CN205720001U - Aluminium foil type medicament residual quick measuring card - Google Patents
Aluminium foil type medicament residual quick measuring card Download PDFInfo
- Publication number
- CN205720001U CN205720001U CN201620614610.5U CN201620614610U CN205720001U CN 205720001 U CN205720001 U CN 205720001U CN 201620614610 U CN201620614610 U CN 201620614610U CN 205720001 U CN205720001 U CN 205720001U
- Authority
- CN
- China
- Prior art keywords
- tablet
- aluminium foil
- indophenols
- acetas
- quick measuring
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000005030 aluminium foil Substances 0.000 title claims abstract description 37
- 239000003814 drug Substances 0.000 title claims abstract description 19
- 108090000371 Esterases Proteins 0.000 claims abstract description 30
- OIPILFWXSMYKGL-UHFFFAOYSA-N acetylcholine Chemical compound CC(=O)OCC[N+](C)(C)C OIPILFWXSMYKGL-UHFFFAOYSA-N 0.000 claims abstract description 26
- 229960004373 acetylcholine Drugs 0.000 claims abstract description 26
- 238000007906 compression Methods 0.000 claims abstract description 7
- 230000006835 compression Effects 0.000 claims abstract description 7
- 230000000994 depressogenic effect Effects 0.000 claims description 9
- 238000001514 detection method Methods 0.000 abstract description 16
- 238000010276 construction Methods 0.000 abstract description 3
- 238000005259 measurement Methods 0.000 abstract description 3
- 238000000034 method Methods 0.000 description 8
- 238000012546 transfer Methods 0.000 description 6
- 235000013311 vegetables Nutrition 0.000 description 6
- 239000000447 pesticide residue Substances 0.000 description 5
- 239000000654 additive Substances 0.000 description 4
- 230000000996 additive effect Effects 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 239000000273 veterinary drug Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- KXDHJXZQYSOELW-UHFFFAOYSA-M Carbamate Chemical compound NC([O-])=O KXDHJXZQYSOELW-UHFFFAOYSA-M 0.000 description 3
- 241001062009 Indigofera Species 0.000 description 3
- 239000003153 chemical reaction reagent Substances 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 239000000575 pesticide Substances 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Natural products CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 2
- 235000000177 Indigofera tinctoria Nutrition 0.000 description 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 239000003242 anti bacterial agent Substances 0.000 description 2
- 229940088710 antibiotic agent Drugs 0.000 description 2
- OEYIOHPDSNJKLS-UHFFFAOYSA-N choline Chemical compound C[N+](C)(C)CCO OEYIOHPDSNJKLS-UHFFFAOYSA-N 0.000 description 2
- 229960001231 choline Drugs 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 239000003480 eluent Substances 0.000 description 2
- 210000000232 gallbladder Anatomy 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 229940097275 indigo Drugs 0.000 description 2
- COHYTHOBJLSHDF-UHFFFAOYSA-N indigo powder Natural products N1C2=CC=CC=C2C(=O)C1=C1C(=O)C2=CC=CC=C2N1 COHYTHOBJLSHDF-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000035945 sensitivity Effects 0.000 description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- 239000005949 Malathion Substances 0.000 description 1
- YASYVMFAVPKPKE-UHFFFAOYSA-N acephate Chemical compound COP(=O)(SC)NC(C)=O YASYVMFAVPKPKE-UHFFFAOYSA-N 0.000 description 1
