CN205684030U - A kind of nano hydrotalcite in-situ synthesized reaction pool device - Google Patents

A kind of nano hydrotalcite in-situ synthesized reaction pool device Download PDF

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Publication number
CN205684030U
CN205684030U CN201620684949.2U CN201620684949U CN205684030U CN 205684030 U CN205684030 U CN 205684030U CN 201620684949 U CN201620684949 U CN 201620684949U CN 205684030 U CN205684030 U CN 205684030U
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China
Prior art keywords
main casing
hole
face
fixed
pressed against
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Expired - Fee Related
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CN201620684949.2U
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Chinese (zh)
Inventor
胡保卫
盛国栋
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Zhejiang Tylenol Environment Repair Co Ltd
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University of Shaoxing
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  • Water Treatment By Sorption (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)

Abstract

The utility model discloses a kind of nano hydrotalcite in-situ synthesized reaction pool device, it includes main casing and top blind flange, top blind flange is fixed on the end face of main casing, three material feeding tubes have been connected on the top sidewall of main casing, feed tube connects in top blind flange, liquid outlet connects on the middle part sidewall of main casing, the end face of top blind flange is fixedly arranged in the middle of stirring motor, the output shaft of stirring motor extends downwardly from the bottom surface of top blind flange, the bottom of the output shaft of stirring motor has upper spline hole, the end face of the base plate of main casing is fixed with fixed block, there is in the middle part of the end face of fixed block stairstepping through hole, bearing is arranged in the top large diameter hole section of stairstepping through hole, the outer ring of bearing is fixed on the medial wall of top large diameter hole section of stairstepping through hole.Nano hydrotalcite raw material is directly synthesized in main casing and closes impurity removing with the arsenic pollutant effluents in main casing by it, its high adsorption capacity, good purification.

