CN205575987U - A ally oneself with and use device for preparing acrylic emulsion - Google Patents

A ally oneself with and use device for preparing acrylic emulsion Download PDF

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Publication number
CN205575987U
CN205575987U CN201620345319.2U CN201620345319U CN205575987U CN 205575987 U CN205575987 U CN 205575987U CN 201620345319 U CN201620345319 U CN 201620345319U CN 205575987 U CN205575987 U CN 205575987U
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CN
China
Prior art keywords
acrylic emulsion
cloth
blade
bed
preparing acrylic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201620345319.2U
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Chinese (zh)
Inventor
李斌
赵国芳
李明杰
毛雄伟
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhejiang Kelisen Chemical Co., Ltd.
Original Assignee
ZHEJIANG XINLI CHEMICALS CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ZHEJIANG XINLI CHEMICALS CO Ltd filed Critical ZHEJIANG XINLI CHEMICALS CO Ltd
Priority to CN201620345319.2U priority Critical patent/CN205575987U/en
Application granted granted Critical
Publication of CN205575987U publication Critical patent/CN205575987U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses an ally oneself with and use device for preparing acrylic emulsion, the unit for the antithetical couplet of at least two sets of parallelly connected settings is included, the emulsifying kettle and the reation kettle that set up with the unit should be allied oneself with including mutual series connection, be linked together through first connecting pipe between emulsifying kettle and the reation kettle, first connecting pipe all is equipped with the governing valve with emulsifying kettle and reation kettle's intercommunication department, communicates both through the second connecting pipe between per two adjacent first connecting pipes, and the intercommunication department of second connecting pipe and two first connecting pipes all is equipped with the governing valve. The utility model discloses but according to actual need is applied to different galactic productions preparations, both can be used for ordinary acrylic emulsion's production preparation, also can be used for special acrylic emulsion's production preparation, and convenient operation has not only saved equipment fixing's occupation space, moreover greatly reduced the equipment cost of mill, greatly improved work efficiency and production productivity.

