CN205635731U - Concise purification device of high simple metal - Google Patents
Concise purification device of high simple metal Download PDFInfo
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- CN205635731U CN205635731U CN201620536454.5U CN201620536454U CN205635731U CN 205635731 U CN205635731 U CN 205635731U CN 201620536454 U CN201620536454 U CN 201620536454U CN 205635731 U CN205635731 U CN 205635731U
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- cylinder
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- pure metal
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Abstract
The utility model relates to a metal purification equipment technical field discloses a concise purification device of high simple metal, including a protection section of thick bamboo, a crystallization section of thick bamboo, cooler pan, a crystallization section of thick bamboo is fixed at protection section of thick bamboo middle part, and place in the cooler pan crystallization section of thick bamboo lower part, and the cooler pan is fixed in protection bobbin base portion, and protection section of thick bamboo wall is provided with connection for vacuum pump and protective gas inlet, still is provided with the observation window on the protection section of thick bamboo. Its simple structure, the purification process is stable, and is pollution -free, and purification efficiency is high, and purity is high.
Description
Technical field
This utility model relates to purification of metals equipment technical field, particularly relates to a kind of high pure metal Refining
Device.
Background technology
High pure metal is the condensation products of modern many new and high technology, along with semiconductor technology, aerospace, wireless
The development of electricity electronics etc., the requirement to high pure metal is more and more higher.In order to improve metal purity, mainly adopt
Chemically and physical method.Wherein physical refining method of purification is mainly: utilize evaporate, solidify, crystallize,
The physical processes such as diffusion, electromigration remove impurity.Wherein can use longitudinal temperature gradient field for gallium
Crystallization process purify, the high purity metal gallium purity of gained is high, and quality is good, but this kind of side of existing employing
It is unstable to there is purification process in the purifying plant that formula purifies, purification process vulnerable to pollution, and purification efficiency is low etc. asks
Topic.
Utility model content
This utility model aims to provide a kind of high pure metal Refining device, well solves above-mentioned asking
Topic, its simple in construction, purification process is stable, pollution-free, and purification efficiency is high, and purity is high.
The technical solution of the utility model is a kind of high pure metal Refining device, including protection cylinder, crystallization
Cylinder, cooler pan, crystallization cylinder is fixed in the middle part of protection cylinder, and crystallization cylinder bottom is placed in cooler pan, cooler pan
Being fixed on bottom protection cylinder, protection cylinder barrel is provided with evacuation interface and gas atmosphere inlet, on protection cylinder
It is additionally provided with observation window.
Further, described crystallization cylinder is round bottom cylinder.
Further, described protection cylinder includes cylinder and is arranged on the cover on cylinder top, described cylinder and cylinder
Sealing ring it is provided with between lid.
Further, described crystallization cylinder and cooler pan are mounted on temperature inductor.
Further, described cooler pan is provided with coolant and flows into pipe and coolant effuser, described cooling
Liquid stream enters pipe and coolant effuser through protection cylinder.
Further, described evacuation interface, gas atmosphere inlet, coolant flow into pipe, coolant outflow
Valve it is mounted on pipe
The beneficial effects of the utility model are: the design of purifying plant of the present utility model, are placed by crystallization cylinder
In protection cylinder, will be placed in the stable environment being hedged off from the outer world and carry out by whole crystallization process, anti-
Stop the external environment pollution to crystallization and purification in purification process；Simultaneously because temperature is susceptible in protection cylinder
Ambient temperature effect, it is ensured that crystallization and purification process stabilization, purification efficiency is high, and purity is high.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model；
In figure: 1. protection cylinder, 11. evacuation interfaces, 12. gas atmosphere inlets, 13. observation windows, 2. crystallization cylinder,
3. cooler pan, 31. coolants flow into pipe, 32. coolant effusers.
Detailed description of the invention
In order to make the purpose of this utility model, technical scheme and advantage clearer, below in conjunction with accompanying drawing,
This utility model is further elaborated.
As it is shown in figure 1, this utility model provides a kind of high pure metal Refining device, including protection cylinder
1, crystallization cylinder 2, cooler pan 3, crystallization cylinder 2 is fixed in the middle part of protection cylinder 1, and crystallization cylinder 2 bottom is placed on
In cooler pan 3, cooler pan 3 is fixed on bottom protection cylinder 1, and protection cylinder 1 barrel is provided with evacuation interface
11 and gas atmosphere inlet 12, protection cylinder 1 is additionally provided with observation window 13.Crystallization cylinder 2 is placed on guarantor
In casing 1, will be placed in the stable environment being hedged off from the outer world and carry out by whole crystallization process, prevent
In the purification process external environment pollution to crystallization and purification；Simultaneously because temperature is susceptible in protection cylinder 1
Ambient temperature effect, it is ensured that crystallization and purification process stabilization, purification efficiency is high.
Crystallization cylinder 2 is round bottom cylinder, and round bottom cylinder is than flat or cone end cylinder and coolant in cooler pan 3
Contact area is big, and good cooling results, speed is fast.Protection cylinder 1 includes cylinder and is arranged on the cylinder on cylinder top
Lid, is provided with sealing ring between cylinder and cover.It is mounted on temperature inductor on crystallization cylinder 2 and cooler pan 3,
The temperature conditions on crystallization cylinder 2 and cooler pan 3 can be understood at any time, it is simple to operator makes corresponding adjustment
Operation.Being provided with coolant on cooler pan 3 and flow into pipe 31 and coolant effuser 32, coolant flows into pipe
31 and coolant effuser 32 through protection cylinder 1, coolant flows into pipe 31 and coolant effuser 32
Design, conveniently according to the temperature in cooler pan 3 in purification process, is adjusted coolant, to ensure
Crystallization cylinder 2 is constantly in most suitable chilling temperature.Evacuation interface 11, gas atmosphere inlet 12,
Coolant flows into and is mounted on valve on pipe 31, coolant effuser 32, it is ensured that protection cylinder 1 seals effect
Really.
During use, first molten metal such as gallium liquid is placed in crystallization cylinder 2, then seals protection cylinder 1, pass through
Evacuation interface 11 on protection cylinder 1 barrel carries out evacuation process to protection cylinder 1, then from protection gas
Body entrance 12 is passed through protective gas such as noble gas, for ensure quality, evacuation and be passed through protective gas can
To carry out repeatedly, it is ensured that without other foreign-matter contaminations and gas in whole protection cylinder 1；Then cooler pan is passed through
Coolant on 3 flows into pipe 31 and is passed through coolant, and molten metal can carry out crystallization and purification, in the process,
Understand crystallization situation at any time by observation window 13 and temperature inductor, flow into pipe 31 and cooling by coolant
Liquid effuser 32 flows in or out coolant, is adjusted chilling temperature, it is ensured that crystalline quality and efficiency.
This utility model purifying plant purification process is stable, pollution-free, and purification efficiency is high, and purity is high.
Certainly, this utility model also can have other various embodiments, without departing substantially from this utility model spirit and
In the case of essence, those of ordinary skill in the art can make various corresponding change according to this utility model
And deformation, but these change accordingly and deform the protection that all should belong to the claim appended by this utility model
Scope.
Claims (6)
1. a high pure metal Refining device, it is characterised in that: include protecting cylinder, crystallization cylinder, cold
But dish, described crystallization cylinder is fixed in the middle part of protection cylinder, and described crystallization cylinder bottom is placed in cooler pan, described
Cooler pan is fixed on bottom protection cylinder, and described protection cylinder barrel is provided with evacuation interface and protective gas enters
Mouthful, described protection cylinder is additionally provided with observation window.
High pure metal Refining device the most according to claim 1, it is characterised in that: described knot
Brilliant cylinder is round bottom cylinder.
High pure metal Refining device the most according to claim 1, it is characterised in that: described guarantor
Casing includes cylinder and is arranged on the cover on cylinder top, is provided with sealing ring between described cylinder and cover.
High pure metal Refining device the most according to claim 1, it is characterised in that: described knot
It is mounted on temperature inductor on brilliant cylinder and cooler pan.
High pure metal Refining device the most according to claim 1, it is characterised in that: described cold
But being provided with coolant on dish and flow into pipe and coolant effuser, described coolant flows into pipe and coolant flows out
Pipe is through protection cylinder.
High pure metal Refining device the most according to claim 5, it is characterised in that take out described in:
Vacuum interface, gas atmosphere inlet, coolant flow into and are mounted on valve on pipe, coolant effuser.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620536454.5U CN205635731U (en) | 2016-06-02 | 2016-06-02 | Concise purification device of high simple metal |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620536454.5U CN205635731U (en) | 2016-06-02 | 2016-06-02 | Concise purification device of high simple metal |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205635731U true CN205635731U (en) | 2016-10-12 |
Family
ID=57051594
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620536454.5U Active CN205635731U (en) | 2016-06-02 | 2016-06-02 | Concise purification device of high simple metal |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205635731U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107022687A (en) * | 2017-05-27 | 2017-08-08 | 郑州大学 | A kind of Smelting magnesium segmented crystallization apparatus |
| CN113652553A (en) * | 2021-08-19 | 2021-11-16 | 武汉拓材科技有限公司 | Production device and method of high-purity gallium |
-
2016
- 2016-06-02 CN CN201620536454.5U patent/CN205635731U/en active Active
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107022687A (en) * | 2017-05-27 | 2017-08-08 | 郑州大学 | A kind of Smelting magnesium segmented crystallization apparatus |
| CN107022687B (en) * | 2017-05-27 | 2018-12-11 | 郑州大学 | A kind of Smelting magnesium segmented crystallization apparatus |
| CN113652553A (en) * | 2021-08-19 | 2021-11-16 | 武汉拓材科技有限公司 | Production device and method of high-purity gallium |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20200811 Address after: 311200 No. 83 Hongken Road, Hongken Farm, Xiaoshan Economic and Technological Development Zone, Hangzhou City, Zhejiang Province Patentee after: Hangzhou kaiyada semiconductor materials Co., Ltd Address before: Jiajiang Xinchang Town hongqicun 614000 Sichuan city in Leshan province 5. Patentee before: LESHAN KAIYADA OPTOELECTRONICS TECHNOLOGY Co.,Ltd. |
|
| TR01 | Transfer of patent right |