CN205435752U - Annular reactor - Google Patents
Annular reactor Download PDFInfo
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- CN205435752U CN205435752U CN201620300530.2U CN201620300530U CN205435752U CN 205435752 U CN205435752 U CN 205435752U CN 201620300530 U CN201620300530 U CN 201620300530U CN 205435752 U CN205435752 U CN 205435752U
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- 238000010438 heat treatment Methods 0.000 claims abstract description 23
- 239000000463 material Substances 0.000 claims abstract description 12
- 238000006243 chemical reaction Methods 0.000 abstract description 18
- 238000012546 transfer Methods 0.000 abstract description 14
- 239000012530 fluid Substances 0.000 abstract description 9
- 239000000376 reactant Substances 0.000 abstract description 8
- 239000012295 chemical reaction liquid Substances 0.000 abstract description 7
- 238000003756 stirring Methods 0.000 abstract description 6
- 238000009826 distribution Methods 0.000 abstract description 4
- 238000009827 uniform distribution Methods 0.000 abstract description 4
- 239000003607 modifier Substances 0.000 abstract description 3
- 238000010979 pH adjustment Methods 0.000 abstract description 3
- 238000000034 method Methods 0.000 abstract description 2
- 238000009434 installation Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000006276 transfer reaction Methods 0.000 description 1
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Abstract
本实用新型公开了一种环形反应器,包括盘管、循环泵出口、循环泵、循环泵入口、进料口、加料泵和加热套,所述加料泵通过导管与进料口连接。本实用新型通过循环泵使反应液在环形反应器内循环流动达到搅拌目的,根据流体的湍流现象来实现反应体系内物料的均匀分布,通过设置加料泵,可使物料较均匀的分散在反应体系中,因湍流出现返混现象会使反应液混合均匀、反应体系充分接触、反应物均一分布,根据此特点还可进行pH的调节以及改性剂的微量添加,通过柔性加热套,增加传热面积,提高传热效率,柔性加热套通过对反应装置360度无死角包覆进行加热操作时,流体可以充分与管壁接触,有较大的传热面积,使反应物体系温度分布均匀,无温度梯度。
The utility model discloses an annular reactor, which comprises a coil pipe, a circulating pump outlet, a circulating pump, a circulating pump inlet, a feeding port, a feeding pump and a heating jacket. The feeding pump is connected to the feeding port through a conduit. The utility model uses a circulation pump to make the reaction liquid circulate in the annular reactor to achieve the purpose of stirring, and realizes the uniform distribution of materials in the reaction system according to the turbulent flow phenomenon of the fluid. By setting the feeding pump, the materials can be more evenly dispersed in the reaction system. In the process, due to the turbulent back-mixing phenomenon, the reaction solution will be mixed evenly, the reaction system will be fully contacted, and the reactants will be uniformly distributed. According to this feature, pH adjustment and trace addition of modifiers can also be carried out. Through the flexible heating jacket, heat transfer can be increased. Area, improve heat transfer efficiency, when the flexible heating jacket covers the reaction device 360 degrees without dead angle for heating operation, the fluid can fully contact with the tube wall, with a large heat transfer area, so that the temperature distribution of the reactant system is uniform, without Temperature gradient.
Description
技术领域technical field
本实用新型具体涉及一种环形反应器,属于反应器技术领域。The utility model specifically relates to an annular reactor, which belongs to the technical field of reactors.
背景技术Background technique
环形反应器是近年来发展起来的一种新型反应器,主要特征是通过外加机械能强制流体作定向的、有规则的循环流动,并在流动中完成混合、传质、传热和化学反应。自从其问世以来,学者们对其进行了种种研究,开发了它的各种应用领域。近年来,它以结构简单,传热传质性能良好、生产强度大等优点在高分子合成工业、生物化学工业和石油化工业等领域中越来越引起人们的重视。传统试验中的电动搅拌由支架、电机、搅拌棒、转速控制装置等组成,安装繁琐有时还会因安装不当而导致实验设备的损坏。The loop reactor is a new type of reactor developed in recent years. The main feature is that the fluid is forced to make a directional and regular circulation flow through the external mechanical energy, and the mixing, mass transfer, heat transfer and chemical reaction are completed in the flow. Since its appearance, scholars have conducted various researches on it and developed its various application fields. In recent years, it has attracted more and more attention in the fields of polymer synthesis industry, biochemical industry and petrochemical industry because of its simple structure, good heat and mass transfer performance, and high production intensity. The electric stirring in the traditional test is composed of a bracket, a motor, a stirring rod, a speed control device, etc. The installation is cumbersome and sometimes the experimental equipment will be damaged due to improper installation.