Description

A kind of combined apparatus for preparing acrylic emulsion
Technical field
This utility model belongs to chemical production technical field, is specifically related to a kind of for preparing acrylic emulsion Combined apparatus.
Background technology
Acrylic emulsion is widely used in the neck such as coating, adhesive with performance and the cheap price of its excellence Territory, replaces organic solvent with water, the pollution both having prevented solvent volatilization to cause, and turn avoid and uses costliness Organic solvent, has saved the energy, reduces cost, but the application of Aqueous Adhesives is the most extremely limited at present, Main cause be the adhesive force of Aqueous Adhesives, adhesive strength and drying time etc. all not as good as solvent type adhesive, Therefore produce a kind of new, efficient, emulsion-type adhesive of quality better to be more particularly important.At propylene Acid emulsion polymerization process can produce a large amount of foam, and the technique of emulsion is produced and will bring pole by substantial amounts of foam Big harm, such as, reduce production capacity, affect product quality and affect being normally carried out of production.Mesh Froth breaking mode in front commercial production mainly has chemical froth breaking method and two kinds of debubbling methods of mechanical defoaming method.Wherein Although chemistry defoamer efficiency is the highest, but chemistry defoamer holds in acrylic emulsion polymerization high-temperature reaction process Easily affect product quality, so chemistry defoamer can not be used;And mechanical defoaming method is green non-poisonous with it and not Affect product quality and be conducive to the advantages such as production, but be currently used for the mechanical defoaming device of acrylic emulsion Defoaming effect is poor, it is impossible to well play froth breaking effect.
In the production of existing acrylic emulsion, generally constituted polymerization by a reactor and an emulsifying kettle etc. Device, and time prepared by some special acrylic emulsion, need a reactor and two pre-emulsification stills etc. to be polymerized Device, thus be accordingly used in and prepare the polyplant of ordinary emulsion and can only carry out the production of common product emulsion, no Applicable special process goes to synthesize special acrylic emulsion or core-shell emulsion polymerization technique, therefore when producing special type When acrylic emulsion and ordinary emulsion, need to be respectively provided with two set polyplants, so substantially increase factory Production cost, occupy more installation space and produce space.
Utility model content
In order to solve the problems referred to above, this utility model provides a kind of combination dress for preparing acrylic emulsion Put, prepared by the production that both may be used for conventional acrylic emulsion, it is also possible to for the life of special acrylic emulsion Produce preparation.
The technical solution of the utility model is: a kind of combined apparatus for preparing acrylic emulsion, including to Few two groups of combination unit being arranged in parallel, this combination unit includes emulsifying kettle and the reactor being serially connected setting, Be connected by the first connecting tube between described emulsifying kettle and reactor, described first connecting tube and emulsifying kettle with And the connectivity part of reactor is equipped with regulation valve, by the second connection between the first connecting tube that each two is adjacent Both are connected by pipe, and the second connecting tube is equipped with regulation valve with the connectivity part of two the first connecting tubes;Described breast Changing and be respectively equipped with the first agitator and the second agitator on still and reactor, described second agitator includes turning Moving axis, the driving means driving rotary shaft rotation and at least one blade being fixedly connected with the rotating shaft, institute State blade and include paddle shaft and in plane blade, described blade by bed of cloth and with the limit of bed of cloth Along the de-bubble frame composition matched, one end of described paddle shaft is fixedly connected with the rotating shaft, the other end and de-bubble Frame is fixing to be connected.
This utility model will arrange many group combination unit, and ordinary circumstance, so that this utility model is the most permissible Prepared by the production for conventional acrylic emulsion, it is also possible to prepared by the production of special acrylic emulsion, Er Qiejie Saved that equipment installs takes up room, reduces equipment cost, improves production production capacity, as preferably, and institute Stating combination unit is 2 groups.
When this utility model prepares special acrylic emulsion, if having only to produce ordinary emulsion, only need to select One of which combination unit carries out the production of ordinary emulsion.If desired during two emulsifying kettles, arbitrary selection Two groups of combination unit, generally, in order to reduce conveying energy consumption, two groups of combination lists that general selection is adjacent Unit, is first shut off two emulsifying kettles and the regulation valve of the first connecting tube connectivity part, by raw material respectively in the two Emulsifying kettle internal emulsification, after emulsifying completes, opens two emulsifying kettles and the regulation valve of the first connecting tube connectivity part, Close the regulation valve between a reactor and the first connecting tube connectivity part in the two combination unit, and beat Drive the regulation valve of the second connecting tube and two the first connecting tube connectivity parts so that the liquid in two emulsifying kettles is equal Enter in one of them reactor, then in acrylic emulsion polymerization process, start driving means, this reality Can be motor by novel middle driving means, driving means will drive rotary shaft to rotate, due to blade and rotation Axle is fixing to be connected, and drives blade to rotate, the blade of blade in this utility model while therefore rotary shaft rotates Being made up of bed of cloth and the de-bubble frame that matches with the edge of bed of cloth, due to bed of cloth, to contain several micro- Little pore, in whipping process, when the surface of foam and bed of cloth collides, foam is through bed of cloth Time, resolved into the foam after several fine particles, and decomposition from bed of cloth by the small pore of bed of cloth One side wear to another side, thus play froth breaking effect, finally via the stirring of paddle cycles, steep the most at last Foam is all eliminated.
This utility model in addition to can producing the acrylic emulsion of common process simultaneously, when by two emulsifying kettles When being used for producing core-shell emulsion with a reactor, after the core pre-emulsion of core-shell emulsion drips, vertical Horse cleans one of them emulsifying kettle, the acrylic acid that emulsifying is produced in this emulsifying kettle the most again by common process The pre-emulsion of emulsion, therefore when producing core-shell emulsion, it is also possible to produce propylene prepared by common process simultaneously Yogurt liquid.
For the ease of conveying and the reduction conveying energy consumption of material, as preferably, in described combination unit, Described emulsifying kettle is arranged in the top of reactor.
The polymerization process of acrylic emulsion belongs to hot environment, in order to play effective froth breaking effect, as excellent Choosing, described bed of cloth is the fiber cloth bed of material.Fiber cloth is the composite made with carbon fiber, and it has pole High intensity, and ultralight, high temperature high voltage resistant, the polymerization of acrylic emulsion belongs to the condition of high temperature, and fiber cloth has There is the effect of high temperature high voltage resistant, therefore can play good froth breaking effect, and service life is longer.
