CN205650198U - Draw reation kettle for guaiacol - Google Patents
Draw reation kettle for guaiacol Download PDFInfo
- Publication number
- CN205650198U CN205650198U CN201620422325.3U CN201620422325U CN205650198U CN 205650198 U CN205650198 U CN 205650198U CN 201620422325 U CN201620422325 U CN 201620422325U CN 205650198 U CN205650198 U CN 205650198U
- Authority
- CN
- China
- Prior art keywords
- kettle
- guaiacol
- kettle cover
- inner bag
- liquid level
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- LHGVFZTZFXWLCP-UHFFFAOYSA-N guaiacol Chemical compound COC1=CC=CC=C1O LHGVFZTZFXWLCP-UHFFFAOYSA-N 0.000 title claims abstract description 30
- 229960001867 guaiacol Drugs 0.000 title claims abstract description 15
- 239000007788 liquid Substances 0.000 claims abstract description 22
- 239000011229 interlayer Substances 0.000 claims abstract description 15
- 238000000605 extraction Methods 0.000 claims abstract description 11
- 239000000284 extract Substances 0.000 claims abstract description 6
- 238000007599 discharging Methods 0.000 claims description 10
- 239000000463 material Substances 0.000 claims description 4
- 239000012774 insulation material Substances 0.000 claims description 3
- 239000007921 spray Substances 0.000 claims 1
- 238000005406 washing Methods 0.000 abstract description 7
- 238000005070 sampling Methods 0.000 abstract description 5
- 238000005086 pumping Methods 0.000 abstract description 4
- 238000003756 stirring Methods 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 238000001514 detection method Methods 0.000 abstract description 2
- 235000013599 spices Nutrition 0.000 abstract description 2
- 239000010410 layer Substances 0.000 abstract 2
- 238000004140 cleaning Methods 0.000 abstract 1
- 238000005485 electric heating Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000012452 mother liquor Substances 0.000 abstract 1
- 230000020477 pH reduction Effects 0.000 abstract 1
- 239000003381 stabilizer Substances 0.000 abstract 1
- 239000000523 sample Substances 0.000 description 13
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 229910000831 Steel Inorganic materials 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000010959 steel Substances 0.000 description 3
- WHRZCXAVMTUTDD-UHFFFAOYSA-N 1h-furo[2,3-d]pyrimidin-2-one Chemical compound N1C(=O)N=C2OC=CC2=C1 WHRZCXAVMTUTDD-UHFFFAOYSA-N 0.000 description 2
- 229910000838 Al alloy Inorganic materials 0.000 description 2
- 235000006173 Larrea tridentata Nutrition 0.000 description 2
- 244000073231 Larrea tridentata Species 0.000 description 2
- 229960002126 creosote Drugs 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 239000002304 perfume Substances 0.000 description 2
- 238000010792 warming Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 239000010692 aromatic oil Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000019504 cigarettes Nutrition 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 239000010413 mother solution Substances 0.000 description 1
- 230000035943 smell Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000001117 sulphuric acid Substances 0.000 description 1
- 235000011149 sulphuric acid Nutrition 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Landscapes
- Extraction Or Liquid Replacement (AREA)
Abstract
The utility model relates to a spices and essence production and processing equipment field provides a draw reation kettle for guaiacol, at the bottom of the cauldron body, kettle cover, cauldron, stabilizer blade, its characterized in that: the internal portion of cauldron is equipped with the inner bag, and the cauldron body constitutes the intermediate layer with the inner bag, be equipped with the heliciform electrothermal tube in the intermediate layer, the kettle cover is equipped with motor, feed inlet, manhole, evacuation mouth, drawing liquid mouth, washing mouth, temperature display, liquid level display, observation window. The utility model realizes the stirring and extracting functions through the stirring device, extracts the upper mother liquor through the liquid extraction port, and realizes the washing and simple acidification functions through the cleaning port; in addition, a temperature sensor and a liquid level sensor are adopted, essence in the reaction kettle is monitored in time, and the heating rectification is carried out by utilizing the interlayer electric heating tube in a vacuum pumping state; moreover, through the structural arrangement of the discharge pipeline, the discharge port, the sampling port and the three one-way valves, the essence quality in the sample detection reaction kettle can be very conveniently extracted.
