CN205614027U - Vacuum melting rapid hardening equipment - Google Patents

Vacuum melting rapid hardening equipment Download PDF

Info

Publication number
CN205614027U
CN205614027U CN201620347917.3U CN201620347917U CN205614027U CN 205614027 U CN205614027 U CN 205614027U CN 201620347917 U CN201620347917 U CN 201620347917U CN 205614027 U CN205614027 U CN 205614027U
Authority
CN
China
Prior art keywords
rotating roller
vacuum
water
vacuum melting
room
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201620347917.3U
Other languages
Chinese (zh)
Inventor
孙宝玉
陈晓东
段永利
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SHENYANG ZHONGBEI VACUUM TECHNOLOGY Co Ltd
Original Assignee
SHENYANG ZHONGBEI VACUUM TECHNOLOGY Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SHENYANG ZHONGBEI VACUUM TECHNOLOGY Co Ltd filed Critical SHENYANG ZHONGBEI VACUUM TECHNOLOGY Co Ltd
Priority to CN201620347917.3U priority Critical patent/CN205614027U/en
Application granted granted Critical
Publication of CN205614027U publication Critical patent/CN205614027U/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Continuous Casting (AREA)

Abstract

The utility model discloses a vacuum melting rapid hardening equipment mainly includes: vacuum feed compartment, vacuum melting room, rotatory roller remove the room, close gold sheet cooling chamber, bin stock device, cooling system, vacuum system, and cooling system does vacuum melting rapid hardening equipment provide the cooling required cooling water or cooling gas, vacuum system links to each other with the vacuum melting room, provides vacuum environment for vacuum melting rapid hardening equipment, be provided with charging basket elevating system, station dial and reciprocating motion's platform truck in the feed compartment of vacuum, the rotatory roller device of during operation water -cooling removes the room from rotatory roller and removes the vacuum melting room, closes the gold sheet cooling chamber and links to each other with the vacuum melting room, is provided with breaker and chilling roll in closing the gold sheet cooling chamber, the bin stock device through the guide valve with close the gold sheet cooling chamber and link to each other. This equipment can be used to make sintered nd -Fe -B rapid hardening alloy, fast quenching neodymium iron boron permanent magnetism powder, soft -magnetic nanocrystalline magnetic, still can be used to use the neodymium iron boron waste material to make the neodymium iron boron permanent magnet.

