preparing indole azoles, described water-cooled pond is connected to recirculated water.
The above-mentioned device for preparing indole azoles, described ice bath device also includes micropump, described micro-
The outlet of type pump and water inlet are each provided in described ice bath pond, and the water inlet of described micropump is provided with filter screen.
The above-mentioned device for preparing indole azoles, in the axial direction in described ice bath pond, described micropump
Water inlet be located at the top of outlet of described micropump.
The above-mentioned device for preparing indole azoles, described micropump is brushless micro water pump.
The above-mentioned device for preparing indole azoles, the pool wall in described ice bath pond is provided with spoiler.
The above-mentioned device for preparing indole azoles, the pool wall in described ice bath pond is provided with discharging tube, institute
State discharging tube and be provided with stop valve.
The beneficial effects of the utility model are as follows:
1. without again after adding an ice cube when using this utility model will to prepare indole azoles
Add ice cube, the most also reduce because changing the ice cube impact on experiment, and decrease experiment energy consumption.
2. this utility model can reduce the amount of labour of experimenter, it is not necessary to ice making and trash ice repeatedly.
Accompanying drawing explanation
Fig. 1 is that this utility model is for preparing the structural representation of the device of indole azoles；
Fig. 2 is that this utility model is for preparing the structural representation of the ice bath device of the device of indole azoles
Figure；
Fig. 3 is the structural representation in Fig. 2 under ice bath device another kind line of vision.
In figure: 1-magnetic stirring apparatus；2-ice bath device；3-three neck round bottom flask；4-constant pressure funnel；5-thermometer；6-ice
Bathing pool；7-semiconductor cooler；8-water-cooled pond；9-spoiler；10-drain pipe；11-stop valve；12-temperature sensor；13-shell
Body；14-micropump.
Detailed description of the invention
In order to be illustrated more clearly that this utility model, below in conjunction with preferred embodiments and drawings, this utility model is done into one
The explanation of step.Parts similar in accompanying drawing are indicated with identical reference.It will be appreciated by those skilled in the art that following
Specifically described content is illustrative and be not restrictive, and should not limit protection domain of the present utility model with this.
As shown in Figures 1 to 3, this utility model is for preparing the device of indole azoles, including magnetic agitation
Device 1, ice bath device 2, three neck round bottom flask 3, constant pressure funnel 4 and thermometer 5, described ice bath device 2 includes housing 13, ice bath pond
6, semiconductor cooler 7, water-cooled pond 8, temperature sensor 12, microprocessor and display module, described ice bath pond 6, described partly leads
Chiller 7, described water-cooled pond 8 and described microprocessor are located in described housing 13, the refrigeration end of described semiconductor cooler 7
Being located in described ice bath pond 6, the end that heats of described semiconductor cooler 7 is located in described water-cooled pond 8；Described temperature sensor 12
Being located in described ice bath pond 6, described display module is located on the outer wall of described housing 13；The signal of described temperature sensor 12 is defeated
Go out the signal input part communication connection of end and described microprocessor, the signal output part of described microprocessor and described display module
Signal input part communication connection；The liquid outlet of described constant pressure funnel 4 is located in a bottleneck of described three neck round bottom flask 3,
Described three neck round bottom flask 3 is located in described ice bath pond 6, and described ice bath device 2 is located on described magnetic stirring apparatus 1；Described temperature
The lower end of degree meter 5 is located in described three neck round bottom flask 3, is provided with magnet rotor in described three neck round bottom flask 3.Wherein for the ease of
Improve the refrigeration of described semiconductor cooler 7, described water-cooled pond 8 is connected with recirculated water
In view of the coolant fluid for the ease of being lowered the temperature by described semiconductor cooler 7 refrigeration end flows in described ice bath pond 6
Dynamic, so that temperature close or identical everywhere around described three neck round bottom flask 3, in the present embodiment, described ice bath device 2 is also
Including micropump 14, as shown in Figures 2 and 3, the outlet of described micropump 14 and water inlet are each provided in described ice bath pond 6,
In the axial direction in described ice bath pond 6, the water inlet of described micropump 14 is located at the top of the outlet of described micropump 14, and institute
The water inlet stating micropump 14 is provided with filter screen.In the present embodiment, brushless micro water pump is used to use as described micropump 14.
And mix for the ease of the coolant fluid in described ice bath pond 6, so that coolant fluid bulk temperature is more uniform, institute
The pool wall stating ice bath pond 6 is provided with spoiler 9.Simultaneously in order to coolant fluid being reclaimed and utilizing, in described ice bath pond 6
Pool wall is provided with discharging tube 10, and described discharging tube 10 is provided with stop valve 11.