- 125000000218 acetic acid group Chemical group C(C)(=O)* 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- CVXBEEMKQHEXEN-UHFFFAOYSA-N carbaryl Chemical compound C1=CC=C2C(OC(=O)NC)=CC=CC2=C1 CVXBEEMKQHEXEN-UHFFFAOYSA-N 0.000 description 1
- DUEPRVBVGDRKAG-UHFFFAOYSA-N carbofuran Chemical compound CNC(=O)OC1=CC=CC2=C1OC(C)(C)C2 DUEPRVBVGDRKAG-UHFFFAOYSA-N 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- OEBRKCOSUFCWJD-UHFFFAOYSA-N dichlorvos Chemical compound COP(=O)(OC)OC=C(Cl)Cl OEBRKCOSUFCWJD-UHFFFAOYSA-N 0.000 description 1
- 229950001327 dichlorvos Drugs 0.000 description 1
- JXSJBGJIGXNWCI-UHFFFAOYSA-N diethyl 2-[(dimethoxyphosphorothioyl)thio]succinate Chemical compound CCOC(=O)CC(SP(=S)(OC)OC)C(=O)OCC JXSJBGJIGXNWCI-UHFFFAOYSA-N 0.000 description 1
- MCWXGJITAZMZEV-UHFFFAOYSA-N dimethoate Chemical compound CNC(=O)CSP(=S)(OC)OC MCWXGJITAZMZEV-UHFFFAOYSA-N 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- YFVOXLJXJBQDEF-UHFFFAOYSA-N isocarbophos Chemical compound COP(N)(=S)OC1=CC=CC=C1C(=O)OC(C)C YFVOXLJXJBQDEF-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229960000453 malathion Drugs 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 229960001952 metrifonate Drugs 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000003032 molecular docking Methods 0.000 description 1
- KRTSDMXIXPKRQR-AATRIKPKSA-N monocrotophos Chemical compound CNC(=O)\C=C(/C)OP(=O)(OC)OC KRTSDMXIXPKRQR-AATRIKPKSA-N 0.000 description 1
- PZXOQEXFMJCDPG-UHFFFAOYSA-N omethoate Chemical compound CNC(=O)CSP(=O)(OC)OC PZXOQEXFMJCDPG-UHFFFAOYSA-N 0.000 description 1
- LCCNCVORNKJIRZ-UHFFFAOYSA-N parathion Chemical compound CCOP(=S)(OCC)OC1=CC=C([N+]([O-])=O)C=C1 LCCNCVORNKJIRZ-UHFFFAOYSA-N 0.000 description 1
- 235000012736 patent blue V Nutrition 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 238000004441 surface measurement Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 210000005182 tip of the tongue Anatomy 0.000 description 1
- 238000012549 training Methods 0.000 description 1
- NFACJZMKEDPNKN-UHFFFAOYSA-N trichlorfon Chemical compound COP(=O)(OC)C(O)C(Cl)(Cl)Cl NFACJZMKEDPNKN-UHFFFAOYSA-N 0.000 description 1
- 230000036642 wellbeing Effects 0.000 description 1
Landscapes
- Investigating Or Analysing Materials By The Use Of Chemical Reactions (AREA)
Abstract
This utility model aluminium foil type medicament residual quick measuring card; including can the aluminium foil of doubling; described aluminium foil is divided into pressure-bearing plate along its fold line and compresses sheet; it is provided with filter paper on described pressure-bearing plate and compression sheet; indophenols acetas tablet it is fixed with on the filter paper of described pressure-bearing plate; it is fixed with acetylcholine esterase tablet on the filter paper of described compression sheet; when described aluminium foil is along fold line doubling; described acetylcholine esterase tablet can be fitted with indophenols acetas tablet, and described acetylcholine esterase tablet, indophenols acetas tablet are coated with the protecting film of layer of transparent.Its purpose is to provide a kind of simple in construction, easy and simple to handle, substantially reduce the measurement time, improve the aluminium foil type medicament residual quick measuring card of detection work efficiency.
Description
Technical field
This utility model relates to a kind of chemical detection method, particularly relates to a kind of aluminium foil type medicament residual quick measuring card.