Description

A kind of vacuum melting rapid hardening equipment
Technical field
The utility model belongs to Advanced Equipment field, particularly relates to a kind of vacuum melting rapid hardening equipment;This equipment is permissible For manufacturing rare earth permanent magnet rapid hardening alloy, fast quenching NdFeB permanet magnetic powder, metal soft Ci powder, vacuum rapid hardening alloy etc..
Background technology
Rare earth permanent-magnetic material, is more and more applied with the magnetic property that it is excellent, is widely used in the nuclear-magnetism of medical treatment Resonance image-forming, computer hard disc driver, sound equipment, mobile phone etc.;With energy-conservation and low-carbon economy requirement, Nd-Fe-B rare-earth permanent magnet Material starts again at auto parts and components, household electrical appliance, energy-conservation and control motor, hybrid vehicle, and field of wind power generation should With.
Nineteen eighty-three, Japan Patent 1,622,492 and 2, first 137,496 disclose Nd-Fe-B rare earth permanent magnetic material, announces The characteristic of Nd-Fe-B rare earth permanent magnetic material, composition and manufacture method, United States Patent (USP) US6,461,565, US6,491,765, US6,537,385, US6,527,874, US5,645,651 also disclose that the manufacture method of Nd-Fe-B rare-earth permanent magnet.
The preparation method manufacturing the RE permanent magnetic alloy that Nd-Fe-B rare earth permanent magnetic material is used typically has two kinds, Yi Zhongshi Alloy molten solution is injected in mould, then by making the ingot mould casting of alloy pig compared with Slow cooling.One is to melt alloy Liquid is cast on the chill roll of rotation, forms the rapid hardening method of rapid hardening alloy thin band or thin slice after chilling.Crystalline substance due to rapid hardening alloy Grain more fine uniform, and Nd-rich phase distribution is good, currently manufactured high performance rare earth permanent-magnetic material typically all uses rapid hardening method Prepare RE permanent magnetic alloy.
United States Patent (USP) US7,585,378 and Chinese patent CN97,217,372.2, CN01,241,237.6 disclose dilute The manufacture method of soil permanent magnet vacuum rapid hardening alloy, neodymium iron boron raw material is cast to tundish after crucible melting, overflows from tundish Aluminium alloy by chill roll cooling rapid hardening form alloy sheet.
But in the existing above-mentioned vacuum melting strip casting manufacturing for rare earth permanent-magnetic material, generally by pure iron, boron The rapid hardening alloy raw materials such as iron, rare earths material and other interpolation metals use disposable entrance crucible to carry out the mode of melting, this Sample in fusion process it is possible that the phenomenon of the more valuable raw material at high temperature volatilization loss such as rare earth;In addition, greatly Raw material is put into crucible in border by compression ring, rare earth material also can be made to aoxidize, add the slag making in melting.Above-mentioned factor affects The utilization rate of precious metal material, causes a certain degree of waste.The vacuum melting that Ai Fake Co., Ltd. of Japan is produced Rapid hardening furnace, although have employed the design of secondary charging, but its purpose is to be filled in crucible internal cause raw material in fusion process and melt The stocking space changed and occur, reaches to increase the effect of batch, and unresolved precious alloy raw material at high temperature loses And the problem that rare earths material melting slag making is serious.
On the other hand, owing to the material cost of rare earth permanent-magnetic material is higher, in industry, researching and developing recovery profit always By the method for the rare earth permanent magnet spent materials such as rare earth permanent magnet substandard products and leftover pieces, in order to reduce the cost of raw material of rare earth permanent-magnetic material, Save existing natural resources.Owing to the degree of oxidation in above-mentioned rare earth permanent magnet spent material is higher, if using these waste materials as molten Refining raw material remelting utilize, can in fusion process, produce substantial amounts of slag, this difficult problem make remelting waste material technique receive restriction and Cannot extensively apply.Therefore, the process of Japan's commonly used non-remelting of relevant enterprise recycles rare earth permanent magnet spent material. For example, ZL99800997.0 and US6,149,861 disclose a kind of method recycling sintered NdFeB waste material, this side In method, carry out to waste material pulverizing, pickling and drying, then calcium reduction process is carried out to this product, is derived from recycling Raw material alloy powder, then regulated its one-tenth be grouped into by adding other alloy powders in this powder, and then manufacture and burn Knot Nd-Fe-B permanent magnet material.ZL02800504.X and US7,056,393 discloses a kind of method utilizing sintered NdFeB substandard products, In the method, use hydrogen decrepitation to carry out coarse crushing to sintered NdFeB substandard products, then make fine powder, then will be by substandard products After the fine powder made mixes with the fine powder that normal proto material is made, make sintered Nd-Fe-B permanent magnet.Above-mentioned non-remelting profit More complicated by the method for waste material not only operation, in addition it is also necessary to the alloy powder of preparation heterogeneity is allocated its composition and improves its burning Knot ability, makes troubles to production process.Prior thing, in this waste material Application way, due to non-remelting, powder that waste material is made In Mo, oxygen and other impurity contents are higher, make the magnetic property of the rare earth permanent-magnetic material thus made be severely impacted.
