CN205461107U - Reactive crystallization jar for crystallization - Google Patents
Reactive crystallization jar for crystallization Download PDFInfo
- Publication number
- CN205461107U CN205461107U CN201620183017.XU CN201620183017U CN205461107U CN 205461107 U CN205461107 U CN 205461107U CN 201620183017 U CN201620183017 U CN 201620183017U CN 205461107 U CN205461107 U CN 205461107U
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- tank body
- electric heater
- heater unit
- crystallization tank
- mounting seat
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Abstract
The utility model discloses a reactive crystallization jar for crystallization, including the crystallizer body, high -pressure injection pump, air compressor and electric heater unit, electric heater unit internally mounted has the heater strip, the last business turn over gas port that is equipped with of electric heater unit, and the air inlet that electric heater unit is connected to the air duct is passed through to air compressor's gas outlet, and high -pressure gas that air compressor produced produces high temperature high -pressure gas through adding of heater strip under the heat effect, and electric heater unit's gas outlet is connected with hot gas flow tube, the utility model discloses with reaction solution with vaporific form blowout for its can be faster with high -temperature gas the heat exchange, has accelerated the evaporation rate of solvent like this, thereby has improved holistic work efficiency.
Description
Technical field
This utility model relates to crystallization apparatus, and specifically a kind of crystal separates out uses reactive crystallization tank.
Background technology
Inside chemistry, after the saturated solution cooling of heat, solute separates out with the form of crystal, and this process is crystallization；Crystallization (crystalllzatlon) refers to the process that solid solute separates out from (mistake) saturated solution.The solute separated out from solution is broadly divided into crystalline precipitate and amorphous sediment.Crystalline precipitate is prone to leach from solution.The granule of crystal the biggest and uniform time, entrainment mother liquor is few, it is easy to washing；Crystallizing the thinnest and uneven crystal, often form thick paste thing, entrainment mother liquor is more, and the most uncomplicated laundering is not even difficult to filter, and the most also can pass through filter paper, and therefore crystallization reaction groove use in actual crystallization process is the biggest.
Evaporative crystallization is the most conventional crystallization means, evaporation solvent, solution is made to be become saturated from unsaturation, continue evaporation, superfluous solute will separate out in crystal, makes evaporative crystallization, traditional seashore evaporate brine and be evaporative crystallization, but the form of evaporative crystallization is bigger in the various power consumption of industrial process, it is therefore desirable to improved this.
Utility model content
The purpose of this utility model is to provide a kind of crystal precipitation reactive crystallization tank, with the problem solving to propose in above-mentioned background technology.
For achieving the above object, the following technical scheme of this utility model offer:
A kind of crystal separates out uses reactive crystallization tank, including crystallization tank body, HP jetting pump, air compressor and electric heater unit, described electric heater unit is internally installed heater strip, electric heater unit is provided with air inlet/outlet, the gas outlet of air compressor connects the air inlet of electric heater unit by airway, the gases at high pressure that air compressor produces produce high temperature and high pressure gas under the heat effect of heater strip, the gas outlet of electric heater unit connects steam flow tube, and steam flow tube extends to crystallize the inner side of tank body, the inwall of crystallization tank body is provided with the air current spray nozzle mounting seat being vertically arranged, and multiple air current spray nozzle is installed in air current spray nozzle mounting seat, air current spray nozzle is by being in charge of connect relative with steam flow tube, the outfan level of air current spray nozzle is towards a left side, level high-temperature high-pressure air flow to the left can be ejected hence with air current spray nozzle；The inlet of described HP jetting pump connects liquid suction pipe, and liquid suction pipe extends to crystallize the inside bottom of tank body；The liquid outlet of HP jetting pump connects liquid-in pipe, liquid-in pipe extends to crystallize the inner side of tank body, it is additionally provided with, on the inwall of crystallization tank body, the atomizer mounting seat being vertically arranged, and atomizer mounting seat and air current spray nozzle mounting seat are just to setting, in atomizer mounting seat, atomizer is installed, the outfan level of atomizer is towards the right side, level vaporific reaction solution to the right can be ejected hence with atomizer, the most vaporific reaction solution and high temperature and high pressure gas realize rapidly heat exchange, aqueous solvent in vaporific reaction solution then can absorb heat rapid evaporation, concentrated reaction solution after Nong Suoing then can fall into crystallization tank interior, now the row that is drawn into again by liquid suction pipe carries out further heat exchange evaporation；The lower end of described liquid suction pipe is provided with dividing plate, utilizes dividing plate can realize the judgement of liquid level；The top of described crystallization tank body is provided with blower fan, and steam can quickly be detached by blower fan.