Description
Technical field
This utility model relates to spices and essence manufacturing and processing equipment field, extracts guaiacol reactor particularly to one.
Background technology
Essence is the imitation fruit by synthetic and the concentration aromatic oil of natural perfume material abnormal smells from the patient.It is a kind of artificial perfume.Multiplex
In manufacturing food, cosmetics and Medicated cigarette etc..
From woodsization creosote, extract natural guaiacol be broadly divided into following five processes, be respectively as follows: 1. extractions, will be containing guaiaci lignum
The woodsization creosote suction stainless steel cauldron of phenol, is subsequently adding the sodium hydroxide that concentration is 10%, makes both stir.
2. filter, when, after extract crystallisation by cooling, just extracting upper strata mother solution out.3. clear water washing, and pump out washings.4th road work
Sequence is acid out, puts into concentration and is adjusted to the sulphuric acid of 30%, and is sufficiently stirred for, and acid out is complete, is discharged from bottom by sulfate wastewater,
Thick guaiacol is washed the most again with clear water.4. rectification under vacuum, in the thick guaiacol suction rustless steel rectifying still after washing,
By firing equipment, rectifying still is heated up, vacuum and the temperature one_to_one corresponding collecting natural guaiacol in still.
Five processes typically need to relate to plurality of devices, and cost puts into very big, and work efficiency is the highest.
Summary of the invention
The purpose of this utility model is exactly to solve above-mentioned technical problem, it is provided that a kind of guaiacol reactor that extracts, structure letter
Single, and it is provided simultaneously with extraction, drawing liquid, washing, rectification several functions.
Technical problem of the present utility model is mainly addressed by following technical proposals:
A kind of extraction guaiacol reactor, including kettle, kettle cover, bottom, leg, it is characterised in that: in described kettle
Portion is provided with inner bag, and kettle forms interlayer with inner bag, and described interlayer side is arranged over oil-in, is provided with out below interlayer opposite side
Hydraulic fluid port, is provided with helical form electrothermal tube in described interlayer, described kettle cover is provided with motor, charging aperture, manhole, vacuum orifice, drawing liquid
Mouth, Butterworth Hatch, temperature show, liquid level shows, pressure shows, observation window, and described motor is provided with kettle cover center, this electricity
Machine is provided with the rotating shaft stretching in kettle, and rotating shaft connects blade, and described Butterworth Hatch is located at kettle cover immediate vicinity position, and this Butterworth Hatch is even
Connecing rotary nozzle, rotary nozzle is located in still, and center, described bottom is provided with discharge pipe.
Concrete, described discharge pipe is provided with discharging opening and sample tap, and described discharge pipe, discharging opening, sample tap are equipped with valve
Door.Opening the first valve that discharge pipe is provided with, sample i.e. flows to another twice valve, after closing first valve, then beats
Open sample tap valve and achieve that quantitative sampling.Sampling pipe removably connects between the two with discharge pipe, is i.e. convenient for changing difference
Quantitative probe tube.Discharging opening is directly connected to produce pot-type equipment, not concrete sampled functions the most.
Concrete, described inner bag is easy heat-conducting, such as the material such as aluminium alloy, rustless steel；Described kettle is insulation material, or
At inner wall of kettle, one warming plate is set.
Concrete, described kettle is directly welded and fixed with bottom, and described kettle is bolted with kettle cover, described kettle and still
Lid contact surface is provided with seal washer.
Concrete, the display of described temperature connects kettle internal temperature sensor, and the display of described liquid level connects kettle inside liquid level sensing
Device.