Content of the invention
The utility model is achieved through the following technical solutions:
A kind of vacuum melting rapid hardening equipment, specifically includes that vacuum charging room, vacuum melting room, rotating roller move room, alloy Piece cooling chamber, Storage appts., cooling system, vacuum system, it is characterised in that: described cooling system is described vacuum melting Rapid hardening equipment provides the cooling water needed for cooling or cooling gas;Described vacuum system is connected with vacuum melting room, is vacuum Vacuum environment needed for melting rapid hardening equipment offer work;Vacuum charging room is arranged on the top of vacuum melting room, adds in vacuum Material indoor are provided with charging basket and charging basket elevating mechanism, and vacuum charging room is connected with vacuum melting room by vacuum valve;Vacuum melts Refining indoor are provided with vacuum melting crucible and switching mechanism, and vacuum melting crucible is arranged on switching mechanism, vacuum melting crucible Flip angle be more than 90 degree;The rotating roller room of movement is connected with vacuum melting room by vacuum separation valve door, and rotating roller moves room Inside being provided with water-cooled rotating roller arrangement, water-cooled rotating roller arrangement can move to vacuum melting room;Alloy sheet cooling chamber is arranged on The lower section of vacuum melting room, alloy sheet cooling chamber is connected with vacuum melting room, is provided with breaker in alloy sheet cooling chamber And chilling roll;Storage appts. is arranged on the lower section of alloy sheet cooling chamber, is provided with material-storage jar in Storage appts., and Storage appts. leads to Cross guide valve to be connected with alloy sheet cooling chamber.
Described vacuum charging indoor are additionally provided with rotating station dial, and station dial is arranged on can be reciprocal On the chassis of movement.
Described vacuum charging indoor are additionally provided with rotating disk, and rotating disk is arranged on chassis, the guide rail of chassis and vacuum charging The door of room is connected, and rotating disk moves together with door.
Described vacuum melting room is horizontal type structure, is provided with body of heater, Qianmen and back door, switching mechanism and vacuum melting room Back door be connected, back door is connected with the body of heater of vacuum melting room, before door opener is provided with for back door by door opener The hydraulic cylinder of rear movement and back door are around the hydraulic cylinder of door opener axis of rotation;Described back door has 2, alternation switch.
In another embodiment, described vacuum melting room is horizontal type structure, is provided with body of heater, Qianmen and back door, Switching mechanism is connected with the back door of vacuum melting room, and back door is connected with the body of heater of vacuum melting room by door opener, and open the door dress Put and be provided with for back door around the hydraulic cylinder of door opener axis of rotation;Described back door has 2, alternation switch.
Described water-cooled rotating roller arrangement comprise tundish, water-cooled rotating roller, bearing, bearing block, device for sealing magnetic fluid, Rotating roller connecting gear;Tundish is connected with bearing block, and bearing block is supported on rotating roller connecting gear;The two of water-cooled rotating roller End has axle, by the bearings in bearing block on bearing block;Bearing block is connected with device for sealing magnetic fluid, water-cooled rotating roller Cooling water be incorporated into water-cooled rotating roller from the device for sealing magnetic fluid of one end, draw from the device for sealing magnetic fluid of the other end; The lower section of rotating roller connecting gear is provided with moving guide rail, and water-cooled rotating roller arrangement moves along guide rail and can move in rotating roller Move between room and vacuum melting room and pause;The moving guide rail arranging below water-cooled rotating roller arrangement and rotating roller move room Door is connected, and the door moving room with rotating roller moves.
Described water-cooled rotating roller arrangement comprises tundish, water-cooled rotating roller, bearing block, device for sealing magnetic fluid, rotation Roller connecting gear;The diameter of described water-cooled rotating roller in the range of 590mm to 1220mm, the linear velocity of water-cooled rotating roller outer rim In the range of 0.8m/s to 60m/s.
Described alloy sheet cooling chamber also comprises cooling chamber cylinder, drive end bearing bracket, rear end cap;Be provided with on cooling chamber cylinder into Material mouth and discharging opening, charging aperture is connected with vacuum melting room, and discharging opening is connected with guide valve, and charging aperture is rectangle, in charging Mouth is provided with breaker;Breaker comprises the rotating shaft rotating against;Chilling roll is Double water-cooled wall construction, interior logical cooling Water, chilling roll inwall is provided with fin, and the axis that described fin is i.e. not parallel to chilling roll is also not orthogonal to axis, Chilling roll rotates forward or reversely rotates.There is axle the rear end of cylinder, and axle passes through rear end cap, arranges between axle and rear end cap Device for sealing magnetic fluid and cooling water is had to introduce and ejector.