As further program of the utility model: described liquid suction pipe is positioned at crystallizer body inner opposite end and is cased with metal filter screen, metal filter screen is utilized to prevent bigger precipitation crystal from entering in pipeline.
As this utility model further scheme: the tip position of described atomizer mounting seat is 0.7m-1.5m with the inside top distance size of crystallization tank body.
As this utility model further scheme: described crystallization tank body uses the design of vacuum clip laminar, ensures the heat insulating ability of entirety with this.
Compared with prior art, the beneficial effects of the utility model are: this utility model by reaction solution with vaporific form ejection so that its can heat exchange faster with high-temperature gas, so accelerate the evaporation rate of solvent, thus improve the work efficiency of entirety.
Accompanying drawing explanation
Fig. 1 is the structural representation of this utility model a kind of crystal precipitation reactive crystallization tank.
In figure: 1-crystallizes tank body, 2-HP jetting pump, 3-air compressor, 4-electric heater unit, 5-heater strip, 6-airway, 7-steam flow tube, 8-air current spray nozzle mounting seat, 9-air current spray nozzle, 10-liquid suction pipe, 11-dividing plate, 12-liquid-in pipe, 13-atomizer mounting seat, 14-atomizer, 15-blower fan.
Detailed description of the invention
Below in conjunction with the accompanying drawing in this utility model embodiment, the technical scheme in this utility model embodiment is clearly and completely described, it is clear that described embodiment is only a part of embodiment of this utility model rather than whole embodiments.Based on the embodiment in this utility model, the every other embodiment that those of ordinary skill in the art are obtained under not making creative work premise, broadly fall into the scope of this utility model protection.
nullRefer to Fig. 1，In this utility model embodiment，A kind of crystal separates out uses reactive crystallization tank，Including crystallization tank body 1、HP jetting pump 2、Air compressor 3 and electric heater unit 4，Described electric heater unit 4 is internally installed heater strip 5，Electric heater unit 4 is provided with air inlet/outlet，The gas outlet of air compressor 3 connects the air inlet of electric heater unit 4 by airway 6，The gases at high pressure that air compressor 3 produces produce high temperature and high pressure gas under the heat effect of heater strip 5，The gas outlet of electric heater unit 4 connects steam flow tube 7，And steam flow tube 7 extends to crystallize the inner side of tank body 1，The inwall of crystallization tank body 1 is provided with the air current spray nozzle mounting seat 8 being vertically arranged，And multiple air current spray nozzle 9 is installed in air current spray nozzle mounting seat 8，Air current spray nozzle 9 docks with steam flow tube 7 phase by being in charge of，The outfan level of air current spray nozzle 9 is towards a left side，Level high-temperature high-pressure air flow to the left can be ejected hence with air current spray nozzle 9；The inlet of described HP jetting pump 2 connects liquid suction pipe 10, and liquid suction pipe 10 extends to crystallize the inside bottom of tank body 1；The liquid outlet of HP jetting pump 2 connects liquid-in pipe 12, liquid-in pipe 12 extends to crystallize the inner side of tank body 1, it is additionally provided with, on the inwall of crystallization tank body 1, the atomizer mounting seat 13 being vertically arranged, and atomizer mounting seat 13 and air current spray nozzle mounting seat 8 are just to setting, atomizer 14 is installed in atomizer mounting seat 13, the outfan level of atomizer 14 is towards the right side, level vaporific reaction solution to the right can be ejected hence with atomizer 14, the most vaporific reaction solution and high temperature and high pressure gas realize rapidly heat exchange, aqueous solvent in vaporific reaction solution then can absorb heat rapid evaporation, it is internal that concentrated reaction solution after Nong Suoing then can fall into crystallization tank body 1, now the row that is drawn into again by liquid suction pipe 10 carries out further heat exchange evaporation；The lower end of described liquid suction pipe 10 is provided with dividing plate 11, utilizes dividing plate 11 can realize the judgement of liquid level；The top of described crystallization tank body 1 is provided with blower fan 15, and steam can quickly be detached by blower fan 15.
Described liquid suction pipe 10 is positioned at crystallization tank body 1 inner opposite end and is cased with metal filter screen, utilizes metal filter screen to prevent bigger precipitation crystal from entering in pipeline.
The tip position of described atomizer mounting seat 13 is 0.7m-1.5m with the inside top distance size of crystallization tank body 1.
Described crystallization tank body 1 uses vacuum clip laminar to design, and ensures the heat insulating ability of entirety with this.
