CN205570220U - A vibration bottle that is used for adsorption material capability test of oil shale ash preparation - Google Patents
A vibration bottle that is used for adsorption material capability test of oil shale ash preparation Download PDFInfo
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- CN205570220U CN205570220U CN201620317208.0U CN201620317208U CN205570220U CN 205570220 U CN205570220 U CN 205570220U CN 201620317208 U CN201620317208 U CN 201620317208U CN 205570220 U CN205570220 U CN 205570220U
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- bottle
- lobe
- shaker flask
- shale ash
- performance test
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Abstract
The utility model particularly relates to a vibration bottle that is used for adsorption material capability test of oil shale ash preparation. The vibration bottle end is equipped with the bellying, and including bellying upper portion, this part is the protruding sphere that makes progress, bellying side evenly distributed concave surface, the inside cavity that is of bellying, the bottle end bellying outside is equipped with the passageway and communicates with each other with the outside. In the oscillatory process, adsorbent and solution all can have level and vertical two kinds of motions, improve the degree of consistency of solution, and action of gravity upwards " having flown " can be overcome along " the track " of concave surface to the adsorbent in the oscillatory process in addition, effectively avoids the adsorbent to precipitate and reunites to can the whole vibration bottle that adsorbs the temperature of fast speed adjusting.
Description
Technical field
This utility model belongs to chemical industry instrument field, is specifically related to a kind of adsorbing material performance prepared for kerosene shale ash
The shaker flask of test.
Background technology
Application kerosene shale ash industrial waste produces industrial wastewater adsorbent, both can realize innoxious, the resource of industrial waste
Change processes, and can reduce again the production cost of adsorbent, it is achieved social environment benefit and the doulbe-sides' victory of economic benefit, therefore this research is right
In the energy and environmental protection aspect, there is important researching value and wide application prospect.In this research field, have been disclosed for
Kerosene shale ash is that raw material preparation has the method (notification number: CN103349960B) of intercalation configuration uranium adsorbing material and with white clay
Be that raw material prepares brucite and hydrated calcium silicate with kerosene shale ash, respectively as uranium adsorbent and firming agent method (notification number:
CN103752261A).But discovery can there is problems in that in actual applications
1. current, agitator uses horizontal whirling vibration mode substantially, and this mode of vibration causes solution in oscillatory process
Do and do horizontal circular movement around center.In actual application, prepare brucite or aquation silicon with kerosene shale ash for raw material
Acid calcium, due to self gravitation effect, is mainly deposited on solution bottom, does horizontal circular movement owing to solution does around center, cause
It is concentrated mainly on shaker flask bottom centre, it is difficult to realize fully dispersed affecting adsorption effect.More seriously brucite or water
Changing calcium silicates and be susceptible to agglomeration in bottle body bottom gathering, impact is for the evaluation of material absorption property further.Due to
Lacking the power of lengthwise movement, in solution, the concentration of different aspects there are differences, and adsorbent is concentrated mainly on bottom, absorption
Occurring mainly in lower floor, although by diffusion, the uranium ion on top can be diffused into bottom and participate in adsorption reaction, but can cause
Adsorption time extends, and causes adsorption dynamics adsorption kinetics error in data bigger.
2. the method that absorption property test at present is used is to be positioned over bottom agitator by shaker flask, with spring by bottle
Fix in an oscillator, agitator will be filled water, by keeping water temperature constant, test sample at a certain temperature
Absorption property.Owing to temperature is relatively big for sample adsorption performance impact, it is extremely important for therefore controlling the actual adsorption temp of sample
's.But being flat bottom existing shaker flask, in oscillatory process, the bottom with vibrator is in close contact, shaker flask and water body
Effective contact area be only the side of shaker flask, cause the solution in shaker flask asynchronous with the water temperature in agitator.
Experimentation shows (RSC Adv., 2015,5,5904-5912): temperature is for hydrated calcium silicate adsorption capacity and attached speed
Fast impact is obvious, these be desirable that adsorption process should the temperature of fast and stable solution as far as possible, reduce experimental error.
Summary of the invention
The purpose of the application is to provide one can quickly avoid adsorbent to be deposited in bottle body bottom, effectively suppresses absorption
Bolus is gathered, and solution is fully contacted with adsorbent, and can quickly adjust the adsorbing material prepared for kerosene shale ash of adsorption temp
The shaker flask of performance test.
The purpose of this utility model is achieved in that
For the shaker flask of adsorbing material performance test prepared by kerosene shale ash, including bottle and bottle cap, bottle is by body
Form with at the bottom of bottle, at the bottom of bottle, be provided with lobe.