It is provided with spiral helicine fin on described chilling roll inwall, also set in the inner space of spiral helicine fin It is equipped with cylinder, the inwall of cylinder is provided with helical form fin;In the helical form fin arranging on cylinder inner wall and chilling roll The hand of spiral of the helical form fin on wall is contrary.
Described vacuum charging indoor are additionally provided with 4 station turnplates, and charging basket is placed on 4 station turnplates, and 4 station turnplates set Putting on chassis, the guide rail of chassis is connected with the door of vacuum charging room, and 4 station turnplates move together with door.
In another embodiment of the present utility model, water-cooled rotating roller arrangement includes tundish, water-cooled rotating roller, water Cold rotating roller is connected with cooling water;Water-cooled rotating roller arrangement also includes little water-cooled rotating roller, and the diameter of little water-cooled rotating roller compares water The diameter of cold rotating roller is little;The axle of little water-cooled rotating roller is parallel with the axle of water-cooled rotating roller and axle upper that be positioned at water-cooled rotating roller Side;The axle of little water-cooled rotating roller and tundish lay respectively at the both sides of the axle of water-cooled rotating roller;Little water-cooled rotating roller is connected with cold But water.
Compared with prior art, the beneficial effects of the utility model:
1., during vacuum melting rapid hardening starts front or vacuum melting rapid hardening, water-cooled rotating roller can move from rotating roller Room moves to vacuum melting room, and this design and method can realize the vacuum melting rapid hardening operation of continous way, reduces operator Member quantity, reduce labour intensity and be obviously improved operating environment, it is often more important that, be conducive to improve rare earth permanent-magnetic material property Energy and uniformity thereof.
2. once vacuumizing raw material under vacuum, repeatedly timesharing adds crucible, has both avoided valuable raw material Vaporization at high temperature, improve again batch.
3. under vacuum raw material is loaded crucible, reduce the oxidative slagging in fusion process, improve noble metal material Expect the utilization rate of especially rare earth material.
4. melting kettle is connected with back door, it is simple to crucible cleaning and repairing, reduces labour intensity, convenient and safe.
5. water-cooled rotating roller uses both-end to support, and improves running accuracy, improves alloy sheet thickness consistent of production Property, hence it is evident that improve properties of product;The sealing of the cooling water at water-cooled rotating roller two ends uses magnet fluid sealing, improves vacuum Under the conditions of sealing reliability.Otherwise once leak, will result in the oxidation of alloy.
6. being provided with fin in alloy sheet chilling roll, alloy sheet chilling roll can rotate forward and also can reversely rotate, In alloy sheet casting and cooling procedure, described alloy sheet chilling roll rotates forward, at alloy sheet from alloy sheet cooling rolling During cylinder is derived, alloy sheet chilling roll reversely rotates;Fully, the temperature that alloy sheet enters material-storage jar is low in alloy sheet cooling, When avoiding discharging, alloy sheet aoxidizes.
Brief description
Fig. 1 is the front view of a kind of vacuum melting rapid hardening equipment in the utility model;
Fig. 2 is the side view of a kind of vacuum melting rapid hardening equipment in the utility model;
Fig. 3 is the top view of a kind of vacuum melting rapid hardening equipment in the utility model;
Fig. 4 is the structural representation of another kind of alloy sheet chilling roll of the present utility model;
Fig. 5 is the front view of another kind of vacuum melting rapid hardening equipment of the present utility model.
Detailed description of the invention
As Figure 1-4, described vacuum melting rapid hardening equipment mainly includes cooling system the 54th, vacuum system the 55th, vacuum Feed compartment the 5th, vacuum melting room the 8th, rotating roller moves the 35th, alloy sheet cooling chamber the 15th, Storage appts. 21, room;Described vacuum charging room 5 tops being arranged on vacuum melting room 8, are provided with charging basket the 4th, charging basket elevating mechanism the 6th, station dial in vacuum charging indoor 5 3rd, the chassis 2 moving back and forth;Station dial 3 is arranged on the chassis 2 that can move back and forth, and the guide rail of chassis 2 and vacuum add The door 1 of material room is connected, and station dial 3 moves together with door 1;Vacuum charging room 5 is by vacuum valve 7 and vacuum melting room 8 It is connected;Described vacuum melting room 8 is provided with body of heater the 10th, Qianmen 26 and back door 11, and Qianmen 26 is provided with guide cover 25, vacuum Being provided with vacuum melting crucible 9 and switching mechanism 12 in working chamber 8, vacuum melting crucible 9 is arranged on switching mechanism 12, vacuum The flip angle of melting kettle 9 is more than 90 degree, and switching mechanism 12 is connected with the back door 11 of vacuum melting room 8, and back door 11 is by opening Door gear 45 is connected with the body of heater 10 of vacuum melting room 8, and door opener 45 is provided with the hydraulic cylinder movable for back door 47 and back door around the hydraulic cylinder 46 of door opener axis of rotation;Back door 11 has two, the door opener 53 at second back door 50 On have the hydraulic cylinder 51 