Operation principle of the present utility model is: utilize atomizer 14 can eject level vaporific reaction solution to the right, the most vaporific reaction solution and high temperature and high pressure gas realize rapidly heat exchange, aqueous solvent in vaporific reaction solution then can absorb heat rapid evaporation, it is internal that concentrated reaction solution after Nong Suoing then can fall into crystallization tank body 1, and now the row that is drawn into again by liquid suction pipe 10 carries out further heat exchange evaporation；Steam can quickly be detached by blower fan 15, and whole efficiency is high, the most energy-conservation.
It is obvious to a person skilled in the art that this utility model is not limited to the details of above-mentioned one exemplary embodiment, and in the case of without departing substantially from spirit or essential attributes of the present utility model, it is possible to realize this utility model in other specific forms.Therefore, no matter from the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, scope of the present utility model is limited by claims rather than described above, it is intended that all changes fallen in the implication of equivalency and scope of claim included in this utility model.Should not be considered as limiting involved claim by any reference in claim.
In addition, it is to be understood that, although this specification is been described by according to embodiment, but the most each embodiment only comprises an independent technical scheme, this narrating mode of description is only for clarity sake, description should can also be formed, through appropriately combined, other embodiments that it will be appreciated by those skilled in the art that as an entirety, the technical scheme in each embodiment by those skilled in the art.
Claims (4)
1. a crystal separates out and uses reactive crystallization tank, it is characterized in that, including crystallization tank body, HP jetting pump, air compressor and electric heater unit, described electric heater unit is internally installed heater strip, electric heater unit is provided with air inlet/outlet, the gas outlet of air compressor connects the air inlet of electric heater unit by airway, the gas outlet of electric heater unit connects steam flow tube, and steam flow tube extends to crystallize the inner side of tank body, the inwall of crystallization tank body is provided with the air current spray nozzle mounting seat being vertically arranged, and multiple air current spray nozzle is installed in air current spray nozzle mounting seat, air current spray nozzle is by being in charge of connect relative with steam flow tube, the outfan level of air current spray nozzle is towards a left side；The inlet of described HP jetting pump connects liquid suction pipe, and liquid suction pipe extends to crystallize the inside bottom of tank body；The liquid outlet of HP jetting pump connects liquid-in pipe, liquid-in pipe extends to crystallize the inner side of tank body, it is additionally provided with, on the inwall of crystallization tank body, the atomizer mounting seat being vertically arranged, and atomizer mounting seat and air current spray nozzle mounting seat are just to setting, being provided with atomizer in atomizer mounting seat, the outfan level of atomizer is towards the right side；The lower end of described liquid suction pipe is provided with dividing plate；The top of described crystallization tank body is provided with blower fan.
Crystal precipitation reactive crystallization tank the most according to claim 1, it is characterised in that described liquid suction pipe is positioned at crystallizer body inner opposite end and is cased with metal filter screen.
Crystal precipitation reactive crystallization tank the most according to claim 1, it is characterised in that the tip position of described atomizer mounting seat is 0.7m-1.5m with the inside top distance size of crystallization tank body.
Crystal precipitation reactive crystallization tank the most according to claim 1, it is characterised in that described crystallization tank body uses the design of vacuum clip laminar.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620183017.XU CN205461107U (en) | 2016-03-10 | 2016-03-10 | Reactive crystallization jar for crystallization |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620183017.XU CN205461107U (en) | 2016-03-10 | 2016-03-10 | Reactive crystallization jar for crystallization |
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| Publication Number | Publication Date |
|---|---|
| CN205461107U true CN205461107U (en) | 2016-08-17 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620183017.XU Expired - Fee Related CN205461107U (en) | 2016-03-10 | 2016-03-10 | Reactive crystallization jar for crystallization |
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| Country | Link |
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| CN (1) | CN205461107U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106241425A (en) * | 2016-08-30 | 2016-12-21 | 安徽今朝环保科技有限公司 | Industrial slag salt transport vehicle based on helical feed |
| CN115069189A (en) * | 2022-07-23 | 2022-09-20 | 西安国康瑞金制药有限公司 | A reaction unit for progesterone preparation |
-
2016
- 2016-03-10 CN CN201620183017.XU patent/CN205461107U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106241425A (en) * | 2016-08-30 | 2016-12-21 | 安徽今朝环保科技有限公司 | Industrial slag salt transport vehicle based on helical feed |
| CN115069189A (en) * | 2022-07-23 | 2022-09-20 | 西安国康瑞金制药有限公司 | A reaction unit for progesterone preparation |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160817 Termination date: 20170310 |
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| CF01 | Termination of patent right due to non-payment of annual fee |