The vertical section of described lobe is circular or parabola shaped, and horizontal cross-section is circular.
Described lobe includes spherical structure lobe top 1-1 and the lobe side raised up.
Described lobe side is evenly distributed with concave surface.
Described lobe side is sphere, and lobe side is tangent with lobe top sphere, the ball of lobe side
Face centre of sphere O is on body.
Two circular vent pipes, two breather being projected as at bottle body bottom are connected at the top on described lobe top
By the straight line of bottom centre, the angle of every pipeline and horizontal plane is 3-5 degree.
The beneficial effects of the utility model are:
Lobe of the present utility model be arranged on oscillatory process, first for solution provide be raised above put forth effort domatic,
The energy that shaker flask horizontal movement produces can be converted into the power of solution lengthwise movement by solution, it is to avoid adsorbent concentrates on the end
During portion, there is difference in solution aspect concentration, causes adsorption efficiency to decline.Secondly lobe effectively expands a bottle floor space, makes vibration
Bottle increases with effective contact area of water body, it is ensured that in shaker flask, residing for solution, temperature environment is more stable.Again, carry for adsorbent
Having supplied the passage moved upward, adsorbent can overcome action of gravity upwards " to fly along " track " of concave surface in oscillatory process
Rise ", it is prevented effectively from adsorbent precipitation and reunites, it is ensured that in oscillatory process, adsorbent and solution all can have level and longitudinal direction
Two kinds of motions, are conducive to more fully measuring the absorbability of adsorbing material.
Accompanying drawing explanation
Fig. 1 is this utility model overall structure figure.
Fig. 2 is this utility model lobe height and eddy velocity curve chart.
Fig. 3 is this utility model embodiment 1 bottom view.
Fig. 4 is this utility model embodiment 4 sectional drawing.
Fig. 5 is this utility model embodiment 4 bottom view.
Fig. 6 is this utility model embodiment 7 sectional drawing.
Fig. 7 is passage 2 vertical section figure.
Fig. 8 is embodiment 9 shaker flask bottom view.
Fig. 9 is that embodiment 9 is along boost line AA shaker flask longitudinal direction sectional drawing in Fig. 8.
Figure 10 is the profile of embodiment 11 conduit 5.
Figure 11 is embodiment 12 shaker flask sectional drawing.
Figure 12 is embodiment 15 shaker flask bottom view.
Detailed description of the invention
Below in conjunction with the accompanying drawings this utility model is described further.
For the problem existing for existing shaker flask, this utility model provides one and can quickly avoid adsorbent to precipitate
At bottle body bottom, effectively suppression adsorbent is reunited, and solution is fully contacted with adsorbent, and can quickly adjust the vibration of adsorption temp
Bottle.As shown in figs. 4 and 5: be provided with lobe 1 at the bottom of bottle, including lobe top 1-1, this part is the sphere that raises up；Protruding
Side, portion 1 is uniformly distributed 4 concave surface 1-2, and this part is a part for spheroid inner surface, and the centre of sphere, Ping Di center, the centre of sphere are at the bottom of bottle
The plane that upright projection point three is constituted is the concave surface 1-2 plane of symmetry, and the line of centres, bottle at the bottom of the centre of sphere and bottle as shown in Figure 6
Center, the end and the centre of sphere are 3-75 degree in upright projection point line at the bottom of bottle, the included angle A of two straight lines；Bottom surface and the friendship of perpendicular radii OD
Point for 100-1, is provided with lobe 1 wall thickness and bottle side wall consistency of thickness for E, OE and ED length ratio at the bottom of bottle, inside is cavity；As
Being provided with 4 passages 2 outside lobe 1 at the bottom of shown bottle of accompanying drawing 7, lobe 1 is communicated with outside by passage 2；Bottle top is bottle
Lid 3, is connected with bottle by ground.
