CN205379897U - Polymerization facility of novel stone material protective agent of fluorine silicon - Google Patents

Polymerization facility of novel stone material protective agent of fluorine silicon Download PDF

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Publication number
CN205379897U
CN205379897U CN201620197500.3U CN201620197500U CN205379897U CN 205379897 U CN205379897 U CN 205379897U CN 201620197500 U CN201620197500 U CN 201620197500U CN 205379897 U CN205379897 U CN 205379897U
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China
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protective agent
fluorine silicon
polyplant
novel stone
barrel
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CN201620197500.3U
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Chinese (zh)
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裴金东
李建
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QUZHOU FLUORIDE AND SILICON RESEARCH INSTITUTES
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QUZHOU FLUORIDE AND SILICON RESEARCH INSTITUTES
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Abstract

The utility model discloses a polymerization facility of novel stone material protective agent of fluorine silicon, by the continuous feeding system, the polymeric kettle becomes with accuse temperature fluid bank of cells, the polymeric kettle includes barrel and agitator motor, agitator motor rotates and is connected with the stirring rake, the stirring rake sets up in the barrel, be equipped with the barrel apron on the barrel, be equipped with the evacuation mouth on the barrel apron, the inert gas entry, drain and charge door, the charge door links to each other with the continuous feeding system, the bottom of barrel is equipped with the discharge gate, be equipped with on the barrel and press from both sides the cover, press from both sides the cover and control temperature fluid groove and link to each other, it is connected with the fluid transportation pump to press from both sides between cover and the accuse temperature fluid groove, accuse temperature fluid is carried to pressing from both sides the cover to the fluid transportation pump. The utility model discloses but moisture content in the effective control polymeric kettle, the influence is stable with the moisture contact to avoid the material, adopt continuous feeding system dropwise add material, the product degree of consistency is high, excellent performance, adopting accuse temperature fluid groove and can guaranteeing that the temperature is steady, prevent local implode, product property that production obtained can be good, the storage life is long.