实用新型内容Utility model content
本实用新型要解决的技术问题克服现有的缺陷,提供一种环形反应器,通过循环泵使反应液在环形反应器内循环流动达到搅拌目的,根据流体的湍流现象来实现反应体系内物料的均匀分布,通过设置加料泵,可使物料较均匀的分散在反应体系中,因湍流出现返混现象会使反应液混合均匀、反应体系充分接触、反应物均一分布,根据此特点还可进行pH的调节以及改性剂的微量添加,通过柔性加热套,增加传热面积,提高传热效率,柔性加热套通过对反应装置360度无死角包覆进行加热操作时,流体可以充分与管壁接触,有较大的传热面积,使反应物体系温度分布均匀,无温度梯度,可以有效解决背景技术中的问题。The technical problem to be solved by the utility model overcomes the existing defects, and provides an annular reactor. The reaction liquid is circulated in the annular reactor through a circulation pump to achieve the purpose of stirring, and the material in the reaction system is realized according to the turbulent flow phenomenon of the fluid. Uniform distribution, by setting the feeding pump, the material can be dispersed in the reaction system more evenly, the back-mixing phenomenon due to turbulent flow will make the reaction liquid mixed evenly, the reaction system is fully contacted, and the reactants are evenly distributed. According to this feature, pH can also be adjusted The adjustment and the micro-addition of the modifier, through the flexible heating jacket, increase the heat transfer area and improve the heat transfer efficiency. When the flexible heating jacket covers the reaction device 360 degrees without dead angle for heating operation, the fluid can fully contact the tube wall , has a large heat transfer area, makes the temperature distribution of the reactant system uniform and has no temperature gradient, and can effectively solve the problems in the background technology.
为了解决上述技术问题,本实用新型提供了如下的技术方案:In order to solve the above technical problems, the utility model provides the following technical solutions:
本实用新型提供一种环形反应器,包括盘管、循环泵出口、循环泵、循环泵入口、进料口、加料泵和加热套,所述加料泵通过导管与进料口连接,所述进料口设置在盘管上,所述盘管被加热套包裹,所述盘管上还设有循环泵入口,所述循环泵入口通过循环泵与循环泵出口连接。The utility model provides an annular reactor, which comprises a coil pipe, a circulating pump outlet, a circulating pump, a circulating pump inlet, a feeding port, a feeding pump and a heating jacket, the feeding pump is connected to the feeding port through a conduit, and the feeding The material inlet is arranged on the coil pipe, and the coil pipe is wrapped by the heating jacket. The coil pipe is also provided with a circulation pump inlet, and the circulation pump inlet is connected with the circulation pump outlet through the circulation pump.
作为本实用新型的一种优选技术方案,所述加热套由柔性材料制成。As a preferred technical solution of the present invention, the heating jacket is made of flexible materials.
本实用新型所达到的有益效果是:一种环形反应器,通过循环泵使反应液在环形反应器内循环流动达到搅拌目的,根据流体的湍流现象来实现反应体系内物料的均匀分布,通过设置加料泵,可使物料较均匀的分散在反应体系中,因湍流出现返混现象会使反应液混合均匀、反应体系充分接触、反应物均一分布,根据此特点还可进行pH的调节以及改性剂的微量添加,通过柔性加热套,增加传热面积,提高传热效率,柔性加热套通过对反应装置360度无死角包覆进行加热操作时,流体可以充分与管壁接触,有较大的传热面积,使反应物体系温度分布均匀,无温度梯度。The beneficial effects achieved by the utility model are: an annular reactor, the reaction liquid circulates in the annular reactor through a circulating pump to achieve the purpose of stirring, and the uniform distribution of the materials in the reaction system is realized according to the turbulent flow phenomenon of the fluid. The feeding pump can make the material more uniformly dispersed in the reaction system. Due to the back-mixing phenomenon of turbulent flow, the reaction liquid will be mixed evenly, the reaction system will be fully contacted, and the reactants will be uniformly distributed. According to this feature, pH adjustment and modification can also be performed. The micro-addition of the agent, through the flexible heating jacket, increases the heat transfer area and improves the heat transfer efficiency. When the flexible heating jacket covers the reaction device 360 degrees without dead ends for heating operation, the fluid can fully contact the tube wall, and there is a large The heat transfer area makes the temperature distribution of the reactant system uniform and there is no temperature gradient.
附图说明Description of drawings
附图用来提供对本实用新型的进一步理解,并且构成说明书的一部分,与本实用新型的实施例一起用于解释本实用新型,并不构成对本实用新型的限制。The accompanying drawings are used to provide a further understanding of the utility model, and constitute a part of the description, and are used to explain the utility model together with the embodiments of the utility model, and do not constitute a limitation to the utility model.