As preferably, the surface of described bed of cloth is perpendicular with the rotation direction of rotary shaft.Table when bed of cloth When face is perpendicular with the rotation direction of the rotary shaft of rotary shaft, bed of cloth is i.e. made to keep vertical with liquid, In rotation process, so that the contact area of bed of cloth and liquid is maximum, and and collision between foam Power is maximum, can be greatly improved defoaming effectiveness.
In this utility model, the arrangement of blade has multiple, in order to improve defoaming effectiveness, as preferably, and institute It is multiple for stating blade, and multiple blades are evenly arranged along the circumference of rotary shaft.
As preferably, described blade is multiple, multiple blade being axially evenly arranged along rotary shaft.
As preferably, described blade is 3~8.
As preferably, described de-bubble frame and paddle shaft are metal material and make.
The shape of this utility model Leaf can have multiple, and as preferably, being shaped as of described blade is rectangular Shape, square or circular.
Compared with prior art, the beneficial effects of the utility model are embodied in:
This utility model according to actual needs, can be applied to the production of different emulsion to be prepared, and both may be used for general Prepared by the production of logical acrylic emulsion, it is also possible to prepared by the production for special acrylic emulsion, not only operate Convenient, what the equipment that saves was installed takes up room, and greatly reduces the equipment cost, greatly of factory Improve work efficiency and produce production capacity.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
Fig. 2 is the structural representation of the second agitator in this utility model.
Detailed description of the invention
As it is shown in figure 1, this utility model includes the combination unit 2 that at least two groups are arranged in parallel, this combination unit 2 include emulsifying kettle 21 and the reactor 22 being serially connected setting, pass through between emulsifying kettle 21 and reactor 22 First connecting tube 23 is connected, and the first connecting tube 23 is equal with the connectivity part of emulsifying kettle 21 and reactor 22 It is provided with regulation valve 24, by the second connecting tube 25, both is connected between the first connecting tube 23 that each two is adjacent Logical, the connectivity part of the second connecting tube 25 and two the first connecting tubes 23 is equipped with regulation valve 24.This practicality is new Type is respectively equipped with the first agitator and the second agitator on emulsifying kettle 21 and reactor 22,
As in figure 2 it is shown, this utility model the second agitator includes rotary shaft 1, drives driving of rotary shaft 1 rotation Dynamic device (being not drawn in figure) and at least one blade 3 of being connected fixing with rotary shaft 1, this utility model Middle driving means can be motor.In this utility model, blade 3 includes paddle shaft 31 and in plane leaf Sheet 32, the de-bubble frame 322 that the blade 32 edge by bed of cloth 321 and with bed of cloth 321 matches forms, One end of paddle shaft 31 is fixing with rotary shaft 1 to be connected, and the other end is fixing with de-bubble frame 322 to be connected.De-bubble frame 322 and paddle shaft 31 be metal material and make.
In this utility model, the arrangement of blade has multiple, in order to improve defoaming effectiveness, in this utility model Blade 3 is multiple, and multiple blades 3 are evenly arranged along the circumference of rotary shaft, are in can removing liquid The foam of different depth, certain blade 3 can also be permissible along being axially evenly arranged along rotary shaft 1 Quickly removing and be positioned at the foam in the same degree of depth, generally, blade 3 is 3~8.
The shape of this utility model Leaf 32 can have multiple, blade 32 be shaped as rectangle, pros Shape or circle.The froth breaking effect of different shapes differs, ordinary circumstance, and this utility model blade 32 is for long Square.
Principle of the present utility model is:
This utility model will arrange many group combination unit, and ordinary circumstance, so that this utility model is the most permissible Prepared by the production for conventional acrylic emulsion, it is also possible to prepared by the production of special acrylic emulsion, and drop Low equipment cost, generally, being combined unit 2 in this utility model is 2~4 groups.
When this utility model prepares special acrylic emulsion, if having only to produce ordinary emulsion, only need to select One of which combination unit 2 carries out the production of ordinary emulsion.If desired during two emulsifying kettles 21, arbitrary Select two groups of combination unit 2, generally, in order to reduce conveying energy consumption, two groups of connection that general selection is adjacent With unit 2, it is first shut off two emulsifying kettles 21 and the regulation valve 24 of the first connecting tube 23 connectivity part, by former Material, respectively at the two emulsifying kettle 21 internal emulsification, after emulsifying completes, opens two emulsifying kettles 21 and first The regulation valve 24 of connecting tube 23 connectivity part, cuts out the reactor 22 and the in the two combination unit 2 Regulation valve 24 between one connecting tube 23 connectivity part, and open the second connecting tube 25 and two the first connecting tubes The regulation valve 24 of 23 connectivity parts so that the liquid in two emulsifying kettles 21 all enters one of them reactor 22 In, then in acrylic emulsion polymerization process, start driving means.
Driving rotary shaft 1 is rotated by driving means, is connected owing to blade 3 is fixing with rotary shaft 1, therefore turns Moving axis 1 drives blade 3 to rotate while rotating, and in this utility model, the blade 32 of blade 3 is by bed of cloth 321 And the de-bubble frame 322 matched with the edge of bed of cloth 321 forms, owing to bed of cloth 321 is containing some Individual small pore, therefore in whipping process, when the surface of foam and bed of cloth 321 collides, foam When through bed of cloth 321, resolved into several fine particles by the small pore of bed of cloth 321, and Foam after decomposition is worn to another side from the one side of bed of cloth 321, thus plays froth breaking effect, finally via The stirring of blade 32 circulation, foam is all eliminated the most at last.
The polymerization process of acrylic emulsion belongs to hot environment, in order to play effective froth breaking effect, this practicality Novel middle bed of cloth 321 is the fiber cloth bed of material.Fiber cloth is the composite made with carbon fiber, and it has High intensity, and ultralight, high temperature high voltage resistant, the polymerization of acrylic emulsion belongs to the condition of high temperature, fiber cloth There is the effect of high temperature high voltage resistant, therefore can play good froth breaking effect, and service life is longer.
In this utility model, bed of cloth 321 can have multiple arrangement, such as, keep certain angle with liquid level Degree, this utility model one of which embodiment, as it is shown in figure 1, bed of cloth 321 in this utility model Surface is perpendicular with the rotation direction of rotary shaft 1.Surface and the rotation side of rotary shaft 1 when bed of cloth 321 When vertical, bed of cloth 321 is i.e. made to keep vertical with liquid, in rotation process, so that cloth Layer 321 is maximum with the contact area of liquid, and and impact force between foam maximum, can be greatly improved Defoaming effectiveness.

Claims (7)

1. the combined apparatus being used for preparing acrylic emulsion, it is characterised in that include that at least two groups are in parallel The combination unit arranged, this combination unit includes emulsifying kettle and the reactor being serially connected setting, described emulsifying It is connected by the first connecting tube between still and reactor, described first connecting tube and emulsifying kettle and reactor Connectivity part be equipped with regulation valve, between the first connecting tube that each two is adjacent by second connecting tube will both Connection, the second connecting tube is equipped with regulation valve with the connectivity part of two the first connecting tubes;Described emulsifying kettle is with anti- Answering and be respectively equipped with the first agitator and the second agitator on still, described second agitator includes rotary shaft, drives The driving means of dynamic rotary shaft rotation and at least one blade being fixedly connected with the rotating shaft, described blade bag Including paddle shaft and in plane blade, described blade matches by bed of cloth and with the edge of bed of cloth De-bubble frame composition, one end of described paddle shaft is fixedly connected with the rotating shaft, and the other end and de-bubble frame are fixing even Connect.
2. the combined apparatus for preparing acrylic emulsion as claimed in claim 1, it is characterised in that In described combination unit, described emulsifying kettle is arranged in the top of reactor.
3. the combined apparatus for preparing acrylic emulsion as claimed in claim 1, it is characterised in that institute Stating bed of cloth is the fiber cloth bed of material.
4. the combined apparatus for preparing acrylic emulsion as claimed in claim 1, it is characterised in that institute The surface stating bed of cloth is perpendicular with the rotation direction of rotary shaft.
5. the combined apparatus for preparing acrylic emulsion as claimed in claim 1, it is characterised in that institute It is multiple for stating blade, and multiple blades are evenly arranged along the circumference of rotary shaft.
6. the combined apparatus for preparing acrylic emulsion as claimed in claim 1, it is characterised in that institute State de-bubble frame and paddle shaft is metal material and makes.
7. the combined apparatus for preparing acrylic emulsion as claimed in claim 1, it is characterised in that institute That states blade is shaped as rectangle.
CN201620345319.2U 2016-04-22 2016-04-22 A ally oneself with and use device for preparing acrylic emulsion Expired - Fee Related CN205575987U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201620345319.2U CN205575987U (en) 2016-04-22 2016-04-22 A ally oneself with and use device for preparing acrylic emulsion

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201620345319.2U CN205575987U (en) 2016-04-22 2016-04-22 A ally oneself with and use device for preparing acrylic emulsion

Publications (1)

Publication Number Publication Date
CN205575987U true CN205575987U (en) 2016-09-14

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Country Status (1)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109679038A (en) * 2019-01-04 2019-04-26 北京华腾东光科技发展有限公司 Emulsion polymerisation system, emulsion polymerisation process and application
CN111718440A (en) * 2020-08-01 2020-09-29 浙江亦龙新材料有限公司 Production process of acrylate emulsion

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109679038A (en) * 2019-01-04 2019-04-26 北京华腾东光科技发展有限公司 Emulsion polymerisation system, emulsion polymerisation process and application
CN111718440A (en) * 2020-08-01 2020-09-29 浙江亦龙新材料有限公司 Production process of acrylate emulsion
CN111718440B (en) * 2020-08-01 2022-06-07 浙江亦龙新材料有限公司 Production process of acrylate emulsion

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Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
TR01 Transfer of patent right

Effective date of registration: 20180525

Address after: 312000 No. 12 weft seven road, Shangyu economic and Technological Development Zone, Hangzhou Bay, Shaoxing, Zhejiang

Patentee after: Zhejiang Kelisen Chemical Co., Ltd.

Address before: 312352 Zhu Kezhen science and Technology Park, Dongguan Street, Shangyu District, Shaoxing, Zhejiang

Patentee before: Zhejiang Xinli Chemicals Co., Ltd.

TR01 Transfer of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20160914

Termination date: 20210422

CF01 Termination of patent right due to non-payment of annual fee