The beneficial effects of the utility model are: realize stirring extraction function by agitating device, then it is female to extract upper strata out by liquid pumping hole
Liquid, and realize washing and simple acid out function by Butterworth Hatch；Additionally have employed temperature sensor and liquid level sensor, pin
Monitoring the essence in reactor in time, and utilize under evacuation state, interlayer electrothermal tube implements heat temperature raising rectification；Furthermore,
Arranged by the structure of discharge pipe, discharging opening, sample tap and three road one-way cocks, easily the reaction of extraction sample detection
Essence quality in still.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
In figure: 1. kettle；2. kettle cover；3. bottom；4. inner bag；5. motor；6. rotating shaft；7. blade；8. electrothermal tube；9. enter
Hydraulic fluid port；10. oil-out；11. charging apertures；12. manholes；13. vacuum orifices；14. liquid pumping holes；15. Butterworth Hatch；16. temperature show
Show；17. liquid levels show；18. observation windows；19. discharge pipes；20. sample taps；21. discharging openings；22. valves；23. interlayers；
24. legs.
Detailed description of the invention
Below by embodiment, and combine accompanying drawing, the technical solution of the utility model is described in further detail.
A kind of extraction guaiacol reactor, including kettle 1, kettle cover 2, bottom 3, leg 24, described kettle 1 is internal to be set
Having an inner bag 4, kettle 1 and inner bag 4 form interlayer 23, and described interlayer 23 side is arranged over oil-in 9, interlayer 23 another
Side-lower is provided with oil-out 10, is provided with helical form electrothermal tube 8 in described interlayer 23, and described kettle cover 2 is provided with motor 5, charging aperture
11, manhole 12, vacuum orifice 13, liquid pumping hole 14, Butterworth Hatch 15, temperature show 16, liquid level shows 17, pressure shows (not
Diagram), observation window 18, described motor 5 is provided with kettle cover 2 center, and this motor 5 is provided with the rotating shaft 6 stretched in kettle 1,
Rotating shaft 6 connects blade 8, and described Butterworth Hatch 15 is located at kettle cover 2 immediate vicinity position, and this Butterworth Hatch 15 connects rotary nozzle (not
Diagram), rotary nozzle is located in still, and center, described bottom 3 is provided with discharge pipe 19.
Described discharge pipe 19 is provided with discharging opening 21 and sample tap 20, described discharge pipe 19, discharging opening 21, sample tap 20
It is equipped with valve 22.Opening the first valve 22 that discharge pipe 19 is provided with, sample i.e. flows to another twice valve 22, closes
After first valve 22, then open sample tap 20 valve 22 and achieve that quantitative sampling.Sampling pipe and discharge pipe 19 liang
Removably connect between person, be i.e. convenient for changing the probe tube of different basis weights.Discharging opening 21 has been directly connected to produce tank the most
Install standby, not concrete sampled functions.
Described inner bag 4 is easy heat-conducting, such as the material such as aluminium alloy, rustless steel；Described kettle 1 is insulation material, or at still
Body 1 inwall arranges a warming plate.Described kettle 1 is directly welded and fixed with bottom 3, and described kettle 1 passes through bolt with kettle cover 2
Fixing, described kettle 1 is provided with seal washer (not shown) with kettle cover 2 contact surface.In described temperature shows 16 connection kettlies 1
Portion's temperature sensor (not shown), described liquid level shows 17 connections kettle 1 inside liquid level sensor (not shown).
The present embodiment is the embodiment of this utility model example, for those skilled in the art, new in this practicality
On the basis of type discloses application process and principle, it is easy to make various types of improvement or deformation, be not limited solely to this practicality
Structure described by novel above-mentioned detailed description of the invention, the most previously described mode is preferred version, and does not have restriction
Property meaning, every according to this utility model made equivalence change with amendment, all this utility model claims scope protect
In the range of protecting.