Description

A kind of nano hydrotalcite in-situ synthesized reaction pool device
Technical field:
This utility model relates to polluting processing technology field, and a kind of nano hydrotalcite fabricated in situ is anti- Answer pool device.
Background technology:
In recent years, arsenic the environmental pollution caused is more and more concerned.On the one hand arsenic pollute by rock decay, volcano eruption Produce etc. natural cause.Prior come from industrial and agricultural production, such as arsenic with containing the exploitation of arsenic metal, smelting, with in glass, face Making raw material with arsenic or arsenic compound in the production process such as material, former medicine, paper, these can form substantial amounts of arsenic-containing waste water and give up Slag, serious environment pollution.Arsenic-containing waste water can further contaminated soil.The compound of arsenic all has high toxicity, trivalent arsenide compound ratio Other arsenic compound toxicity are higher.Therefore, it is badly in need of a kind of recovery technique of development As polluted soil is effectively administered.
At present, solidification and stabilization is considered as a kind of efficient, simple to operate, energy technology that quickly rehabilitating soil arsenic pollutes. In solidification and stabilization technology, develop and develop that have the stabilisation adsorbent of high-adsorption-capacity to arsenic be core skill therein Art.
Nano material is a kind of new function material that development in recent years is got up and received significant attention, and nano material has Higher specific surface area and chemism, therefore, nano material itself has the strongest absorbability to arsenic, than general absorption The adsorption capacity that material is bigger, and within the shorter response time, i.e. can reach adsorption equilibrium.Nano hydrotalcite specific surface area Greatly, thermal stability is good, and interlayer anion can be exchanged with each other, can highly effective absorption fixed arsenic.But, conventional skill Art is typically first to synthesize nano hydrotalcite, then puts into arsenic Polluted area and repairs, and such complex process, cost is high.
Utility model content:
The purpose of this utility model is to overcome the deficiencies in the prior art, it is provided that a kind of nano hydrotalcite in-situ synthesized reaction pond Device, nano hydrotalcite raw material is directly synthesized in main casing and closes impurity removing with the arsenic pollutant effluents in main casing by it, Its high adsorption capacity, good purification.
This utility model solves the scheme of described technical problem:
A kind of nano hydrotalcite in-situ synthesized reaction pool device, it includes main casing and top blind flange, and top blind flange is fixed On the end face of main casing, the top sidewall of main casing having connected three material feeding tubes, feed tube connects in top blind flange On, liquid outlet connects on the middle part sidewall of main casing, and the end face of top blind flange is fixedly arranged in the middle of stirring motor, stirring motor Output shaft extends downwardly from the bottom surface of top blind flange, and the bottom of the output shaft of stirring motor has upper spline hole, the base plate of main casing End face be fixed with fixed block, there is in the middle part of the end face of fixed block stairstepping through hole, bearing is arranged on the top of stairstepping through hole In large diameter hole section, the outer ring of bearing is fixed on the medial wall of top large diameter hole section of stairstepping through hole, central rotational block Sleeve is in the inner ring of bearing and on the medial wall of the inner ring that is fixed on bearing, and the bottom surface of central rotational block is fixed with wearing layer, Wearing layer is pressed against on the bottom surface of main casing, has lower splined hole, the two ends of second(-)motion shaft in the middle part of the end face of central rotational block Having spline protruded to start, two spline protrudeds sleeve of starting is in corresponding upper spline hole or lower splined hole, solid on second(-)motion shaft Surely there is agitator arm.
The middle part of described second(-)motion shaft has spline shaft, on the second(-)motion shaft at the upper and lower of spline shaft Form spiro union portion.
The middle part of described agitator arm has spline through hole, and spline shaft sleeve, in the spline through hole of agitator arm, is spent Being bolted with on the spiro union portion of the lower section in key axle portion and be pressed against nut and clamp nut, the top end face being pressed against nut is pressed against agitator arm Bottom surface, middle part on, the end face of clamp nut is pressed against on the bottom surface being pressed against nut, and the top of spline shaft is inserted with spacer, every The bottom surface of set is pressed against the middle top surface of agitator arm, the spiro union portion of the top of spline shaft is bolted with two and is mutually pressed against Fixing nut, the bottom surface of the fixing nut of lower section is pressed against on the end face of spacer.