Top 1-1, this part is the sphere that raises up, it is ensured that the adsorbent risen in oscillatory process falls after rise downwards and will not stop
Stay on 1-1, and then cause reuniting.Lobe side is uniformly distributed 4 concave surface 1-2, and this part is of spheroid inner surface
Point, concave surface 1-2 is symmetrical in the centre of sphere, Ping Di center, the centre of sphere in three planes constituted of upright projection point at the bottom of bottle.This design is protected
Having demonstrate,proved in oscillatory process, adsorbent and solution all can have level and longitudinally two kinds of motions, improve the uniformity of solution, and
Adsorbent can overcome action of gravity upwards " to fly up " along " track " of 1-2 in oscillatory process, is prevented effectively from adsorbent and sinks
Form sediment and reunite.The bottle end, is provided with lobe 1 wall thickness and bottle side wall consistency of thickness, and lobe is internal is cavity.This design ensure that
Bottom can enter water body, increases the contact area of water body and solution, is conducive to actual temperature control.It is provided with 4 outside bottle end lobe 1
Individual passage 2, lobe 1 is communicated with outside by passage 2.Which ensure that, when bottle lies against bottom agitator, liquid is permissible
Enter in lobe 1.At the bottom of the centre of sphere and bottle, the line of centres, Ping Di center and the centre of sphere are at upright projection point line at the bottom of bottle, two straight lines
Included angle A be 3-75 degree；The intersection point of bottom surface and the perpendicular radii OD ratio that is E, OE and ED length is for 100-1, and this design can root
Adjust the curved surface gradient of 1-2 according to practical situation, meet the vibration requirement of different adsorbents.Bottle top is bottle cap 3, by mill
Mouth is connected with bottle, prevents solution and adsorbent in due course from spilling.
Provide the most emphatically this utility model embodiment
Embodiment 1
As it is shown in figure 1, the shaker flask of the adsorbing material performance test prepared for kerosene shale ash, including bottle and bottle cap 3,
Bottle is formed by the bottom of body and bottle, is provided with lobe 1 at the bottom of bottle.Bottle top is bottle cap 3, is connected with bottle by ground.Described
The vertical section of lobe be circular or parabola shaped, the horizontal cross-section of lobe is circular.
The setting of this utility model lobe can oscillatory process for solution provide be raised above put forth effort domatic, it is possible to
The energy that shaker flask horizontal movement produces is converted into the power of solution lengthwise movement, reduces solution aspect concentration difference, it is to avoid
Adsorbent concentrates on bottom centre's problem.
Embodiment 2
Same as in Example 1, be only difference is: by series of experiments, inventor find as lobe height h and
When bottle height H meets following relation, the power of solution lengthwise movement is the strongest:
H=-1.67h2+26.67h-76.6
10cm≥h≥3cm。
Under this condition, relation between shaker flask eddy velocity and height as in figure 2 it is shown, wherein abscissa be lobe
Highly h, unit cm, vertical coordinate is eddy velocity, unit m/s, and when h is 8cm, this utility model eddy velocity is 10m/s.?
During carrying out enlarged experiment, h=8cm, there is the most excellent oscillation effect.
Embodiment 3
Although the lobe that embodiment 1 provides solves adsorbent and concentrates on the problem of bottom, but is found through experiments:
If the too high meeting of lobe causes the adsorbent of bottom in oscillatory process can not more effectively incorporate eddy current, but still deposits
In at the bottom of bottle, lobe is the most rationally set, is the important technology feature reaching this utility model effect.As shown in Figure 3.Lobe
When meeting following relation between area of a circle radius R and bottle height H at the bottom of end area of a circle radius r, bottle, not only adsorbent can more have
Imitate incorporates eddy current, can form horizontal mobility near the solution at the bottom of bottle, make oscillation effect the most notable in oscillatory process.
3 >=R/r >=1.5,3 >=H/R >=1.7.
Wherein the relation of area of a circle radius r at the bottom of solution level flow velocity at the bottom of bottle and lobe is
V=-0.18r2+2.88r-6.52
8cm≥r≥2.8cm
Embodiment 4
In embodiment 1-3, mainly by the structure of bottle is improved, improve solution longitudinal direction and cross-flow velocity reaches
To the technique effect of raising shaker flask efficiency, as shown in Figure 4, shaker flask lobe includes the projection of the spherical structure raised up
Top, portion 1-1 and lobe side, be evenly distributed with concave surface 1-2 in lobe side.It is illustrated in figure 5 at the bottom of the present embodiment bottle
Bottom view.
Raise up sphere, it is ensured that the adsorbent risen in oscillatory process falls after rise downwards and will not rest on lobe top 1-
Causing on 1 reuniting, provide the passage moved upward, adsorbent and solution for adsorbent and solution can in oscillatory process simultaneously
Overcome action of gravity upwards " to fly up " with " track " along concave surface 1-2, be prevented effectively from adsorbent precipitation and reunite, it is ensured that shaking
During swinging, adsorbent and solution all can have level and longitudinally two kinds of motions, improve the uniformity of solution.
Embodiment 5
For ease of the making of shaker flask, the concave surface of lobe side is 4, and 4 concave surfaces are solution and adsorbent carries simultaneously
Having supplied bigger " sliding the preparation before domatic taking off ", oscillation effect is more preferable.
Embodiment 6
The same as in Example 4, difference is that described lobe side is sphere, lobe side and lobe upper ball
Face is tangent, and the sphere centre of sphere O of lobe side is on body, and this design makes the connection that lobe top and lobe side smooth
Together, the most at utmost ensure that fluid is minimum at the resistance being subject to through this two parts joining place.
Embodiment 7
The same as in Example 4, difference is described, the sphere centre of sphere O of lobe side and the line at Ping Di center with
The angle of horizontal plane is 3-75 degree.
Embodiment 8
As shown in figs. 4 and 5: be provided with lobe 1 at the bottom of bottle, including lobe top 1-1, this part is convex balling-up
Face；Lobe 1 side is uniformly distributed 4 concave surface 1-2, and this part is a part for spheroid inner surface, the centre of sphere, Ping Di center, ball
The heart is the concave surface 1-2 plane of symmetry in the plane that upright projection point three at the bottom of bottle is constituted, and the centre of sphere and Ping Di center as shown in Figure 6
Line, Ping Di center are 3-75 degree with the centre of sphere in upright projection point line at the bottom of bottle, the included angle A of two straight lines；Bottom surface and vertical half
The intersection point of the footpath OD ratio that is E, OE and ED length for 100-1, is provided with lobe 1 wall thickness and bottle side wall consistency of thickness at the bottom of bottle, protruding
Portion 1 is internal is cavity；Being provided with passage 2 as shown in Figure 7 outside lobe 1 at the bottom of bottle, lobe 1 is communicated with outside by passage 2；
Bottle top is bottle cap 3, is connected with bottle by ground.
Embodiment 9
The same as in Example 9, difference is to connect two circular vent pipes at the top of lobe top 1-1, and two lead to
Trachea is at the straight line by bottom centre that is projected as of bottle body bottom, and the angle of every pipeline and horizontal plane is 3-5 degree.As
Shown in Fig. 8-9.
Embodiment 10
Substantially the same manner as Example 9, difference is to connect two circular vent pipes 4 at 1-1 top, lobe top,
Article two, breather is at the straight line by bottom centre that is projected as of bottle body bottom, outside lobe top 1-1 is by 4 and bottle
Portion communicates, and the angle of every pipeline and horizontal plane is 3-5 degree.
Embodiment 9, before actual application, needs to adjust bottle angle and the gas of lobe top 1-1 is discharged,
Liquid can be made to fill up, and it is the most inconvenient to use, and the solution at 1-1 top and whole fluid exchange obstructed, this causes 1-1
The temperature of middle liquid can there are differences with the temperature of actual liquid.By the improvement of the present embodiment, gas can be arranged by conduit
Going out, liquid can be entered in 1-1 by conduit, solves the problem that embodiment 9 exists.
Embodiment 11
Substantially the same manner as Example 9, difference is that breather 5 is by plane 5-1 and semicircle curved surface as shown in Figure 10
5-2 forms, and 2-5 times of a length of semicircle curved surface 5-2 diameter of plane 5-1, plane 5-1 is perpendicular to bottle bottom surface.
This design breather 5 is except having aerofluxus, outside the effect of exchanging liquid, owing to causing solution in agitator motion
Doing and move in a circle around bottle center, breather 5 serves between the effect of stirring paddle, beneficially solution, solution and adsorbent
Between mixing.Semicircle curved surface 5-2 prevents adsorbent from resting on its upper end, reduces resistance simultaneously.
Embodiment 12
Substantially the same manner as Example 11, difference is two breather 5 conllinear, this straight line and level as shown in figure 11
The angle in face is 3-5 degree.This conllinear designs, and contributes to liquid and flows in breather, and the vertical area stirred expands
Contribute to beneficially between solution, be sufficiently mixed further between solution and adsorbent.
Embodiment 13
Substantially the same manner as Example 11, difference is that breather 5 is positioned at the centre of sphere, Ping Di center, the centre of sphere at bottle dolly
In straight 3 planes constituted of subpoint.This design ensure that breather 5 does not stop that adsorbent rises along 1-2.
Embodiment 14
Although embodiment 3 provides the scope of oscillation effect more preferably significantly r, R/r and H/R, and solution must height
Necessarily be greater than h, r crosses conference and causes the solution and the quantity of adsorbing material that consume in experimentation excessive in actual applications, and
And the oscillation rate for agitator has higher requirement, comprehensive factors above, show to work as h=by further experiment
3cm；H=9cm；r=3cm；During R=4.5cm, this shaker flask has good oscillation effect for the solution of 100mL.
Embodiment 15
Essentially identical with embodiment 10-13, it is in place of optimization: R=4.5cm；H=9cm；As shown in figure 12, bottom is with recessed
The radius r of the circle that face 1-2 is tangent2=3cm；As shown in figures 9 and 11, the vertical peak of breather and plane perpendicular distance h2≤
4.2cm, this shaker flask has good oscillation effect for the solution of 100mL.
Claims (10)
1. a shaker flask for the adsorbing material performance test prepared for kerosene shale ash, including bottle and bottle cap, bottle is by bottle
Form at the bottom of body and bottle, it is characterised in that: it is provided with lobe (1) at the bottom of bottle.
The shaker flask of a kind of adsorbing material performance test prepared for kerosene shale ash the most according to claim 1, it is special
Levying and be: the vertical section of described lobe is parabola shaped, horizontal cross-section is circular.
The shaker flask of a kind of adsorbing material performance test prepared for kerosene shale ash the most according to claim 1, it is special
Levy and be: described lobe includes the lobe top of spherical structure and lobe side, the described projection raised up
Side, portion is evenly distributed with concave surface.
The shaker flask of a kind of adsorbing material performance test prepared for kerosene shale ash the most according to claim 3, it is special
Levy and be: lobe at the bottom of bottle (1) outside is provided with passage (2), and lobe (1) is communicated with outside by passage (2).
The shaker flask of a kind of adsorbing material performance test prepared for kerosene shale ash the most according to claim 3, it is special
Levying and be: described lobe side is sphere, the sphere center of circle O of lobe side is on body.
The shaker flask of a kind of adsorbing material performance test prepared for kerosene shale ash the most according to claim 3, it is special
Levying and be: connect two breathers at the top of described lobe top (1-1), the angle of every pipeline and horizontal plane is 3-
5 degree.
The shaker flask of a kind of adsorbing material performance test prepared for kerosene shale ash the most according to claim 3, it is special
Levy and be: connect two breathers at the top on described lobe top, two breathers bottle body bottom be projected as pass through
The straight line of bottom centre, the angle of every pipeline and horizontal plane is 3-5 degree.
8. according to the shaker flask of a kind of adsorbing material performance test prepared for kerosene shale ash described in claim 6 or 7, its
It is characterised by: described breather is round tube or the pipe being made up of plane (5-1) and semicircle curved surface (5-2).
The shaker flask of a kind of adsorbing material performance test prepared for kerosene shale ash the most according to claim 3, it is special
Levy and be: lobe (1) highly h is 3cm；Bottle height H is 9cm；Lobe (1) end area of a circle radius r is 3cm；The bottle end
Area of a circle radius R is 4.5cm.
The shaker flask of a kind of adsorbing material performance test prepared for kerosene shale ash the most according to claim 8, it is special
Levy and be: the vertical peak of breather and plane perpendicular distance h2Less than 4.2cm；Bottle height H is 9cm；Bottom and concave surface 1-2
The radius r of tangent circle2=3cm；Bottle end area of a circle radius R is 4.5cm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620317208.0U CN205570220U (en) | 2016-04-15 | 2016-04-15 | A vibration bottle that is used for adsorption material capability test of oil shale ash preparation |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620317208.0U CN205570220U (en) | 2016-04-15 | 2016-04-15 | A vibration bottle that is used for adsorption material capability test of oil shale ash preparation |
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| CN205570220U true CN205570220U (en) | 2016-09-14 |
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| CN201620317208.0U Expired - Fee Related CN205570220U (en) | 2016-04-15 | 2016-04-15 | A vibration bottle that is used for adsorption material capability test of oil shale ash preparation |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105688719A (en) * | 2016-04-15 | 2016-06-22 | 黑龙江科技大学 | Shake flask for performance test of adsorbing material prepared from oil shale ash |
-
2016
- 2016-04-15 CN CN201620317208.0U patent/CN205570220U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105688719A (en) * | 2016-04-15 | 2016-06-22 | 黑龙江科技大学 | Shake flask for performance test of adsorbing material prepared from oil shale ash |
| CN105688719B (en) * | 2016-04-15 | 2017-12-26 | 黑龙江科技大学 | A kind of shaker flask of the sorbing material performance test prepared for kerosene shale ash |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160914 Termination date: 20180415 |
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| CF01 | Termination of patent right due to non-payment of annual fee |