When utilizing this utility model to prepare indole azoles, first build this utility model according to Fig. 1, then exist
Add coolant fluid (such as saline) in described ice bath pond 6, in described ice bath pond 6, add prefabricated ice cube the most again, then will
The raw material preparing indole azoles is respectively put in described three neck round bottom flask 3 and described constant pressure funnel 4, then opens
Open described magnetic stirring apparatus 1, described semiconductor cooler 7 and described micropump 14 and can start experiment.Utilizing this practicality new
During type prepares indole azoles, it is only necessary to add rubble ice in ice bath pond 6 described in experiment starts forward direction, directly
Terminate all without adding or change ice cube again in described ice bath pond 6 to experiment, arrange without in carrying out in experiment simultaneously
Water, has been effectively ensured experiment and has carried out under a stable experimental temperature, it is ensured that smoothly completing of experiment, decreased experiment simultaneously
The workload of personnel.
Above-described embodiment of the present utility model is only for clearly demonstrating this utility model example, and is not
Restriction to embodiment of the present utility model, for those of ordinary skill in the field, on the basis of described above
On can also make other changes in different forms, cannot all of embodiment be given exhaustive here, every genus
Obviously changed in what the technical solution of the utility model extended out or change still in protection model of the present utility model
The row enclosed.
Claims (7)
1. the device being used for preparing indole azoles, it is characterised in that include magnetic stirring apparatus (1), ice bath
Device (2), three neck round bottom flask (3), constant pressure funnel (4) and thermometer (5), described ice bath device (2) includes housing (13), ice
Bathing pool (6), semiconductor cooler (7), water-cooled pond (8), temperature sensor (12), microprocessor and display module, described ice bath
Pond (6), described semiconductor cooler (7), described water-cooled pond (8) and described microprocessor are located in described housing (13), described
The refrigeration end of semiconductor cooler (7) is located in described ice bath pond (6), and the end that heats of described semiconductor cooler (7) is located at institute
State in water-cooled pond (8)；Described temperature sensor (12) is located in described ice bath pond (6), and described display module is located at described housing
(13) on outer wall；The signal output part of described temperature sensor (12) and the signal input part communication link of described microprocessor
Connecing, the signal output part of described microprocessor communicates to connect with the signal input part of described display module；Described constant pressure funnel (4)
Liquid outlet be located in a bottleneck of described three neck round bottom flask (3), described three neck round bottom flask (3) is located at described ice bath pond
(6), in, described ice bath device (2) is located on described magnetic stirring apparatus (1)；The lower end of described thermometer (5) is located at described three mouthfuls
In round-bottomed flask (3), described three neck round bottom flask is provided with magnet rotor in (3).
Device for preparing indole azoles the most according to claim 1, it is characterised in that described water-cooled
Pond (8) is connected to recirculated water.
Device for preparing indole azoles the most according to claim 2, it is characterised in that described ice bath
Device (2) also includes that micropump (14), the outlet of described micropump (14) and water inlet are each provided in described ice bath pond (6),
And the water inlet of described micropump (14) is provided with filter screen.
Device for preparing indole azoles the most according to claim 3, it is characterised in that at described ice
In the axial direction of bathing pool (6), the water inlet of described micropump (14) is located at the top of the outlet of described micropump (14).
Device for preparing indole azoles the most according to claim 4, it is characterised in that described miniature
Pump (14) is brushless micro water pump.
6. according to the arbitrary described device for preparing indole azoles of Claims 1 to 5, it is characterised in that
The inwall of described ice bath pond (6) is provided with spoiler (9).
7. according to the arbitrary described device for preparing indole azoles of Claims 1 to 5, it is characterised in that
The pool wall of described ice bath pond (6) is provided with discharging tube (10), and described discharging tube (10) is provided with stop valve (11).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620713631.2U CN205731263U (en) | 2016-07-07 | 2016-07-07 | A kind of device for preparing indole azoles |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620713631.2U CN205731263U (en) | 2016-07-07 | 2016-07-07 | A kind of device for preparing indole azoles |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205731263U true CN205731263U (en) | 2016-11-30 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620713631.2U Expired - Fee Related CN205731263U (en) | 2016-07-07 | 2016-07-07 | A kind of device for preparing indole azoles |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205731263U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106645268A (en) * | 2017-02-20 | 2017-05-10 | 河南工程学院 | Solidifying point determining device |
-
2016
- 2016-07-07 CN CN201620713631.2U patent/CN205731263U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106645268A (en) * | 2017-02-20 | 2017-05-10 | 河南工程学院 | Solidifying point determining device |
| CN106645268B (en) * | 2017-02-20 | 2023-03-28 | 河南工程学院 | Freezing point measuring device |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20161130 Termination date: 20170707 |