movable for back door and the back door hydraulic cylinder 52 around door opener axis of rotation equally;Second Back door 50 is connected with switching mechanism 49 and the vacuum melting crucible 48 being arranged on switching mechanism 49, and two back doors are alternately opened Close;It is additionally provided with temperature measuring equipment on the body of heater 10 of vacuum melting room 8 and the 37th, smash material device 38 and observation window 39;Rotating roller moves room 35 are connected with vacuum melting room 8 by vacuum separation valve door 36, and rotating roller is provided with water-cooled rotating roller arrangement 29 in moving room 35, Water-cooled rotating roller arrangement 29 drives to move in rotating roller by rotating roller connecting gear 41 and moves between room 35 and vacuum melting room 8 Dynamic;Described water-cooled rotating roller arrangement 29 comprises tundish the 34th, water-cooled rotating roller the 28th, bearing the 31st, bearing block the 32nd, magnet fluid sealing Device the 30th, rotating roller tumbler the 33rd, rotating roller connecting gear 41;Tundish 34 is connected with bearing block 32, and bearing block 32 supports On rotating roller connecting gear 41;There is axle at the two ends of water-cooled rotating roller 28, are supported on bearing blocks 32 by bearing 31;Bearing block 32 are connected with device for sealing magnetic fluid 30, and the cooling water in water-cooled rotating roller 28 introduces from the device for sealing magnetic fluid 30 of one end, Draw from the device for sealing magnetic fluid 30 of the other end;The lower section of rotating roller connecting gear 41 is provided with moving guide rail 40, and water-cooled is revolved Roller-rotating device 29 moves along guide rail 40 and moves in rotating roller and move between room 35 and vacuum melting room 8 and pause;Moving guide rail 40 move room door 27 with rotating roller is connected, and moves in rotating roller and moves with door 27 under the drive of room door drive 42;Close Gold plaque cooling chamber 15 is arranged on the lower section of vacuum melting room 8, and alloy sheet cooling chamber 15 is connected with the body of heater 10 of vacuum melting room 8, Described alloy sheet cooling chamber 15 comprises cooling chamber cylinder the 13rd, drive end bearing bracket the 22nd, rear end cap the 16th, alloy sheet breaker the 24th, alloy Piece chilling roll 14;Being provided with charging aperture and discharging opening on cooling chamber cylinder 13, charging aperture is connected with vacuum melting room 8, discharging Mouth is connected with guide valve 20, and charging aperture is rectangle, and charging aperture is provided with alloy sheet breaker 24;Alloy sheet chilling roll 14 is Double water-cooled wall construction, interior logical cooling water, and cylinder 14 inwall is provided with fin 23, and described fin is both not parallel to close The axis of gold plaque chilling roll 14 is also not orthogonal to axis, alloy sheet chilling roll 14 or rotate forward or reversely rotate Rolling;The rear end of cylinder is provided with power transmission shaft 19, and power transmission shaft 19 passes through rear end cap 16, is provided with magnetic between power transmission shaft and rear end cap 16 Fluid seal apparatus 17 and cooling water introduce and ejector 18;Shown in Fig. 4 is the structure of another kind of alloy sheet chilling roll, It is provided with spiral helicine fin 56 on described alloy sheet chilling roll inwall, also set in the inner space of spiral helicine fin It is equipped with cylinder 57, the inwall of cylinder is provided with helical form fin 58, the helical form fin that the inwall of cylinder is arranged and alloy The hand of spiral of the helical form fin on piece chilling roll inwall is contrary;Described Storage appts. 21 is arranged on alloy sheet cooling chamber The lower section of 15, is provided with material-storage jar in Storage appts. 21, Storage appts. 21 is connected with alloy sheet cooling chamber 15 by guide valve; Equipment of the present utility model also comprises upper mounting plate 43 and lower platform 44.
Fig. 5 is the structural representation of another kind of vacuum melting rapid hardening equipment of the present utility model.In this embodiment, Water-cooled rotating roller arrangement 29 includes tundish the 34th, water-cooled rotating roller 28, is connected with cooling water in water-cooled rotating roller 28;Water-cooled rotating roller Device 29 also includes little water-cooled rotating roller 59, and the diameter of little water-cooled rotating roller 59 is less than the diameter of water-cooled rotating roller 28;Little water-cooled The axle of rotating roller 59 is parallel with the axle of water-cooled rotating roller 28 and the top of axle that is positioned at water-cooled rotating roller 28;Little water-cooled rotating roller 59 Axle and tundish 34 lay respectively at the both sides of axle of water-cooled rotating roller 28;Little water-cooled rotating roller 59 is connected with cooling water.
Further illustrate remarkable result of the present utility model below by the contrast of embodiment.
Embodiment 1
By former to praseodymium neodymium alloy, terbium metal, dysprosium iron, pure iron, ferro-boron, gallium, metal zirconium, metallic cobalt, metallic aluminium, metallic copper Material is configured to Pr by weight percentage6.3Nd23.1Dy2Tb0.6B0.95Co1.2Zr0.12Ga0.1Al0.2Cu0.2FeSurplusAlloy raw material, will Pure iron and ferro-boron load No. 1 charging basket, and pure iron, ferro-boron and a small amount of praseodymium neodymium alloy are loaded No. 2 charging baskets, by praseodymium neodymium alloy, dysprosium iron, Terbium metal, gallium load No. 3 charging baskets, and metal zirconium, metallic cobalt, metallic aluminium, metallic copper are loaded No. 4 charging baskets, afterwards operation bag Include: 4 charging baskets are sent into the vacuum charging room of vacuum melting rapid hardening equipment by (1), open vacuum charging room and vacuum after vacuumizing Vacuum valve between working chamber;(2) by the cooperation of lifting device, 4 station turnplates and the chassis moving back and forth by No. 1 and No. 2 The raw material of charging basket adds the crucible of vacuum melting room under vacuum, is heated to temperature 300-1500 DEG C scope;(3) with aforementioned Method the raw material of No. 3 charging baskets and No. 4 charging baskets is also added the crucible of vacuum melting room, be filled with argon gas and refining afterwards;(4) will The water-cooled rotating roller arrangement that rotating roller moves indoor is sent to vacuum melting room, and the crucible that fascinates passes through tundish by under molten condition Liquation be cast in the outer rim of water-cooled rotating roller formed alloy sheet;(5) alloy sheet leaving water-cooled rotating roller falls conjunction immediately On the alloy sheet breaker of gold plaque cooling chamber, slip into the alloy sheet chilling roll rotating, (6) through broken alloy sheet With the rotation of alloy sheet chilling roll, alloy sheet enters material-storage jar, after closing guide valve afterwards and closing the lid to material-storage jar Material-storage jar removal is completed operation.
Embodiment 2
Will be containing praseodymium neodymium alloy, terbium metal, dysprosium iron, pure iron, ferro-boron, gallium, metal zirconium, metallic cobalt, metallic aluminium, metallic copper Raw material and neodymium iron boron waste material be configured to Pr by weight percentage6.3Nd23.1Dy2Tb0.6B0.95Co1.2Zr0.12Ga0.1Al0.2Cu0.2FeSurplus Alloy raw material, wherein, neodymium iron boron waste material content accounts for the 10-60% of gross weight;Pure iron and ferro-boron are loaded No. 1 charging basket, by neodymium iron Boron waste material loads No. 2 charging baskets, neodymium iron boron slag cleaning plant is loaded No. 3 charging baskets, by praseodymium neodymium alloy, dysprosium iron, terbium metal, metal Gallium, metal zirconium, metallic cobalt, metallic aluminium, metallic copper load No. 4 charging baskets, and operating procedure includes afterwards: charging basket is sent into vacuum by (1) The vacuum charging room of melting rapid hardening equipment, opens the vacuum valve between vacuum charging room and vacuum melting room after vacuumizing;(2) lead to The raw material of No. 1 and No. 2 charging basket is added by cooperation under vacuum that cross lifting device, 4 station turnplates and the chassis moving back and forth Enter the crucible of vacuum melting room, be heated to temperature 1400-1500 DEG C scope and refine;(3) by aforesaid method by No. 3 charging baskets Slag cleaning plant drops to the surface of the crucible liquation of vacuum melting room, allows slag be adsorbed onto on slag cleaning plant, afterwards Slag cleaning plant is mentioned, in income to No. 3 charging baskets, continues to lift up with No. 3 charging baskets, then be put back into 4 station turnplates;(4) use The raw material of No. 4 charging baskets is also added the crucible of vacuum melting room by the method for operating procedure (2), is filled with argon gas and refining afterwards;(5) The water-cooled rotating roller arrangement that rotating roller moves indoor is sent to vacuum melting room, and the crucible that fascinates passes through tundish by molten condition Under liquation be cast in the outer rim of water-cooled rotating roller formed alloy sheet;(6) alloy sheet leaving water-cooled rotating roller is fallen immediately On the alloy sheet breaker of alloy sheet cooling chamber, slip into, through broken alloy sheet, the alloy sheet chilling roll rotating, (7) with the rotation of alloy sheet chilling roll, alloy sheet enters material-storage jar, closes guide valve afterwards and closes the lid to material-storage jar After by material-storage jar removal complete operation.
Embodiment 3
Pure iron, ferro-boron, ferrosilicon, ferro-niobium, metallic copper raw materials by weight are configured to Fe78.4Cu0.6Nb2.5Si9.5B9 Alloy, by pure iron as raw material, ferro-boron, ferrosilicon, No. 1 to No. 3 charging basket of loading, raw material ferro-niobium, metallic copper are loaded No. 4 charging baskets, it Rear operation includes: (1) by charging basket send into vacuum melting rapid hardening equipment vacuum charging room, open after vacuumizing vacuum charging room and Vacuum valve between vacuum melting room;(2) by the cooperation of lifting device, 4 station turnplates and the chassis moving back and forth by No. 1 extremely The raw material of No. 3 charging baskets adds the crucible of vacuum melting room under vacuum and heats;(3) by aforesaid method by No. 4 charging baskets Raw material also add the crucible of vacuum melting room, refine afterwards;(4) rotating roller is moved the water-cooled rotating roller arrangement of indoor Being sent to vacuum melting room, the crucible that fascinates is cast to the liquation under molten condition in the outer rim of water-cooled rotating roller by tundish Form alloy sheet;(5) alloy sheet leaving water-cooled rotating roller is fallen on the alloy sheet breaker of alloy sheet cooling chamber immediately, warp Crossing broken alloy sheet and slipping into the alloy sheet chilling roll rotating, (6) are with the rotation of alloy sheet chilling roll, alloy sheet Enter material-storage jar, after closing guide valve afterwards and closing the lid to material-storage jar, material-storage jar removal is completed operation.