Claims (4)
1. extract a guaiacol reactor, including kettle, kettle cover, bottom, leg, it is characterised in that: described kettle
Inside is provided with inner bag, and kettle forms interlayer with inner bag, and described interlayer side is arranged over oil-in, is provided with below interlayer opposite side
Oil-out, is provided with helical form electrothermal tube in described interlayer, described kettle cover is provided with motor, charging aperture, manhole, vacuum orifice, takes out
Liquid mouth, Butterworth Hatch, temperature show, liquid level shows, observation window, and described motor is provided with kettle cover center, and this motor is provided with to be stretched
Entering the rotating shaft in kettle, rotating shaft connects blade, and described Butterworth Hatch is located at kettle cover immediate vicinity position, and this Butterworth Hatch connects rotation spray
Head, rotary nozzle is located in still, and center, described bottom is provided with discharge pipe, and described discharge pipe is provided with discharging opening and sample tap,
Described discharge pipe, discharging opening, sample tap are equipped with valve.
A kind of extraction guaiacol reactor the most according to claim 1, it is characterised in that: described inner bag is easy heat conduction
Material, described kettle is insulation material.
A kind of extraction guaiacol reactor the most according to claim 1, it is characterised in that: described kettle is straight with bottom
Connecing and be welded and fixed, described kettle is bolted with kettle cover, and described kettle and kettle cover contact surface are provided with seal washer.
A kind of extraction guaiacol reactor the most according to claim 1, it is characterised in that: the display of described temperature connects
Kettle internal temperature sensor, the display of described liquid level connects kettle inside liquid level sensor.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620422325.3U CN205650198U (en) | 2016-05-11 | 2016-05-11 | Draw reation kettle for guaiacol |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620422325.3U CN205650198U (en) | 2016-05-11 | 2016-05-11 | Draw reation kettle for guaiacol |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205650198U true CN205650198U (en) | 2016-10-19 |
Family
ID=57403570
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620422325.3U Expired - Fee Related CN205650198U (en) | 2016-05-11 | 2016-05-11 | Draw reation kettle for guaiacol |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205650198U (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107602724A (en) * | 2017-09-21 | 2018-01-19 | 浙江海洋大学 | A kind of chitin process units |
| CN108794652A (en) * | 2017-04-26 | 2018-11-13 | 中国科学院过程工程研究所 | A kind of chitin integraterd manufacturing system and its processing method |
| CN110152582A (en) * | 2019-06-18 | 2019-08-23 | 王树东 | A kind of accurate reaction kettle of temperature measurement convenient for sampling |
| CN113201404A (en) * | 2021-04-22 | 2021-08-03 | 江西思派思香料化工有限公司 | Distillation plant is used in spices production and processing of convenient operation |
| CN114232107A (en) * | 2021-12-17 | 2022-03-25 | 沪本新材料科技（上海）有限公司 | Preparation device of wormwood extract and production method of wormwood chinlon polyester fiber |
| CN116240075A (en) * | 2023-04-10 | 2023-06-09 | 华百仕(河北)食品科技有限公司 | Extraction equipment for natural food essence |
-
2016
- 2016-05-11 CN CN201620422325.3U patent/CN205650198U/en not_active Expired - Fee Related
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108794652A (en) * | 2017-04-26 | 2018-11-13 | 中国科学院过程工程研究所 | A kind of chitin integraterd manufacturing system and its processing method |
| CN107602724A (en) * | 2017-09-21 | 2018-01-19 | 浙江海洋大学 | A kind of chitin process units |
| CN110152582A (en) * | 2019-06-18 | 2019-08-23 | 王树东 | A kind of accurate reaction kettle of temperature measurement convenient for sampling |
| CN113201404A (en) * | 2021-04-22 | 2021-08-03 | 江西思派思香料化工有限公司 | Distillation plant is used in spices production and processing of convenient operation |
| CN114232107A (en) * | 2021-12-17 | 2022-03-25 | 沪本新材料科技（上海）有限公司 | Preparation device of wormwood extract and production method of wormwood chinlon polyester fiber |
| CN116240075A (en) * | 2023-04-10 | 2023-06-09 | 华百仕(河北)食品科技有限公司 | Extraction equipment for natural food essence |
| CN116240075B (en) * | 2023-04-10 | 2023-08-22 | 华百仕(河北)食品科技有限公司 | Extraction equipment for natural food essence |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20161019 Termination date: 20170511 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |