CN205719924U - Spectrum detection instrument sample room - Google Patents

Spectrum detection instrument sample room Download PDF

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Publication number
CN205719924U
CN205719924U CN201620321002.5U CN201620321002U CN205719924U CN 205719924 U CN205719924 U CN 205719924U CN 201620321002 U CN201620321002 U CN 201620321002U CN 205719924 U CN205719924 U CN 205719924U
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CN
China
Prior art keywords
sample room
sample
detection instrument
spectrum detection
room
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Expired - Fee Related
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CN201620321002.5U
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Chinese (zh)
Inventor
吴松楠
陈迎曦
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Suzhou Lei Xu Electro-Optical Technology Inc (us) 62 Martin Road Concord Massachusetts 017
Original Assignee
Suzhou Lei Xu Electro-Optical Technology Inc (us) 62 Martin Road Concord Massachusetts 017
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Priority to CN201620321002.5U priority Critical patent/CN205719924U/en
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Abstract

This utility model relates to a kind of spectrum detection instrument sample room, includes sample room body, wherein: sample room body is spheroid, and sample room body is provided with exciting light entrance, flashlight outlet, sample room connector.Meanwhile, this internal optics diffuse-reflectance inner surface structure that is provided with of sample room, this internal sample room inner bag that is provided with of sample room, sample room inner bag is provided with sample injection port, sample flow export.Thereby, it is possible to meet gas, liquid hold test needs, it is achieved the diversification of test sample.Further, the interaction of sample and exciting light can be effectively improved and amplify spectral signal, thus improve spectral signal intensity and reduce signal noise.Furthermore, unitary construction is simple, it is easy to assembling manufacturing, it is simple to safeguards, can coordinate various spectrum detection instrument that the sample in sample room is carried out spectral detection and analysis.