The top of described fixed block is fixed with protection set, and second(-)motion shaft sleeve, in protection set, protects the medial wall of set On the annular groove that has is nested with primary seal circle, primary seal circle is pressed against on the lateral wall of second(-)motion shaft.
Prominent effect of the present utility model is:
Compared with prior art, nano hydrotalcite raw material is directly synthesized and dirty with the arsenic in main casing in main casing by it Dye waste water closes impurity removing, its high adsorption capacity, good purification.
Accompanying drawing illustrates:
Fig. 1 is the structural representation of reaction tank device of the present utility model;
Fig. 2 is the partial enlarged drawing of Fig. 1.
Detailed description of the invention:
Embodiment, is shown in as shown in Figure 1 to Figure 2, and a kind of nano hydrotalcite in-situ synthesized reaction pool device, it includes main casing 36 and top blind flange 37, top blind flange 37 is fixed on the end face of main casing 36, and the top sidewall of main casing 36 has connected three Individual material feeding tube 31, feed tube 1 connects in top blind flange 37, and liquid outlet 2 connects on the middle part sidewall of main casing 36, top The end face of portion's cover plate 37 is fixedly arranged in the middle of stirring motor 371, and the output shaft of stirring motor 371 extends downwardly from the end of top blind flange 37 Face, the bottom of the output shaft of stirring motor 371 has upper spline hole 372, and the end face of the base plate of main casing 36 is fixed with fixed block 361, there is in the middle part of the end face of fixed block 361 stairstepping through hole 362, the top that bearing 363 is arranged on stairstepping through hole 362 is the most straight In the section of hole, footpath, the outer ring of bearing 363 is fixed on the medial wall of top large diameter hole section of stairstepping through hole 362, central rotational Block 364 sleeve is in the inner ring of bearing 363 and on the medial wall of the inner ring that is fixed on bearing 363, the bottom surface of central rotational block 364 Being fixed with wearing layer 365, wearing layer 365 is pressed against on the bottom surface of main casing 36, under having in the middle part of the end face of central rotational block 364 Splined hole 366, the two ends of second(-)motion shaft 38 have spline protruded and start 381, and two spline protrudeds start 381 sleeves corresponding upper In splined hole 372 or lower splined hole 366, second(-)motion shaft 38 is fixed with agitator arm 39.
Further, the middle part of described second(-)motion shaft 38 has a spline shaft 382, the top of spline shaft 382 and Spiro union portion 383 is formed on second(-)motion shaft 38 at bottom.
Further, the middle part of described agitator arm 39 has spline through hole, and spline shaft 382 sleeve is at agitator arm In the spline through hole of 39, the spiro union portion 383 of the lower section of spline shaft 382 is bolted with and is pressed against nut 384 and clamp nut 385, The top end face being pressed against nut 384 is pressed against on the bottom surface, middle part of agitator arm 39, and the end face of clamp nut 385 is pressed against and is pressed against spiral shell On the bottom surface of female 384, the top of spline shaft 382 is inserted with spacer 386, and the bottom surface of spacer 386 is pressed against agitator arm 39 Middle top surface, the spiro union portion 383 of the top of spline shaft 382 is bolted with two fixing nuts 387 being mutually pressed against, lower section The bottom surface of fixing nut 384 is pressed against on the end face of spacer 386.
Further, the top of described fixed block 361 is fixed with protection set 30, and second(-)motion shaft 38 sleeve is at protection set In 30, the annular groove that the medial wall of protection set 30 has is nested with primary seal circle 301, during primary seal circle 301 is pressed against Between rotary shaft 38 lateral wall on.
Operation principle: the waste water of arsenic contaminated soil is entered in main casing 36 by feed tube 1, and three feedstock Pipe 31 will be mixed with waste water in magnesium oxide liquid, aluminum chloride liquid and ammonia entrance main casing 36 by delivery pump, thus Directly by fixing for arsenic absorption during synthesis nano hydrotalcite, improve its adsorption effect, then discharge from liquid outlet 2.
Wherein, agitator arm 39 rotates and makes stirring mixing more uniform, and effect is more preferable, and its second(-)motion shaft 38 and Its upper-part all can remove and install, very convenient.
Finally, embodiment of above is merely to illustrate this utility model, and is not limitation of the utility model, relevant skill The those of ordinary skill in art field, in the case of without departing from spirit and scope of the present utility model, it is also possible to make various change Changing and modification, the technical scheme of the most all equivalents falls within category of the present utility model, patent protection model of the present utility model Enclose and should be defined by the claims.

