CN205461128U - Extraction and stratification device - Google Patents

Extraction and stratification device Download PDF

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Publication number
CN205461128U
CN205461128U CN201620271837.4U CN201620271837U CN205461128U CN 205461128 U CN205461128 U CN 205461128U CN 201620271837 U CN201620271837 U CN 201620271837U CN 205461128 U CN205461128 U CN 205461128U
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CN
China
Prior art keywords
valve
layering
pipeline
extracting
utility
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201620271837.4U
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Chinese (zh)
Inventor
王培松
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ZHONGJIN PHARMACEUTICAL CO Ltd TIANJIN
Original Assignee
ZHONGJIN PHARMACEUTICAL CO Ltd TIANJIN
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ZHONGJIN PHARMACEUTICAL CO Ltd TIANJIN filed Critical ZHONGJIN PHARMACEUTICAL CO Ltd TIANJIN
Priority to CN201620271837.4U priority Critical patent/CN205461128U/en
Application granted granted Critical
Publication of CN205461128U publication Critical patent/CN205461128U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model provides an extraction and stratification device, including the layering jar, layering tank bottoms portion is equipped with first pipeline and second pipeline, be equipped with first valve on the first pipeline, be equipped with the second valve on the second pipeline in proper order, survey mouth and third valve. Extraction and stratification device discharge lower floor twice emission of solvent time after accomplishing the layering, after discharging for the first time stop the layering liquid level and is observing a mouthful department, carry out second time after the secondary layering of waiting to stew and discharge, solved that the in -process is discharged in the layering because the liquid flow results in two kinds of solvents a small amount of the mix to appear, adopt the layering of this decker secondary can effectively improve the purity of solution, promotion product quality.

Description

A kind of extracting and demixing device
Technical field
This utility model belongs to medicine and manufactures field, especially relates to a kind of extracting and demixing device.
Background technology
Refining abstraction technique to be widely used in pharmacy, chemical industry and food service industry, enterprise is carrying out refinement extraction Need when taking to be layered, after reaching two kinds of demixing of solvents, lower floor's solvent will be drained, and ensure upper strata The purity of solvent, prior art is directly discharged in lower floor's dissolving agent process, owing to the flowing of liquid can cause There is a small amount of mixing in layered portion, causes purity to decline, affects quality and the effect of product.
Utility model content
In view of this, this utility model is directed to a kind of extracting and demixing device, to avoid in extracting and demixing During, there is a small amount of mixing in two kinds of solvents, it is impossible to thoroughly by two kinds of materials separately, reduce the product of product Matter.
For reaching above-mentioned purpose, the technical solution of the utility model is achieved in that
A kind of extracting and demixing device, including layering tank, described layering pot bottom is provided with the first pipeline and second Pipeline, described first pipeline is provided with the first valve, described second pipe is sequentially provided with the second valve, Observation port and the 3rd valve.
Further, described layering pot bottom connects cooling pipe, and described cooling pipe is distributed in the shape of a spiral In layering tank, it is possible to reduce dissolubility by cooling, improve extraction degree.
Further, described first pipe level is arranged.
Further, described second pipe layering tank to before the 3rd valve for being vertically arranged, through the 3rd It is horizontally disposed with after valve.
Further, described layering pot bottom is inverted conical shape, is 45 degree of overturning angles with vertical direction.
Further, described first valve, the second valve and the 3rd valve are gate valve, ball valve, stop valve In one.
Further, described observation port material is glass or transparent plastic, and observation port is externally provided with reinforcement.
Relative to prior art, a kind of extracting and demixing device described in the utility model has the advantage that
A kind of extracting and demixing device described in the utility model is discharged lower floor's solvent time-division after completing layering Twice discharge, rests at observation port by laminated fluid level after discharge for the first time, and secondary stratification to be stood is laggard Row discharge for the second time, solves in layering discharge process owing to liquid flowing causes two kinds of solvents to occur on a small quantity Mixing, uses this decker secondary stratification can be effectively improved the purity of solution, improving product quality.
Accompanying drawing explanation
The accompanying drawing constituting a part of the present utility model is further appreciated by of the present utility model for providing, Schematic description and description of the present utility model is used for explaining this utility model, is not intended that this reality With novel improper restriction.In the accompanying drawings:
Fig. 1 is the structural representation described in this utility model embodiment.
Description of reference numerals:
1-is layered tank, 2-cooling pipe, 3-the second valve, 4-observation port, 5-the 3rd valve, 6-first Valve.
Detailed description of the invention
It should be noted that in the case of not conflicting, in embodiment in this utility model and embodiment Feature can be mutually combined.
In description of the present utility model, it is to be understood that term " " center ", " longitudinally ", " horizontal stroke To ", " on ", D score, "front", "rear", "left", "right", " vertically ", " water Flat ", the orientation that indicates of " top ", " end ", " interior ", " outward " etc. or position relationship be based on attached Orientation shown in figure or position relationship, be for only for ease of description this utility model and simplify description, and not Be instruction or the hint device of indication or element must have specific orientation, with specific azimuth configuration and Operation, therefore it is not intended that to restriction of the present utility model.Additionally, term " first ", " second " Etc. being only used for describing purpose, and it is not intended that instruction or hint relative importance or implicit indicate indication The quantity of the technical characteristic shown.Thus, the feature defining " first ", " second " etc. can be expressed Or implicitly include one or more this feature.In description of the present utility model, unless otherwise Illustrating, " multiple " are meant that two or more.
In description of the present utility model, it should be noted that unless otherwise clearly defined and limited, Term " is installed ", " being connected ", " connection " should be interpreted broadly, and connects for example, it may be fixing, Can also be to removably connect, or be integrally connected;Can be to be mechanically connected, it is also possible to be electrical connection; Can be to be joined directly together, it is also possible to be indirectly connected to by intermediary, can be the company of two element internals Logical.For the ordinary skill in the art, can understand that above-mentioned term is at this by concrete condition Concrete meaning in utility model.
Describe this utility model below with reference to the accompanying drawings and in conjunction with the embodiments in detail.
As it is shown in figure 1, a kind of extracting and demixing device, including layering tank 1, bottom described layering tank 1 it is Inverted conical shape, is 45 degree of overturning angles with vertical direction, be provided with bottom described layering tank 1 first pipeline, Second pipe and cooling pipe 2, described cooling pipe 2 is distributed in layering tank 1 in the shape of a spiral, it is possible to Reduce dissolubility by cooling, improve extraction degree.Described first pipeline is provided with the first valve 6, described The second valve 3, observation port 4 and the 3rd valve 5 it is sequentially provided with on second pipe.Described first Pipeline Water Flat arrange, described second pipe before layering tank 1 to the 3rd valve 5 for being vertically arranged, through the 3rd valve It is horizontally disposed with after door 5.Described observation port 4 material is glass or transparent plastic, and observation port 4 is externally provided with Reinforcement.Described first valve the 6, second valve 3 and the 3rd valve 5 are gate valve, ball valve, stop valve In one.
A kind of extracting and demixing device described in the utility model closes the first valve 6 and the 3rd valve 5, quiet Put and make ethyl acetate and water stratification in layering tank, after then waiting for extracting and demixing, see at observation port 4 Observe laminated fluid level, if it is all water that observation port 4 is observed, open the 3rd valve 5, discharge under being positioned at The water of layer, until observation port 4 is able to observe that laminated fluid level position, closes the 3rd after observing layering Valve 5, has a small amount of water to be mixed in ethyl acetate during just draining, needs to wait second After secondary clearing, close the second valve 3, open the 3rd valve 5, discharge and be positioned at the second valve 3 and the 3rd After liquid between valve 5, layering tank 1 just can leave the ethyl acetate that purity is higher, open first Valve 6 is discharged by the first pipeline and is collected.
The foregoing is only preferred embodiment of the present utility model, not in order to limit this utility model, All within spirit of the present utility model and principle, any modification, equivalent substitution and improvement etc. made, Within should be included in protection domain of the present utility model.