Description

Spectrum detection instrument sample room
Technical field
This utility model relates to a kind of sample room, particularly relates to a kind of spectrum detection instrument sample room.
Background technology
Spectral detection is widely used in various research and production work as a kind of quick, accurate, lossless detection means In the middle of making.During detection, it is common that with specific excitation light irradiation sample, sample and exciting light effect, then pass through spectrum Instrument detects its transmission light, reflection light, scattered light.The accuracy of testing result is except by the sensitivity of equipment, reliability sum According to the preparation being also highly dependent on sample beyond the accuracy impact analyzed.Generally solid sample density big and with exciting light Effect is strong, and therefore spectral signal is strong, noise is low, and testing result is the most accurate.Major part gas, fluid density are relatively low, with sharp Luminous effect is more weak, and therefore spectral signal is the most weak, have impact on the accuracy of testing result.
In existing embodiment, in order to obtain accurate gas, liquid spectral detection result, generally in experiment Time need to provide substantial amounts of sample, then through special sample treatment (such as being liquefied by gaseous sample), then with extremely strong sharp The luminous sample that irradiates obtains certain signal intensity.Meanwhile, need to recycle the sensitiveest spectrogrph to detect.
Thus, such traditional detection method not only wastes substantial amounts of sample, and too strong exciting light is also easy to sample Product burn out, and highly sensitive spectrogrph also improves the cost of experiment.
Utility model content
For solving above-mentioned technical problem, the purpose of this utility model is to provide a kind of spectrum detection instrument sample room.
Spectrum detection instrument sample room of the present utility model, includes sample room body, wherein: described sample room body is ball Body, described sample room body is provided with exciting light entrance, flashlight outlet, sample room connector, and described sample room is the most internal Being provided with optics diffuse-reflectance inner surface structure, this internal sample room inner bag that is provided with of described sample room, on the inner bag of described sample room It is provided with sample injection port, sample flow export.
Further, above-mentioned spectrum detection instrument sample room, wherein, described optics diffuse-reflectance inner surface is configured to optics and overflows Reflectance coating, described optics diffuse-reflectance coating is paint solidification film layer.
Further, above-mentioned spectrum detection instrument sample room, wherein, described optics diffuse-reflectance inner surface structure includes Basic unit, is distributed some polyhedral structures in described basic unit.
Further, above-mentioned spectrum detection instrument sample room, wherein, described polyhedral structure is cube, pyramid, rib One or more in post combine.
Further, above-mentioned spectrum detection instrument sample room, wherein, the outlet of described exciting light entrance, flashlight, sample Room connector, sample injection port, sample flow export, for open type opening;
Or, the outlet of described exciting light entrance, flashlight, sample room connector, sample injection port, sample flow export, all Being provided with independent lid, described lid can pass through exciting light and/or be flashlight.
Yet further, above-mentioned spectrum detection instrument sample room, wherein, described sample room inner bag is spheroid.
By such scheme, this utility model at least has the advantage that
1, disclosure satisfy that gas, holding of liquid test needs, it is achieved the diversification of test sample.
2, the interaction of sample and exciting light can be effectively improved and amplify spectral signal, thus it is strong to improve spectral signal Spend and reduce signal noise.
3, unitary construction is simple, it is easy to assembling manufacturing, it is simple to safeguard, various spectrum detection instrument can be coordinated in sample room Sample carry out spectral detection and analysis.
Described above is only the general introduction of technical solutions of the utility model, in order to better understand skill of the present utility model Art means, and can being practiced according to the content of description, below with preferred embodiment of the present utility model and coordinate accompanying drawing detailed Describe in detail bright as after.
Accompanying drawing explanation
Fig. 1 is the structural representation of spectrum detection instrument sample room.
Fig. 2 is the structural representation of optics diffuse-reflectance inner surface structure.
Fig. 3 is that sample room body is briefly described the structural representation into closing empty ball.
Fig. 4 is the light path operating diagram of sample room.
In figure, the implication of each reference is as follows.
1 sample room body 2 exciting light entrance
3 flashlights export 4 sample room connectors
5 optics diffuse-reflectance inner surfacies construct 6 sample room inner bags
7 sample injection port 8 sample flow exports
9 basic unit 10 cubes
11 pyramid 12 prisms
13 lids
Detailed description of the invention
Below in conjunction with the accompanying drawings and embodiment, detailed description of the invention of the present utility model is described in further detail.Below Embodiment is used for illustrating this utility model, but is not limited to scope of the present utility model.
Such as the spectrum detection instrument sample room of Fig. 1 to 4, including sample room body 1, its unusual part is: sample Room body 1 is spheroid, and sample room body 1 is provided with exciting light entrance 2, flashlight outlet 3, sample room connector 4.Meanwhile, In order to effectively promote light radiation effect, in sample room body 1, it is provided with optics diffuse-reflectance inner surface structure 5.Further, examine Consider the facility to the detection of follow-up sample presentation, in sample room body 1, be provided with sample room inner bag 6, sample room inner bag 6 is provided with sample Product inlet 7, sample flow export 8.
From the point of view of this utility model one preferably embodiment, optics diffuse-reflectance coating can be used to constitute optics diffuse-reflectance Inner surface structure 5.Specifically, for the ease of manufacturing, optics diffuse-reflectance coating is paint solidification film layer.Further, real in reality Shi Shi, also can use the material of other optics diffusing characteristic diffusers to constitute this film layer, as long as meeting necessary diffuse-reflectance.
Meanwhile, the structural member of non-coating type can also be used to realize effective diffuse-reflectance.Specifically, such optics is unrestrained anti- Penetrate inner surface structure 5 and include basic unit 9, some polyhedral structure in basic unit 9, is distributed.In order to promote diffuse-reflectance effect, Realize Uniform Irradiation, the polyhedral structure involved by this utility model be the one in cube 10, pyramid 11, prism 12 or Multiple combination.
From the point of view of further, in order to realize the detection needs of quick sample presentation, sampling, exciting light entrance 2, flashlight outlet 3, sample Product room connector 4, sample injection port 7, sample flow export 8, for open type opening.In other words, this kind of open type opening is similar to Cavity structure, actual moulding, bore can configure according to subsequent use demand.Certainly, it is contemplated that some special inspection Survey and need, it is desirable to effective confined space is provided, at exciting light entrance 2, flashlight outlet 3, sample room connector 4, sample Inlet 7, sample flow export 8, be equipped with independent lid 13.Further, the lid 13 that this utility model uses can be through exciting Light and/or be flashlight.
From the point of view of further, it is contemplated that the thing to be detected placed in sample room inner bag 6 just can be excited light and flashlight Often irradiation, does not affect Detection results, and sample room inner bag 6 can also be for spheroid, and it can pass through exciting light and flashlight.
Operation principle of the present utility model is as follows:
Can be briefly described by sample room body as closing empty ball, its cross sectional representation is as shown in Figure 3.Wherein, dA1And dA2 For two infinitely small bins of inner surface, the distance of two bins is S, and the radius of ball is R, and the radial direction of ball is face The normal direction of unit, the angle between radius R and distance S is a.
Here, suppose that bin has the characteristic of Ideal Diffuse Reflection Lambertian.In other words, bin unit in any direction is stood Light radiation in body angle is proportional to cos (a).Wherein, a be bin normal direction with emergent light direction add angle, total light yield is proportional to π.And And, in the middle of actual application, the situation of general Rough Horizontal Plane is the most close with this.Thus, bin dA1The light launched is by bin dA2Receive Ratio is
As can be seen here, in ball, any bin is identical from the light radiation received by another bin any, itself and angle Unrelated, unrelated with launching bin.If by infinitely small bin dA2Change the area A of limited size into2, then result above becomes face Long-pending A2The ratio receiving light isWherein ASArea for ball.Thus it is not difficult to find out, if (reality should with diffuse-reflectance It being matsurface in) face constitutes the inner surface of ball, and the light radiation that its internal any bin receives is identical, the most uniformly 's.
From the point of view of the sample room schematic diagram shown in Fig. 4.Wherein AiFor exciting light entrance port, AeFor flashlight exit portal, A For exciting light direct projection area, ASFor ball inner surface area, ρ is reflectance, FiFor exciting light flux.Also assume that bin has reason Think the characteristic of diffuse-reflectance Lambertian, then face to be illuminated amasss the brightness-formula of A and isWherein π is normalizing constant.
Assume AiAnd AeArea and ASCompare less, and set ball inner surface as Ideal Diffuse Reflection, according to previous Fig. 3's Specifically describe, the light radiation that ball inner surface receives everywhere is identical, then after a diffuse-reflectance ball inner surface receive total Luminous flux isWherein f is AiAnd AeArea and with ball surface area ASRatio Example.
In like manner, the total light flux that the ball inner surface produced after n-th reflection receives is Fiρn(1-f)n.N secondary reflection is produced The total light flux that raw ball inner surface receives is added and obtainsIt is assumed here that f < 1 (typically smaller than 10%).
Therefore, the brightness of ball inner surface is WhereinAs can be seen here after repeatedly diffuse-reflectance the brightness of inner surface from incipientRise toI.e. improve M times.
For example, it is that 5% (the area sum of exciting light entrance port and flashlight exit portal accounts for ball gross area ratio as f Example), when reflection coefficient is 98%, M is 14, i.e. signal intensity improves 14 times, and this is attributed to the most anti-at ball inner surface of light Penetrate.
From the point of view of actually used, in application principles above to spherical sample room provided by the utility model, a branch of low The exciting light (or detection light) of power, improves 14 times at ball inner surface through multiple reflections, brightness, can excite more sample Spectral signal.In like manner, certain sample spectral signals is also exaggerated 14 times through multiple reflections, and both are multiplied obtained signal To be original 196 times.Therefore, this sample room can be effectively improved the signal collection efficiency of portable measurement equipment and measure essence Degree.
By above-mentioned character express and combine accompanying drawing it can be seen that this utility model is gathered around has the following advantages:
1, disclosure satisfy that gas, holding of liquid test needs, it is achieved the diversification of test sample.
2, the interaction of sample and exciting light can be effectively improved and amplify spectral signal, thus it is strong to improve spectral signal Spend and reduce signal noise.
3, unitary construction is simple, it is easy to assembling manufacturing, it is simple to safeguard, various spectrum detection instrument can be coordinated in sample room Sample carry out spectral detection and analysis.
The above is only preferred implementation of the present utility model, is not limited to this utility model, it is noted that For those skilled in the art, on the premise of without departing from this utility model know-why, it is also possible to do Going out some improvement and modification, these improve and modification also should be regarded as protection domain of the present utility model.

Claims (6)

1. spectrum detection instrument sample room, includes sample room body (1), it is characterised in that: described sample room body (1) is ball Body, described sample room body (1) is provided with exciting light entrance (2), flashlight outlet (3), sample room connector (4), described It is provided with optics diffuse-reflectance inner surface structure (5) in sample room body (1), in described sample room body (1), is provided with sample room Inner bag (6), described sample room inner bag (6) is provided with sample injection port (7), sample flow export (8).
Spectrum detection instrument sample room the most according to claim 1, it is characterised in that: described optics diffuse-reflectance inner surface constructs (5) being optics diffuse-reflectance coating, described optics diffuse-reflectance coating is paint solidification film layer.
Spectrum detection instrument sample room the most according to claim 1, it is characterised in that: described optics diffuse-reflectance inner surface constructs (5) including basic unit (9), described basic unit is distributed some polyhedral structures on (9).
Spectrum detection instrument sample room the most according to claim 3, it is characterised in that: described polyhedral structure is cube (10), one or more in pyramid (11), prism (12) combine.
Spectrum detection instrument sample room the most according to claim 1, it is characterised in that: described exciting light entrance (2), flashlight Outlet (3), sample room connector (4), sample injection port (7), sample flow export (8), for open type opening;
Or, described exciting light entrance (2), flashlight outlet (3), sample room connector (4), sample injection port (7), sample stream Outlet (8), is equipped with independent lid (13).
Spectrum detection instrument sample room the most according to claim 1, it is characterised in that: described sample room inner bag (6) is spheroid.
CN201620321002.5U 2016-04-18 2016-04-18 Spectrum detection instrument sample room Expired - Fee Related CN205719924U (en)

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Application Number Priority Date Filing Date Title
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105823731A (en) * 2016-04-18 2016-08-03 苏州镭旭光电科技有限公司 Sample chamber of efficient spectral detection instrument

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105823731A (en) * 2016-04-18 2016-08-03 苏州镭旭光电科技有限公司 Sample chamber of efficient spectral detection instrument

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20161123

Termination date: 20170418

CF01 Termination of patent right due to non-payment of annual fee