Background technology
Food safety is matters vital to national well-being and the people's livelihood, and the problem on the tip of the tongue is always the big problem that our country faces,
The most illegal pesticide, veterinary drug, additive are used in veterinary antibiotics, grain, and healthy to the people causes pole
Big harm.In order to allow the general common people can the food that exceeds standard of rapid identification pesticide, veterinary drug, additive, we have developed
A kind of detection method utilizing quick thick salt method, the method is the legal detection method through country's license, the speed survey of use
Card is also with formal national standard for the product relied on.According to the regulation of national standard, need to be at 37 degree during thick salt method detection
At a temperature of continuous heating 3 minutes, i.e. require that staff is pinched 3 minutes as long as, this detection mode has fettered manpower the most significantly, inspection
Survey efficiency is low.And, the thick salt method used the most on the market all uses synthesis stationery material, this kind of material heat conductivity
Low, heat transfer is slow, heat transfer efficiency is low, causes the measurement time long, inefficiency.
Utility model content
The technical problems to be solved in the utility model be to provide a kind of simple in construction, easy and simple to handle, substantially reduce measurement
Time, improve detection work efficiency aluminium foil type medicament residual quick measuring card.
This utility model aluminium foil type medicament residual quick measuring card, including can the aluminium foil of doubling, described aluminium foil divides along its fold line
For pressure-bearing plate and compression sheet, described pressure-bearing plate is fixed with indophenols acetas tablet, described compression sheet is fixed with acetylcholine esterase
Tablet, when described aluminium foil is along fold line doubling, described acetylcholine esterase tablet can be fitted with indophenols acetas tablet, described choline
The protecting film of layer of transparent it is coated with on esterase tablet, indophenols acetas tablet.
This utility model aluminium foil type medicament residual quick measuring card, wherein said pressure-bearing plate, the middle part of compression sheet are provided with position
Relative depressed part, described indophenols acetas tablet, the bottom of acetylcholine esterase tablet embed in described depressed part.
This utility model aluminium foil type medicament residual quick measuring card, wherein said protecting film is provided with and described depressed part position
Relative lobe, described indophenols acetas tablet, the top of acetylcholine esterase tablet embed in described lobe.
This utility model aluminium foil type medicament residual quick measuring card, wherein said aluminium foil be shaped as rectangle or square.
This utility model aluminium foil type medicament residual quick measuring card simple in construction, easy and simple to handle, employing aluminium foil is transfer substrate, aluminum
Paper tinsel heat transfer coefficient is more than the heat transfer coefficient of synthetic paper, and after using aluminium foil heat transfer, the detection time shortens 1/2, it is only necessary to staff pinches 1.5 points
About clock, greatly reduce the constraint to manpower, shorten the detection time, significantly improve detection efficiency, coordinate heating automatically
After instrument, it is also possible to large-scale use.
Below in conjunction with the accompanying drawings aluminium foil type medicament of the present utility model residual quick measuring card is described further.
Accompanying drawing explanation
Fig. 1 is the stereochemical structure partial cutaway schematic of this utility model aluminium foil type medicament residual quick measuring card;
Fig. 2 is the another perspective view of this utility model aluminium foil type medicament residual quick measuring card.
Detailed description of the invention
As shown in Figure 1 and Figure 2, this utility model aluminium foil type medicament residual quick measuring card include can the aluminium foil 1 of doubling, this aluminium foil 1
Shape can be rectangle or square, the present embodiment illustrates as a example by rectangle.Aluminium foil 1 is divided into along its fold line and holding
Tabletting 11 and compression sheet 12, pressure-bearing plate 11 is fixed with indophenols acetas tablet 2, compresses and is fixed with acetylcholine esterase tablet on sheet 12
3, when aluminium foil 1 is along fold line doubling, acetylcholine esterase tablet 3 can be fitted with indophenols acetas tablet 2, acetylcholine esterase tablet 3, indigo
It is coated with the protecting film 4 of layer of transparent on phenol acetas tablet 2, prevents quick measuring card to be contaminated by dust, during use, by protecting film 4
Remove.