Claims (4)

1. a nano hydrotalcite in-situ synthesized reaction pool device, it is characterised in that: it includes main casing (36) and top blind flange (37), top blind flange (37) is fixed on the end face of main casing (36), the top sidewall of main casing (36) has connected three former Material feed pipe (31), feed tube (1) connects in top blind flange (37), and liquid outlet (2) connects the medial side in main casing (36) On wall, the end face of top blind flange (37) is fixedly arranged in the middle of stirring motor (371), and the output shaft of stirring motor (371) extends downwardly from The bottom surface of top blind flange (37), the bottom of the output shaft of stirring motor (371) has upper spline hole (372), main casing (36) The end face of base plate is fixed with fixed block (361), has stairstepping through hole (362), bearing in the middle part of the end face of fixed block (361) (363) being arranged in the top large diameter hole section of stairstepping through hole (362), the outer ring of bearing (363) is fixed on stairstepping through hole (362), on the medial wall of top large diameter hole section, central rotational block (364) sleeve and is fixed in the inner ring of bearing (363) On the medial wall of the inner ring of bearing (363), the bottom surface of central rotational block (364) is fixed with wearing layer (365), wearing layer (365) it is pressed against on the bottom surface of main casing (36), there is in the middle part of the end face of central rotational block (364) lower splined hole (366), middle The two ends of rotary shaft (38) have spline protruded and start (381), and two spline protrudeds start (381) sleeve in corresponding upper spline hole (372) or in lower splined hole (366), second(-)motion shaft (38) is fixed with agitator arm (39).
A kind of nano hydrotalcite in-situ synthesized reaction pool device the most according to claim 1, it is characterised in that: described centre The middle part of rotary shaft (38) has spline shaft (382), the second(-)motion shaft (38) at the upper and lower of spline shaft (382) On form spiro union portion (383).
A kind of nano hydrotalcite in-situ synthesized reaction pool device the most according to claim 2, it is characterised in that: described stirring The middle part of impeller (39) has spline through hole, spline shaft (382) sleeve in the spline through hole of agitator arm (39), splined shaft It is bolted with on the spiro union portion (383) of the lower section in portion (382) and is pressed against nut (384) and clamp nut (385), be pressed against nut (384) Top end face be pressed against on the bottom surface, middle part of agitator arm (39), the end face of clamp nut (385) is pressed against and is pressed against nut (384) Bottom surface on, the top of spline shaft (382) is inserted with spacer (386), and the bottom surface of spacer (386) is pressed against agitator arm (39) Middle top surface, the spiro union portion (383) of the top of spline shaft (382) is bolted with two fixing nuts being mutually pressed against (387), the bottom surface of the fixing nut (384) of lower section is pressed against on the end face of spacer (386).
A kind of nano hydrotalcite in-situ synthesized reaction pool device the most according to claim 3, it is characterised in that: described fixing The top of block (361) is fixed with protection set (30), and second(-)motion shaft (38) sleeve, in protection set (30), protects the interior of set (30) Being nested with primary seal circle (301) in the annular groove having on sidewall, primary seal circle (301) is pressed against second(-)motion shaft (38) On lateral wall.
CN201620684949.2U 2016-06-27 2016-06-27 A kind of nano hydrotalcite in-situ synthesized reaction pool device Expired - Fee Related CN205684030U (en)

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CN201620684949.2U CN205684030U (en) 2016-06-27 2016-06-27 A kind of nano hydrotalcite in-situ synthesized reaction pool device

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Application Number Priority Date Filing Date Title
CN201620684949.2U CN205684030U (en) 2016-06-27 2016-06-27 A kind of nano hydrotalcite in-situ synthesized reaction pool device

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108573762A (en) * 2018-04-17 2018-09-25 华东理工大学 The method that electrochemistry prepares hydrotalcite in-situ treatment nuclear power plant radioactive liquid waste containing strontium
CN110217876A (en) * 2019-05-30 2019-09-10 中南大学 A kind of method that zinc-iron houghite processing trivalent arsenic waste water is formed in situ in double drop methods
CN111644098A (en) * 2020-06-27 2020-09-11 台州弘霖工业设计有限公司 Fermentation cylinder rabbling mechanism with many impeller

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108573762A (en) * 2018-04-17 2018-09-25 华东理工大学 The method that electrochemistry prepares hydrotalcite in-situ treatment nuclear power plant radioactive liquid waste containing strontium
CN108573762B (en) * 2018-04-17 2021-11-19 华东理工大学 Method for in-situ treatment of strontium-containing radioactive waste liquid of nuclear power plant by using hydrotalcite prepared by electrochemistry
CN110217876A (en) * 2019-05-30 2019-09-10 中南大学 A kind of method that zinc-iron houghite processing trivalent arsenic waste water is formed in situ in double drop methods
CN110217876B (en) * 2019-05-30 2021-08-13 中南大学 Method for treating trivalent arsenic wastewater by in-situ formation of zinc-iron hydrotalcite through double-drop method
CN111644098A (en) * 2020-06-27 2020-09-11 台州弘霖工业设计有限公司 Fermentation cylinder rabbling mechanism with many impeller

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C14 Grant of patent or utility model
GR01 Patent grant
TR01 Transfer of patent right

Effective date of registration: 20190705

Address after: 312030 Dahe Village, Anchang Town, Keqiao District, Shaoxing City, Zhejiang Province

Patentee after: Zhejiang Tylenol environment repair Co., Ltd.

Address before: No. 508 round City West Road, Shaoxing, Zhejiang Province

Patentee before: Shaoxing University

TR01 Transfer of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20161116

Termination date: 20200627

CF01 Termination of patent right due to non-payment of annual fee