Claims (11)

1. a vacuum melting rapid hardening equipment, mainly includes that vacuum charging room, vacuum melting room, rotating roller move room, alloy sheet Cooling chamber, Storage appts., cooling system, vacuum system, it is characterised in that: described cooling system is described vacuum melting speed Solidifying equipment provides the cooling water needed for cooling or cooling gas;Described vacuum system is connected with vacuum melting room, melts for vacuum Vacuum environment needed for rapid hardening equipment offer work for the refining;Described vacuum melting room is horizontal type structure, be provided with body of heater, Qianmen and Back door, switching mechanism is connected with the back door of vacuum melting room;Described vacuum charging room is arranged on the top of vacuum melting room, Vacuum charging indoor are provided with charging basket and charging basket elevating mechanism, and vacuum charging room is connected with vacuum melting room by vacuum valve; Vacuum melting indoor are provided with vacuum melting crucible and switching mechanism, and vacuum melting crucible is arranged on switching mechanism, and vacuum melts The flip angle of refining crucible is more than 90 degree;The rotating roller room of movement is connected with vacuum melting room by vacuum separation valve door, rotating roller Mobile indoor are provided with water-cooled rotating roller arrangement, and water-cooled rotating roller arrangement can move to vacuum melting room;Alloy sheet cooling chamber Being arranged on the lower section of vacuum melting room, alloy sheet cooling chamber is connected with vacuum melting room, is provided with brokenly in alloy sheet cooling chamber Crushing device and chilling roll;Storage appts. is arranged on the lower section of alloy sheet cooling chamber, is provided with material-storage jar, bin stock in Storage appts. Device is connected with alloy sheet cooling chamber by guide valve.
2. vacuum melting rapid hardening equipment according to claim 1, it is characterised in that: described vacuum charging indoor also set up There is rotating station dial.
3. vacuum melting rapid hardening equipment according to claim 1, it is characterised in that: described vacuum charging indoor also set up Having rotating disk, rotating disk is arranged on chassis, and the guide rail of chassis is connected with the door of vacuum charging room.
4. vacuum melting rapid hardening equipment according to claim 1, it is characterised in that: described back door by door opener with The body of heater of vacuum melting room is connected, and door opener is provided with for back door around the hydraulic cylinder of door opener axis of rotation;Institute The back door stated has 2, alternation switch.
5. vacuum melting rapid hardening equipment according to claim 1, it is characterised in that: described back door by door opener with The body of heater of vacuum melting room is connected, and door opener is provided with the hydraulic cylinder movable for back door and back door around the dress that opens the door Put the hydraulic cylinder of axis of rotation;Described back door has 2, alternation switch.
6. vacuum melting rapid hardening equipment according to claim 1, it is characterised in that: water-cooled rotating roller arrangement includes centre Bag, water-cooled rotating roller, bearing, bearing block, device for sealing magnetic fluid, rotating roller connecting gear;Tundish is connected with bearing block, axle Bearing is supported on rotating roller connecting gear;There is axle at the two ends of water-cooled rotating roller, by the bearings in bearing block at bearing On seat;Bearing block is connected with device for sealing magnetic fluid, and the cooling water in water-cooled rotating roller draws from the device for sealing magnetic fluid of one end Enter, draw from the device for sealing magnetic fluid of the other end;The lower section of rotating roller connecting gear is provided with moving guide rail, water-cooled rotating roller Device moves along guide rail and moves in rotating roller and move between room and vacuum melting room and pause;Set below water-cooled rotating roller arrangement The door that the moving guide rail put moves room with rotating roller is connected, and the door moving room with rotating roller moves.
7. vacuum melting rapid hardening equipment according to claim 1, it is characterised in that: water-cooled rotating roller arrangement includes centre Bag, water-cooled rotating roller, be connected with cooling water in water-cooled rotating roller;Water-cooled rotating roller arrangement also includes little water-cooled rotating roller, little water-cooled The diameter of rotating roller is less than the diameter of water-cooled rotating roller;The axle of little water-cooled rotating roller is parallel with the axle of water-cooled rotating roller and is positioned at water The top of the axle of cold rotating roller;The axle of little water-cooled rotating roller and tundish lay respectively at the both sides of the axle of water-cooled rotating roller;Little water Cold rotating roller is connected with cooling water.
8. vacuum melting rapid hardening equipment according to claim 1, it is characterised in that: described water-cooled rotating roller arrangement comprises Tundish, water-cooled rotating roller, bearing block, device for sealing magnetic fluid, rotating roller connecting gear;The diameter of described water-cooled rotating roller In the range of 590mm to 1220mm, the linear velocity of water-cooled rotating roller outer rim is in the range of 0.8m/s to 60m/s.
9. vacuum melting rapid hardening equipment according to claim 1, it is characterised in that: described alloy sheet cooling chamber also includes Cooling chamber cylinder, drive end bearing bracket, rear end cap;It is provided with charging aperture and discharging opening, charging aperture and vacuum melting room on cooling chamber cylinder Being connected, discharging opening is connected with guide valve, and charging aperture is rectangle, and charging aperture is provided with breaker;Breaker comprises phase To the rotating shaft rotating;Chilling roll is Double water-cooled wall construction, interior logical cooling water, and chilling roll inwall is provided with fin, cold But cylinder rotates forward or reversely rotates;There is axle the rear end of chilling roll, and axle passes through rear end cap, sets between axle and rear end cap It is equipped with device for sealing magnetic fluid and cooling water introduces and ejector.
10. vacuum melting rapid hardening equipment according to claim 1, it is characterised in that: it is provided with spiral shell on chilling roll inwall The fin of rotation shape, is additionally provided with cylinder in the inside of chilling roll, the inwall of cylinder is also equipped with helical form fin;Cylinder The helical form fin arranging on inwall is contrary with the hand of spiral of the helical form fin on chilling roll inwall.
11. vacuum melting rapid hardening equipment according to claim 1, it is characterised in that: described vacuum charging indoor also set Being equipped with 4 station turnplates, charging basket is placed on 4 station turnplates, and 4 station turnplates are arranged on chassis, and the guide rail of chassis and vacuum add The door of material room is connected, and 4 station turnplates move together with the door of vacuum charging room.
CN201620347917.3U 2016-04-25 2016-04-25 Vacuum melting rapid hardening equipment Active CN205614027U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201620347917.3U CN205614027U (en) 2016-04-25 2016-04-25 Vacuum melting rapid hardening equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201620347917.3U CN205614027U (en) 2016-04-25 2016-04-25 Vacuum melting rapid hardening equipment