Claims (7)

1. an extracting and demixing device, it is characterised in that: include being layered tank (1), described layering tank (1) bottom is provided with the first pipeline and second pipe, and described first pipeline is provided with the first valve (6), The second valve (3), observation port (4) and the 3rd valve (5) it is sequentially provided with on described second pipe.
A kind of extracting and demixing device the most according to claim 1, it is characterised in that: described layering Tank (1) bottom connects cooling pipe (2), and described cooling pipe (2) is distributed in layering in the shape of a spiral In tank (1).
A kind of extracting and demixing device the most according to claim 1, it is characterised in that: described first Pipe level is arranged.
A kind of extracting and demixing device the most according to claim 1, it is characterised in that: described second Pipeline is front for being vertically arranged to the 3rd valve (5), after the 3rd valve (5) in layering tank (1) It is horizontally disposed with.
A kind of extracting and demixing device the most according to claim 1, it is characterised in that: described layering Tank (1) bottom is inverted conical shape, is 45 degree of overturning angles with vertical direction.
A kind of extracting and demixing device the most according to claim 1, it is characterised in that: described first Valve (6), the second valve (3) and the 3rd valve (5) are in gate valve, ball valve, stop valve Kind.
A kind of extracting and demixing device the most according to claim 1, it is characterised in that: described observation Mouth (4) material is glass or transparent plastic, and observation port (4) is externally provided with reinforcement.
CN201620271837.4U 2016-03-31 2016-03-31 Extraction and stratification device Expired - Fee Related CN205461128U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201620271837.4U CN205461128U (en) 2016-03-31 2016-03-31 Extraction and stratification device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201620271837.4U CN205461128U (en) 2016-03-31 2016-03-31 Extraction and stratification device

Publications (1)

Publication Number Publication Date
CN205461128U true CN205461128U (en) 2016-08-17

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Application Number Title Priority Date Filing Date
CN201620271837.4U Expired - Fee Related CN205461128U (en) 2016-03-31 2016-03-31 Extraction and stratification device

Country Status (1)

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CN (1) CN205461128U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108854158A (en) * 2017-05-16 2018-11-23 湖北生物医药产业技术研究院有限公司 Resin column elutes liquor collecting device
CN113082775A (en) * 2021-03-31 2021-07-09 张田田 Chemical solution separating tank

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108854158A (en) * 2017-05-16 2018-11-23 湖北生物医药产业技术研究院有限公司 Resin column elutes liquor collecting device
CN108854158B (en) * 2017-05-16 2023-11-07 湖北生物医药产业技术研究院有限公司 Resin column eluent collection device
CN113082775A (en) * 2021-03-31 2021-07-09 张田田 Chemical solution separating tank
CN113082775B (en) * 2021-03-31 2022-07-29 山东龙华生物股份有限公司 Chemical solution separating tank

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Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20160817

Termination date: 20180331

CF01 Termination of patent right due to non-payment of annual fee