Preferably, for ease of the stability after placing tablet and ensureing tablet placement, it is to avoid tablet position is moved, pressure-bearing plate
11, the middle part compressing sheet 12 is provided with the depressed part that position is relative, indophenols acetas tablet 2, acetylcholine esterase tablet 3 bottom embedding
Enter in depressed part.So, after tablet is placed on aluminium foil 1, position is fixed, and is not easy to mobile, it is ensured that the effectiveness of detection during folding
And accuracy.In like manner, for further enhancing the stability of tablet position, protecting film 4 is provided with relative with depressed part position
Lobe, indophenols acetas tablet 2, the top of acetylcholine esterase tablet 3 embed in lobe.So, tablet is limited to recessed
In the space formed behind the portion of falling into and lobe docking, it is less susceptible to mobile.
The Cleaning Principle of quick measuring card of the present utility model is: it is acetic acid and indigo that acetylcholine esterase can be catalyzed indophenols Acetate hydrolysis
Phenol, organophosphor or carbamate have inhibitory action to acetylcholine esterase, make catalysis, hydrolysis, the process of variable color change
Become, thus can determine whether out the existence whether having high dose organophosphor or carbamate chemicals for agriculture in sample.
Use this quick measuring card to carry out detection and have a following two method:
One, overall algoscopy
A, choose representational vegetable sample, wipe surface earth, be cut into the square fragment of about 1cm, take 5g and put into
In bottle with cap, add 10ml pure water or buffer, shake 50 times, stand more than 2min.
B, take a piece of quick measuring card, tear protecting film 4 off, pick extract with acetylcholine esterase tablet 3, place 10min carried out above
Pre-reaction, when having ready conditions, places 10min in 37 DEG C of Thermotank devices, and acetylcholine esterase tablet 3 surface after pre-reaction must be protected
Hold moistening.
C, by quick measuring card doubling, pinch 2min with hands or in thermostat, place 2min, making indophenols acetas tablet 2 and gallbladder
Alkali esterase tablet 3 overlapping reacts, and changes sentence read result according to the color of acetylcholine esterase tablet 3.
D, every batch of mensuration should set the blank card of a pure water or buffer.
Two, surface measurements method
A, the earth wiped on vegetable, 2~3 eluents (distilled water), at vegetable surface, are being dripped with another sheet vegetable
Rub gently at liquid.
B, take after a piece of quick measuring card tears protecting film 4 off, the drop on vegetable is dropped on acetylcholine esterase tablet 3.
C, placement 10min pre-reaction carried out above, place 10min, pre-reaction in the thermostat of 37 DEG C when having ready conditions
After acetylcholine esterase tablet 3 surface must keep moistening (time inadequate, adding one again).
D, by quick measuring card doubling, pinch 2min or with thermostat constant temperature 2min with hands, make indophenols acetas tablet 2 and choline
Esterase tablet 3 overlapping reacts.
E, every batch of mensuration should set the blank card of an eluent or distilled water, to make reference.
Result judges:
Comparing with blank card, acetylcholine esterase tablet 3 invariant color or the most light blue positive findings that is, constant indigo plant is
Strong positive result, illustrates that persticide residue is higher, aobvious light blue for weak positive findings, illustrates that persticide residue is relatively low.Gallbladder
Alkali esterase tablet 3 becomes sky blue or identical with blank card, for negative findings.
Subordinate list 1 quick measuring card lowest detectable limit (unit mg/kg) to several common pesticides
Bayer 71628 | 1.7 | Orthene | 3.5 | Isocarbophos | 3.1 | Parathion | 1.7 | Rogor | 1.3 |
Azodrin | 2.5 | Malathion | 2.0 | Dichlorvos | 0.3 | Metrifonate | 0.3 | ||
Furadan | 0.5 | Sevin | 2.5 | The good winter in year | 1.0 | Omethoate | 2.3 |
In sum, quick measuring card of the present utility model is the standard of the Fast Determination of Pesticide Residue announced for 2003 with country
Method is principle, utilizes the reagent paper that the acetylcholine esterase sensitive to organophosphor and carbamate height and developer are made,
Now passing through research and development for many years makes the sensitivity of this reagent paper higher, and faster, the holding time is longer for response speed, allows based on this principle
Pesticide residue fast detection card have easy to operate, be not required to particular formulation reagent, be not required to professional training, detection sensitivity high,
It it is the places such as vegetable production base, the market of farm produce, supermarket, school, hotel, the factory first-selection that is used for quickly detecting pesticide residues.