Publications (1)

Publication Number Publication Date
CN205614027U true CN205614027U (en) 2016-10-05

Family

ID=57028085

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201620347917.3U Active CN205614027U (en) 2016-04-25 2016-04-25 Vacuum melting rapid hardening equipment

Country Status (1)

Country Link
CN (1) CN205614027U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108436094A (en) * 2018-06-15 2018-08-24 杭州汉苹科技有限公司 A kind of neodymium iron boron fast quenching powder for preparing continuously sprays quick quenching furnace with large-scale three chamber pressure differentials
CN109848397A (en) * 2019-04-18 2019-06-07 杭州圣檀服饰有限公司 A kind of magnetic head manufacturing device

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108436094A (en) * 2018-06-15 2018-08-24 杭州汉苹科技有限公司 A kind of neodymium iron boron fast quenching powder for preparing continuously sprays quick quenching furnace with large-scale three chamber pressure differentials
CN109848397A (en) * 2019-04-18 2019-06-07 杭州圣檀服饰有限公司 A kind of magnetic head manufacturing device

Similar Documents

Publication Publication Date Title
CN107262687B (en) A kind of manufacturing method of vacuum melting rapid hardening equipment and rapid hardening alloy
US10658094B2 (en) NdFeB magnet containing cerium and manufacturing method thereof
US10468167B2 (en) High-performance NdFeB permanent magnet produced with NdFeB scraps and production method thereof
US9892832B2 (en) Low-cost double-main-phase Ce permanent magnet alloy and its preparation method
US9620269B2 (en) Method and equipment for processing NdFeB rare earth permanent magnetic alloy with hydrogen pulverization
JP4840544B2 (en) Method and apparatus for recovering hydrogen pulverized powder of raw material alloy for rare earth magnet
US10563276B2 (en) High-performance NdFeB permanent magnet comprising nitride phase and production method thereof
EP2671958A1 (en) Method for producing r-t-b system sintered magnet
CN108759471B (en) Continuous vacuum induction melting slab furnace, alloy casting piece manufacturing method and alloy casting piece
CN108580819B (en) Vacuum induction melting cast sheet furnace, alloy cast sheet manufacturing method and alloy cast sheet
CN103990805A (en) Powder manufacturing method and equipment of neodymium iron boron rare earth permanent magnetic alloy
CN104599801A (en) Rare earth permanent magnetic material and preparation method thereof
CN107262688B (en) A kind of vacuum melting rapid hardening equipment and rapid hardening alloy manufacturing methods with secondary cooling
CN104575901A (en) Neodymium iron boron magnet added with terbium powder and preparation method thereof
CN205718441U (en) A kind of vacuum melting rapid hardening equipment with cooling twice
CN111009368A (en) Neodymium-iron-boron magnetic material and preparation method thereof
CN104575902A (en) Neodymium iron boron magnet added with cerium and preparation method thereof
CN103000324B (en) A kind of sintered rare-earth permanent magnetic material and preparation method thereof
CN205614027U (en) Vacuum melting rapid hardening equipment
CN102568729B (en) Method for preparing bulk composite nanocrystalline rare earth permanent magnetic material
CN109604615A (en) The method that low cost prepares sintered Nd-Fe-B permanent magnet
Yang et al. Combination strategy for high-performance Sm (CoFeCuZr) z sintered permanent magnet: Synergistic improvement of the preparation process
JP2003013116A (en) Method for manufacturing rare-earths-based alloy with ultralow oxygen content and fine and homogeneous crystalline structure, by reduction of rare-earth oxide
US20130049908A1 (en) Component and manufacring process of rare earth permanent magnet material
CN1062232A (en) Produce the method for rare-earth iron-boron permanent magnetic material with the rare-earth iron-boron waste material

Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant