CN205549632U - Stills structure of medicine midbody - Google Patents

Stills structure of medicine midbody Download PDF

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Publication number
CN205549632U
CN205549632U CN201620138037.5U CN201620138037U CN205549632U CN 205549632 U CN205549632 U CN 205549632U CN 201620138037 U CN201620138037 U CN 201620138037U CN 205549632 U CN205549632 U CN 205549632U
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CN
China
Prior art keywords
steam
cauldron
kettle
outlet
submerged pump
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201620138037.5U
Other languages
Chinese (zh)
Inventor
欧阳春生
邹临
任建华
张兴利
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiangxi Euclid Chemical Co Ltd
Original Assignee
Jiangxi Euclid Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jiangxi Euclid Chemical Co Ltd filed Critical Jiangxi Euclid Chemical Co Ltd
Priority to CN201620138037.5U priority Critical patent/CN205549632U/en
Application granted granted Critical
Publication of CN205549632U publication Critical patent/CN205549632U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model provides a stills structure of medicine midbody, includes the cauldron physically, the bottom of the cauldron body is equipped with the material export, and the material exit is provided with the submerged pump, the export of submerged pump faces the material export, the external portion of cauldron is equipped with presss from both sides the cover, the bottom of clamp cover is equipped with steam inlet, and steam inlet is linked together through first pipeline and the heating furnace that is located outside the clamp cover, be provided with the electrical control valve on the first pipeline, the internal top of cauldron is equipped with temperature sensor. The beneficial effects of the utility model are that solid form thing or high boiling point material bottom the submerged pump can be personally experienced sth. Part of the body the cauldron are fast carried away from the material export, have improved distilling efficiency, temperature sensor is used for detecting the internal temperature of cauldron to give controlling means with data transfer, controlling means controls the electrical control valve from this, the inlet of adjusting steam, and reuse through the partial steam that heats flows back the heating furnace once more from steam outlet in has effectively practiced thrift the energy.

Description

A kind of distillating still structure of pharmaceutical intermediate
Technical field
This utility model relates to distillating still technical field, is specifically related to the distillating still structure of a kind of pharmaceutical intermediate.
Background technology
Chemical Manufacture is typically used for purify and distilling apparatus, distillating still is exactly conventional one, it is to utilize liquid to have different boiling points, liquid is added into the purpose that vapours reaches to separate, therefore it is required that distillating still have to have good heats, traditional distillating still is only capable of the general control carrying out temperature, the precision of distillation can be caused low and the waste of the energy, and carry out heated after vapours the most all can be expelled directly out, because itself some heat of heat, so can cause the raising of cost, the waste of the energy;In material, decorating film or high boiling material can be deposited in the bottom of kettle, and traditional discharge relies primarily on material and is deposited in the liquid level difference of autoclave body bottom and completes, and this marker method discharge is slow, inefficient;For convenience of the situation in viewing kettle, typically can be provided with glass vision panel, and the effect of heat insulation of glass vision panel is poor, the utilization rate causing heat energy is low.
Utility model content
The purpose of this utility model is to provide the distillating still structure of a kind of pharmaceutical intermediate, with the problem solving to propose in above-mentioned background technology.
For achieving the above object, the following technical scheme of this utility model offer:
The distillating still structure of a kind of pharmaceutical intermediate, including kettle, the bottom of described kettle is provided with material outlet, is provided with submerged pump at material outlet, and the outlet of described submerged pump faces material outlet;It is provided with chuck outside described kettle, the bottom of described chuck is provided with steam inlet, steam inlet is connected with the heating furnace being positioned at outside chuck by the first pipeline, it is provided with electric control valve on described first pipeline, described kettle inner top is provided with temperature sensor, described temperature sensor and electric control valve all electrically connect with control device, and described chuck top is provided with steam (vapor) outlet, and steam (vapor) outlet is connected with heating furnace by second pipe;Being provided with liquid level tube outside described kettle, the two ends of described liquid level tube were connected with the top and bottom of kettle by communicating pipe, and described liquid level tube is provided with graduation mark.
As further program of the utility model: the bottom of described chuck is additionally provided with water out.
As this utility model further scheme: described kettle top is provided with material inlet.
As this utility model further scheme: described control device is PLC.
As this utility model further scheme: the material of described liquid level tube is glass.
The beneficial effects of the utility model are that decorating film or the high boiler material of autoclave body bottom can quickly be transferred out by submerged pump from material outlet, improve the efficiency of distillation;Temperature sensor is for detecting the temperature in kettle, and transfer data to control device, control device and thus control electric control valve, the inlet of regulation steam, some vapor through heating is back in heating furnace reuse from steam (vapor) outlet again, is effectively saved the energy;Liquid level tube can quickly view the liquid level in kettle, and carries out record by graduation mark.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
In figure: 1-material inlet, 2-kettle, 3-temperature sensor, 4-steam (vapor) outlet, 5-second pipe, 6-heating furnace, 7-the first pipeline, 8-electric control valve, 9-steam inlet, 10-material outlet, 11-water out, 12-submerged pump, 13-chuck, 14-communicating pipe, 15-liquid level tube, 16-graduation mark.
Detailed description of the invention
Below in conjunction with the accompanying drawing in this utility model embodiment, the technical scheme in this utility model embodiment is clearly and completely described, it is clear that described embodiment is only a part of embodiment of this utility model rather than whole embodiments.Based on the embodiment in this utility model, those of ordinary skill in the art are not under making creative work premise
The every other embodiment obtained, broadly falls into the scope of this utility model protection.
Refer to Fig. 1, in this utility model embodiment, a kind of distillating still structure of pharmaceutical intermediate, including kettle 2, the bottom of described kettle 2 is provided with material outlet 10, is provided with submerged pump 12 at material outlet 10, and the outlet of described submerged pump 12 faces material outlet 10, decorating film bottom kettle 2 or high boiler material can quickly be transferred out by submerged pump 12 from material outlet 10, improve the efficiency of distillation;
Described kettle 2 is outside is provided with chuck 13, the bottom of described chuck 13 is provided with steam inlet 9, steam inlet 9 is connected with the heating furnace 6 being positioned at outside chuck 13 by the first pipeline 7, it is provided with electric control valve 8 on described first pipeline 7, described kettle 2 inner top is provided with temperature sensor 3, described temperature sensor 3 and electric control valve 8 all electrically connect with control device, described chuck 13 top is provided with steam (vapor) outlet 4, steam (vapor) outlet 4 is connected with heating furnace 6 by second pipe 5, temperature sensor 3 is for detecting the temperature in kettle 2, and transfer data to control device, control device and thus control electric control valve 8, the inlet of regulation steam, some vapor through heating is back in heating furnace 6 reuse from steam (vapor) outlet 4 again, it is effectively saved the energy.
Described kettle 2 is outside is provided with liquid level tube 15, the two ends of described liquid level tube 15 are connected by the top and bottom of communicating pipe 14 with kettle 2, the material of described liquid level tube 15 is glass, described liquid level tube 15 is provided with graduation mark 16, liquid level tube 15 can quickly view the liquid level in kettle 2, and carries out record by graduation mark.
The bottom of described chuck 13 is additionally provided with water out 11, and condensed water is discharged from water out 11.
Described kettle 2 top is provided with material inlet 1.
Described control device is PLC.
It is obvious to a person skilled in the art that this utility model is not limited to the details of above-mentioned one exemplary embodiment, and in the case of without departing substantially from spirit or essential attributes of the present utility model, it is possible to realize this utility model in other specific forms.Therefore, no matter from the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, scope of the present utility model is limited by claims rather than described above, it is intended that all changes fallen in the implication of equivalency and scope of claim included in this utility model.Should not be considered as limiting involved claim by any reference in claim.
In addition, it is to be understood that, although this specification is been described by according to embodiment, but the most each embodiment only comprises an independent technical scheme, this narrating mode of description is only for clarity sake, description should can also be formed, through appropriately combined, other embodiments that it will be appreciated by those skilled in the art that as an entirety, the technical scheme in each embodiment by those skilled in the art.

Claims (5)

1. a distillating still structure for pharmaceutical intermediate, including kettle, it is characterised in that the bottom of described kettle is provided with material outlet, is provided with submerged pump at material outlet, the outlet of described submerged pump faces material outlet;It is provided with chuck outside described kettle, the bottom of described chuck is provided with steam inlet, steam inlet is connected with the heating furnace being positioned at outside chuck by the first pipeline, it is provided with electric control valve on described first pipeline, described kettle inner top is provided with temperature sensor, described temperature sensor and electric control valve all electrically connect with control device, and described chuck top is provided with steam (vapor) outlet, and steam (vapor) outlet is connected with heating furnace by second pipe;Being provided with liquid level tube outside described kettle, the two ends of described liquid level tube were connected with the top and bottom of kettle by communicating pipe, and described liquid level tube is provided with graduation mark.
The distillating still structure of a kind of pharmaceutical intermediate the most according to claim 1, it is characterised in that the bottom of described chuck is additionally provided with water out.
The distillating still structure of a kind of pharmaceutical intermediate the most according to claim 1, it is characterised in that described kettle top is provided with material inlet.
The distillating still structure of a kind of pharmaceutical intermediate the most according to claim 1, it is characterised in that described control device is PLC.
The distillating still structure of a kind of pharmaceutical intermediate the most according to claim 1, it is characterised in that the material of described liquid level tube is glass.
CN201620138037.5U 2016-02-24 2016-02-24 Stills structure of medicine midbody Expired - Fee Related CN205549632U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201620138037.5U CN205549632U (en) 2016-02-24 2016-02-24 Stills structure of medicine midbody

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201620138037.5U CN205549632U (en) 2016-02-24 2016-02-24 Stills structure of medicine midbody

Publications (1)

Publication Number Publication Date
CN205549632U true CN205549632U (en) 2016-09-07

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201620138037.5U Expired - Fee Related CN205549632U (en) 2016-02-24 2016-02-24 Stills structure of medicine midbody

Country Status (1)

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CN (1) CN205549632U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110035809A (en) * 2016-11-10 2019-07-19 拉米罗·塞尼奥雷特·韦尔杜戈 Steam distillation extracts the equipment of volatile oil and internal distillating method in organic material
CN110090466A (en) * 2019-04-12 2019-08-06 南通华宇化工科技有限公司 A kind of temperature gradient control method in the distillation technique of medicine intermediate

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110035809A (en) * 2016-11-10 2019-07-19 拉米罗·塞尼奥雷特·韦尔杜戈 Steam distillation extracts the equipment of volatile oil and internal distillating method in organic material
CN110035809B (en) * 2016-11-10 2022-01-25 拉米罗·塞尼奥雷特·韦尔杜戈 Apparatus for extracting volatile oil from organic raw material by steam distillation and internal distillation method
CN110090466A (en) * 2019-04-12 2019-08-06 南通华宇化工科技有限公司 A kind of temperature gradient control method in the distillation technique of medicine intermediate

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Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20160907

Termination date: 20180224

CF01 Termination of patent right due to non-payment of annual fee