So, quick measuring card of the present utility model can be used for the nuisances such as veterinary antibiotics, Pesticide Residues In Grain, residue of veterinary drug, additive
The detection of matter, can be civilian, it is also possible to for food safety detection mechanism, can with Rapid identification pesticide residues, residue of veterinary drug,
Whether the harmful substances such as additive exceed standard.
Embodiment described above is only to be described preferred implementation of the present utility model, not to this practicality
Novel scope is defined, and on the premise of without departing from this utility model design spirit, those of ordinary skill in the art are to this
Various deformation that the technical scheme of utility model is made and improvement, all should fall into the protection that this utility model claims determine
In the range of.
Claims (4)
1. aluminium foil type medicament residual quick measuring card, it is characterised in that: include can the aluminium foil (1) of doubling, described aluminium foil (1) is along it
Fold line is divided into pressure-bearing plate (11) and compresses sheet (12), and described pressure-bearing plate (11) is fixed with indophenols acetas tablet (2), described
Compress and be fixed with acetylcholine esterase tablet (3) on sheet (12), when described aluminium foil (1) is along fold line doubling, described acetylcholine esterase tablet
(3) can fit with indophenols acetas tablet (2), described acetylcholine esterase tablet (3), indophenols acetas tablet (2) are coated with
The protecting film (4) of layer of transparent.
Aluminium foil type medicament the most according to claim 1 residual quick measuring card, it is characterised in that: described pressure-bearing plate (11), compression
The middle part of sheet (12) is provided with the depressed part that position is relative, described indophenols acetas tablet (2), the end of acetylcholine esterase tablet (3)
Portion embeds in described depressed part.
Aluminium foil type medicament the most according to claim 2 residual quick measuring card, it is characterised in that: described protecting film (4) is upper to be arranged
Have a lobe relative with described depressed part position, described indophenols acetas tablet (2), acetylcholine esterase tablet (3) top embedding
Enter in described lobe.
Aluminium foil type medicament the most according to any one of claim 1 to 3 residual quick measuring card, it is characterised in that: described aluminium foil
(1) be shaped as rectangle or square.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201620614610.5U CN205720001U (en) | 2016-06-21 | 2016-06-21 | Aluminium foil type medicament residual quick measuring card |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201620614610.5U CN205720001U (en) | 2016-06-21 | 2016-06-21 | Aluminium foil type medicament residual quick measuring card |
Publications (1)
Publication Number | Publication Date |
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CN205720001U true CN205720001U (en) | 2016-11-23 |
Family
ID=57316512
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201620614610.5U Expired - Fee Related CN205720001U (en) | 2016-06-21 | 2016-06-21 | Aluminium foil type medicament residual quick measuring card |
Country Status (1)
Country | Link |
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CN (1) | CN205720001U (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108398426A (en) * | 2018-03-15 | 2018-08-14 | 鲁东大学 | A kind of simple rapid detection for pesticide residue device and its application |
-
2016
- 2016-06-21 CN CN201620614610.5U patent/CN205720001U/en not_active Expired - Fee Related
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108398426A (en) * | 2018-03-15 | 2018-08-14 | 鲁东大学 | A kind of simple rapid detection for pesticide residue device and its application |
CN108398426B (en) * | 2018-03-15 | 2021-03-23 | 鲁东大学 | Simple pesticide residue rapid detection device and application thereof |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CP01 | Change in the name or title of a patent holder | ||
CP01 | Change in the name or title of a patent holder |
Address after: 264000 Airport Road, Zhifu, Shandong, No. 80, No. Patentee after: Shandong Qingyun experimental consumables Co.,Ltd. Address before: 264000 Airport Road, Zhifu, Shandong, No. 80, No. Patentee before: YANTAI QINGYUN INSTRUMENTS EQUIPMENT Co.,Ltd. |
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CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20161123 |