Description

A kind of polyplant of fluorine silicon Novel stone protective agent
Technical field
This utility model belongs to chemicals production device technique field, particularly relates to the polyplant of a kind of fluorine silicon Novel stone protective agent.
Background technology
Proidonite material protective agent is the stone protectant product of latest generation, in breathability with silicone based stone protector product similar, but waterproof and oilproof is antifouling and on weather resistance more than silicone based stone protector product fine, it is expected to progressively replace silicone based stone protectant product, is the product of a kind of good market prospect.
Proidonite material protective agent is a kind of copolymerized polymer product, and copolymerization uniformity affects properties of product;It addition, this product is to water sensitive, moisture can affect product stability, and then affects properties of product.
Utility model content
This utility model purpose is in that the above-mentioned technical problem solving exist in prior art, the polyplant of a kind of fluorine silicon Novel stone protective agent is provided, can effectively controlling moisture in polymeric kettle, realize continuous feed and steady temperature control, the proidonite material protective agent properties of product of production are excellent, it is long to store the phase.
In order to solve above-mentioned technical problem, this utility model adopts the following technical scheme that
A kind of polyplant of fluorine silicon Novel stone protective agent, it is characterized in that: by continuous feed system, polymeric kettle and temperature controlled fluid groove composition, polymeric kettle includes cylinder and stirring motor, stirring motor is rotatably connected to stirring paddle, stirring paddle is arranged in cylinder, cylinder is provided with cylinder cover plate, cylinder cover plate is provided with vacuum orifice, inert gas entrance, drain and charge door, charge door is connected with continuous feed system, the bottom of cylinder is provided with discharging opening, cylinder is provided with chuck, chuck is connected with temperature controlled fluid groove, it is connected to fluid delivery pump between chuck and temperature controlled fluid groove, fluid delivery pump carries temperature controlled fluid to chuck.
Further, vacuum orifice place is provided with vacuum valve.
Further, inert gas entrance place is provided with inert gas entrance valve.
Further, drain place is provided with atmospheric valve.
Further, charge door place is provided with charging valve, and described discharge outlet is provided with outlet valve.
Further, stirring paddle is made up of rotating shaft and blade, and blade is fixed on the bottom of rotating shaft.
Further, stirring motor is fire-proof motor.
Further, temperature controlled fluid is water.
This utility model, owing to have employed technique scheme, has the advantages that
This utility model has vacuum orifice and inert gas entrance, it is possible to reduce the purpose of moisture in polymeric kettle by the constantly displacement of evacuation and logical noble gas, it is to avoid the moisture adverse effect to material stability;In polymeric kettle, material contains organic solvent, the stirring motor adopted should select fire-proof motor, stirring paddle is made up of rotating shaft and blade, blade is fixed and bottom rotating shaft, according to barrel lenght, blade is likely to be arranged to multiple structure, makes stirring more abundant, it is easy to mass-and heat-transfer, in the middle part of rotating shaft, blade can be set up in appropriate location;Continuous feed system can regulate the charging proportioning of feed rate and different material, controls the polymerization uniformity, with the product of excellent;Employing temperature controlled fluid heats, and heats up steadily, it is possible to avoid the hot-spot phenomenons such as the barrel wall that steam heating causes, it is prevented that implode occurs.Such this utility model can effectively control moisture in polymeric kettle, it is to avoid material and contact with moisture and affect stability;Adopting continuous feed system dropping material, the product uniformity is high, function admirable;Adopting temperature controlled fluid groove to can ensure that heating and cooling are steady, it is prevented that local implode, the proidonite material protective agent properties of product that production obtains are excellent, it is long to store the phase.
Accompanying drawing explanation
Below in conjunction with accompanying drawing, the utility model is described in further detail:
Fig. 1 is the structural representation of the polyplant of this utility model a kind of fluorine silicon Novel stone protective agent.
Number in the figure: 1-continuous feed system, 2-polymeric kettle, 3-temperature controlled fluid groove, 4-fluid delivery pump, 21-cylinder, 22-stirring motor, 23-stirring paddle, 231-rotating shaft, 232-blade, 24-cylinder cover plate, 25-vacuum orifice, 26-inert gas entrance, 27-drain, 28-charge door, 29-vacuum valve, 210-inert gas entrance valve, 211-atmospheric valve, 212-charging valve, 213-discharging opening, 214-outlet valve, 215-chuck.
Detailed description of the invention
As it is shown in figure 1, be the polyplant of this utility model a kind of fluorine silicon Novel stone protective agent, it is made up of continuous feed system 1, polymeric kettle 2 and temperature controlled fluid groove 3.Polymeric kettle 2 includes cylinder 21 and stirring motor 22, and stirring motor 22 is rotatably connected to stirring paddle 23, and stirring paddle 23 is arranged in cylinder 21, and stirring paddle 23 is made up of rotating shaft 231 and blade 232, and blade 232 is fixed on the bottom of rotating shaft 231.Cylinder 21 is provided with cylinder cover plate 24, and cylinder cover plate 24 is provided with vacuum orifice 25, inert gas entrance 26, drain 27 and charge door 28.Vacuum orifice 25 place is provided with vacuum valve 29, and inert gas entrance 26 place is provided with inert gas entrance valve 210, and drain 27 place is provided with atmospheric valve 211, and charge door 28 place is provided with charging valve 212, and charge door 28 is connected with continuous feed system 1.The bottom of cylinder 21 is provided with discharging opening 213, and discharging opening 213 place is provided with outlet valve 214.Cylinder 21 is provided with chuck 215, and chuck 215 is connected with temperature controlled fluid groove 3, is connected to fluid delivery pump 4 between chuck 215 and temperature controlled fluid groove 3, and fluid delivery pump 4 carries temperature controlled fluid to chuck 215, and temperature controlled fluid is preferably water.The each junction of this utility model adopts tetrafluoro washer sealing, and adopts bolt to fasten.
This utility model has vacuum orifice 25, inert gas entrance 26 and drain 27, it is possible to reduce the purpose of moisture in polymeric kettle 2 by the constantly displacement of evacuation and logical noble gas, it is to avoid the moisture adverse effect to material stability;In polymeric kettle 2, material contains organic solvent, the stirring motor 22 adopted selects fire-proof motor, stirring paddle 23 is made up of 231 and blade 232, blade 232 is fixed and bottom 231, according to cylinder 21 length, blade 232 is likely to be arranged to multiple structure, makes stirring more abundant, it is easy to mass-and heat-transfer, in the middle part of 231, blade 232 can be set up in appropriate location;Continuous feed system 1 can regulate the charging proportioning of feed rate and different material, controls the polymerization uniformity, with the product of excellent;Employing temperature controlled fluid heats, and heats up steadily, it is possible to avoid the hot-spot phenomenons such as the barrel wall that steam heating causes, it is prevented that implode occurs.
This utility model is when producing, it is first shut off outlet valve 214 and charging valve 212, then pass through vacuum valve 29, polymeric kettle 2 is carried out purging displacement by the switching of inert gas entrance valve 210 and atmospheric valve 211, remove moisture, dewater qualified after, partial material is added by continuous feed system 1, subsequently, stirring motor 22 drives stirring paddle 23 to carry out being sufficiently stirred for effect, and by the temperature controlled fluid in temperature controlled fluid groove 3, temperature of charge in still is risen to setting reaction temperature, after temperature of charge arrives design temperature, start to drip leftover materials, after dropwising, continue insulation polymerization certain time, make polymerization abundant, after being incubated, cooling stopped reaction, and discharging.The proidonite material protective agent properties of product that this utility model production obtains are excellent, it is long to store the phase.
These are only specific embodiment of the utility model, but technical characteristic of the present utility model is not limited thereto.Any based on this utility model, for solving essentially identical technical problem, it is achieved essentially identical technique effect, done simple change, equivalent replacement or modification etc., all it is covered by among protection domain of the present utility model.