在附图中:In the attached picture:
图1是本实用新型实施例所述的一种环形反应器整体结构示意图;Fig. 1 is a schematic diagram of the overall structure of a ring reactor described in the embodiment of the present invention;
图中标号:1、盘管;2、循环泵出口;3、循环泵;4、循环环泵入口;5、进料口;6、加料泵;7、加热套。Labels in the figure: 1. Coil; 2. Circulation pump outlet; 3. Circulation pump; 4. Circulation ring pump inlet; 5. Feed inlet; 6. Feed pump; 7. Heating jacket.
具体实施方式detailed description
以下结合附图对本实用新型的优选实施例进行说明,应当理解,此处所描述的优选实施例仅用于说明和解释本实用新型,并不用于限定本实用新型。The preferred embodiments of the present utility model are described below in conjunction with the accompanying drawings. It should be understood that the preferred embodiments described here are only used to illustrate and explain the present utility model, and are not intended to limit the present utility model.
实施例:请参阅图1,本实用新型一种环形反应器,包括盘管1、循环泵出口2、循环泵3、循环泵入口4、进料口5、加料泵6和加热套7,所述加料泵6通过导管与进料口5连接,所述进料口5设置在盘管1上,所述盘管1被加热套7包裹,所述盘管1上还设有循环泵入口4,所述循环泵入口4通过循环泵3与循环泵出口2连接,所述加热套7由柔性材料制成。Embodiment: please refer to Fig. 1, a kind of annular reactor of the present utility model, comprises coil pipe 1, circulation pump outlet 2, circulation pump 3, circulation pump inlet 4, feed inlet 5, feeding pump 6 and heating mantle 7, all The feed pump 6 is connected to the feed port 5 through a conduit, the feed port 5 is arranged on the coil 1, the coil 1 is wrapped by the heating jacket 7, and the coil 1 is also provided with a circulation pump inlet 4 , the circulation pump inlet 4 is connected to the circulation pump outlet 2 through the circulation pump 3, and the heating jacket 7 is made of flexible material.
需要说明的是,本实用新型为一种环形反应器,工作时,通过循环泵使反应液在环形反应器内循环流动达到搅拌目的,根据流体的湍流现象来实现反应体系内物料的均匀分布,通过设置加料泵,可使物料较均匀的分散在反应体系中,因湍流出现返混现象会使反应液混合均匀、反应体系充分接触、反应物均一分布,根据此特点还可进行pH的调节以及改性剂的微量添加,通过柔性加热套,增加传热面积,提高传热效率,柔性加热套通过对反应装置360度无死角包覆进行加热操作时,流体可以充分与管壁接触,有较大的传热面积,使反应物体系温度分布均匀,无温度梯度。It should be noted that the utility model is an annular reactor. When working, the circulating pump circulates the reaction liquid in the annular reactor to achieve the purpose of stirring, and realizes the uniform distribution of materials in the reaction system according to the turbulent flow phenomenon of the fluid. By setting the feeding pump, the material can be dispersed evenly in the reaction system. Due to the turbulent back-mixing phenomenon, the reaction liquid will be mixed evenly, the reaction system will be fully contacted, and the reactants will be uniformly distributed. According to this feature, pH adjustment and The micro-addition of the modifier increases the heat transfer area and improves the heat transfer efficiency through the flexible heating jacket. When the flexible heating jacket covers the reaction device at 360 degrees without dead angle for heating operation, the fluid can fully contact with the tube wall, and the The large heat transfer area makes the temperature distribution of the reactant system uniform without temperature gradient.
最后应说明的是:以上所述仅为本实用新型的优选实施例而已,并不用于限制本实用新型,尽管参照前述实施例对本实用新型进行了详细的说明,对于本领域的技术人员来说,其依然可以对前述各实施例所记载的技术方案进行修改,或者对其中部分技术特征进行等同替换。凡在本实用新型的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本实用新型的保护范围之内。Finally, it should be noted that: the above is only a preferred embodiment of the utility model, and is not intended to limit the utility model, although the utility model has been described in detail with reference to the foregoing embodiments, for those skilled in the art , it is still possible to modify the technical solutions described in the foregoing embodiments, or perform equivalent replacements for some of the technical features. Any modification, equivalent replacement, improvement, etc. made within the spirit and principles of the present utility model shall be included in the protection scope of the present utility model.
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Cited By (1)
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CN106905449A (en) * | 2017-03-28 | 2017-06-30 | 北京化工大学 | A kind of ring-like dynamic response device of blade rotor |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN106905449A (en) * | 2017-03-28 | 2017-06-30 | 北京化工大学 | A kind of ring-like dynamic response device of blade rotor |
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