Claims (8)

1. the polyplant of a fluorine silicon Novel stone protective agent, it is characterized in that: by continuous feed system, polymeric kettle and temperature controlled fluid groove composition, described polymeric kettle includes cylinder and stirring motor, described stirring motor is rotatably connected to stirring paddle, described stirring paddle is arranged in described cylinder, described cylinder is provided with cylinder cover plate, described cylinder cover plate is provided with vacuum orifice, inert gas entrance, drain and charge door, described charge door is connected with described continuous feed system, the bottom of described cylinder is provided with discharging opening, described cylinder is provided with chuck, described chuck is connected with described temperature controlled fluid groove, it is connected to fluid delivery pump between described chuck and described temperature controlled fluid groove, described fluid delivery pump carries temperature controlled fluid to described chuck.
2. the polyplant of a kind of fluorine silicon Novel stone protective agent according to claim 1, it is characterised in that: described vacuum orifice place is provided with vacuum valve.
3. the polyplant of a kind of fluorine silicon Novel stone protective agent according to claim 1, it is characterised in that: described inert gas entrance place is provided with inert gas entrance valve.
4. the polyplant of a kind of fluorine silicon Novel stone protective agent according to claim 1, it is characterised in that: described drain place is provided with atmospheric valve.
5. the polyplant of a kind of fluorine silicon Novel stone protective agent according to claim 1, it is characterised in that: described charge door place is provided with charging valve, and described discharge outlet is provided with outlet valve.
6. the polyplant of a kind of fluorine silicon Novel stone protective agent according to claim 1, it is characterised in that: described stirring paddle is made up of rotating shaft and blade, and described blade is fixed on the bottom of described rotating shaft.
7. the polyplant of a kind of fluorine silicon Novel stone protective agent according to claim 1, it is characterised in that: described stirring motor is fire-proof motor.
8. the polyplant of a kind of fluorine silicon Novel stone protective agent according to claim 1, it is characterised in that: described temperature controlled fluid is water.
CN201620197500.3U 2016-03-15 2016-03-15 Polymerization facility of novel stone material protective agent of fluorine silicon Active CN205379897U (en)

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CN201620197500.3U CN205379897U (en) 2016-03-15 2016-03-15 Polymerization facility of novel stone material protective agent of fluorine silicon

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Application Number Priority Date Filing Date Title
CN201620197500.3U CN205379897U (en) 2016-03-15 2016-03-15 Polymerization facility of novel stone material protective agent of fluorine silicon

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108479663A (en) * 2018-04-03 2018-09-04 英丽化学(上海)股份有限公司 A kind of decabromodiphenylethane production preparation facilities
CN112221456A (en) * 2020-10-29 2021-01-15 昌和化学新材料(江苏)有限公司 Low-acid-value triphenyl phosphite production process and device

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108479663A (en) * 2018-04-03 2018-09-04 英丽化学(上海)股份有限公司 A kind of decabromodiphenylethane production preparation facilities
CN112221456A (en) * 2020-10-29 2021-01-15 昌和化学新材料(江苏)有限公司 Low-acid-value triphenyl phosphite production process and device
CN112221456B (en) * 2020-10-29 2023-09-05 昌和化学新材料(江苏)有限公司 Process and device for producing triphenyl phosphite with low acid value

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