CN205360659U - Chemical industry crystallization kettle convenient to observe and ejection of compact - Google Patents
Chemical industry crystallization kettle convenient to observe and ejection of compact Download PDFInfo
- Publication number
- CN205360659U CN205360659U CN201620114524.8U CN201620114524U CN205360659U CN 205360659 U CN205360659 U CN 205360659U CN 201620114524 U CN201620114524 U CN 201620114524U CN 205360659 U CN205360659 U CN 205360659U
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- crystallization kettle
- gear
- crystallization
- endosome
- stirring rod
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Abstract
The utility model discloses a chemical industry crystallization kettle convenient to observe and ejection of compact, including crystallization kettle ectosome, crystallization kettle endosome, agitating unit and discharging device, be provided with the intermediate layer cavity between crystallization kettle ectosome and the crystallization kettle endosome, crystallization kettle endosome top is provided with the feed inlet, intermediate layer cavity top is connected with the wet return, and the bottom is connected with the inlet tube, the inside agitating unit that is provided with of crystallization kettle endosome, be provided with the observation window on the crystallization kettle endosome lateral wall, crystallization kettle endosome bottom is provided with the discharge gate, the discharge gate bottom is connected with discharging device, the utility model discloses a set up the observation window on the lateral wall of crystallization kettle endosome to setting up the thermocouple on agitating unit, making people can learn the temperature conditions in the crystallization kettle in real time, the people of can being convenient for adjust the reaction temperature comparatively accurately, thereby improve reaction effect, accord with people's demand, what the filter that sets up was more convenient will tie post -crystalline crystal and liquid separation, save process time.
Description
Technical field
This utility model relates to a kind of chemical industry equipment, and specifically a kind of being easy to observes the chemical crystallization still with discharging.
Background technology
Crystallization kettle is after mixing of materials reaction, the crystallizer that interlayer domestic demand chilled water or chilled water are sharply lowered the temperature, it is by setting high accuracy polishing in the size of interlayer area, the version of agitator and material outlet form, tank body, and cleans the requirement without dead angle in tank body and meet technique use condition；Owing in crystallization kettle, space is bigger, when reacting, upper strata is often bigger with the temperature contrast of lower floor, and traditional simple measuring accuracy is not high, and cannot in real time the temperature in crystallization kettle be measured, thus cannot accurately measure temperature conditions when material reacts in crystallization kettle, reaction condition more can not be regulated and controled by people accurately, it is impossible to be applicable to the reaction that the precise requirements of temperature is higher, thus greatly limit its use scope；Meanwhile, there is also discharging opening and easily lump, the defect such as non-separation of solid-liquid after crystallization.
Utility model content
The purpose of this utility model is in that to provide a kind of being easy to observe the chemical crystallization still with discharging, with the problem solving to propose in above-mentioned background technology.
For achieving the above object, this utility model provides following technical scheme:
A kind of being easy to observes the chemical crystallization still with discharging, including body, agitating device and drawing mechanism in crystallization kettle ectosome, crystallization kettle；It is provided with interlayer cavity between body in described crystallization kettle ectosome and crystallization kettle；In crystallization kettle, body top is provided with charging aperture；Described interlayer cavity top is connected to return pipe, and bottom is connected to water inlet pipe；Described return pipe is connected with cooling water tank；Described water inlet pipe is connected with water pump；Described water pump is connected with cooling water tank by connecting tube；In crystallization kettle, body is internally provided with agitating device；Described agitating device includes rotating rod, scrapes wall blade, upper stirring rod and lower stirring rod；It is provided with in the middle part of described rotating rod and scrapes described in wall blade stirring rod and be arranged to I-shaped；Described lower stirring rod is arranged to U-shaped；Rotating rod, upper stirring rod and lower stirring rod are provided with thermocouple；Described thermocouple is connected with display screen by the internal wire arranged of rotating rod；Rotating rod inner hollow, top is fixing with the second gear to be connected；Described second gear is arranged in actuating device；Described actuating device is additionally provided with the first gear；Described first gear is fixedly connected in the rotating shaft of the first motor；Described first motor is arranged on the upper surface of actuating device；First gear and the second gear engage each other；Second gear is provided above display screen fixture；Body sidewall is provided with in crystallization kettle observation window；Discharging opening it is provided with bottom body in crystallization kettle；It is connected to drawing mechanism bottom described discharging opening；Described drawing mechanism is provided with screen plate, comb teeth and drawing mechanism baffle plate；The filtering holes of described screen plate is less than the diameter of crystal；Described comb teeth is arranged on the fixing axle of comb teeth；The rotating shaft of the fixing axle of described comb teeth and the second motor is fixing to be connected.
As further program of the utility model: described charging aperture stretches out crystallization kettle ectosome five centimetres；Charging aperture is furnished with charging mask.
As further program of the utility model: bottom described display screen fixture in movable embedding the second gear, top is fixing with display screen to be connected.
As this utility model further scheme: be provided with support bottom described crystallization kettle ectosome.
Compared with prior art, the beneficial effects of the utility model are:
This utility model by arranging observation window on the sidewall of body in crystallization kettle, and thermocouple is set on agitating device so that people can learn the temperature conditions in crystallization kettle in real time, it is possible to is easy to people and comparatively accurately reaction temperature is adjusted, thus improving reaction effect, meet people's demand；Crystal after crystallization is separated by screen plate more easily that arrange with liquid, and the crystal separated can directly participate in follow-up reaction, saves process time；Arranging of comb teeth ensures that the crystal of outflow will not lump excessive, even if there being the crystal of bulk also can be rubbed by comb teeth when being gathered in discharging opening, facilitates discharging.
Accompanying drawing explanation
Fig. 1 is for ease of observing the structural representation of the chemical crystallization still with discharging.
Fig. 2 is for ease of observing and the structural representation of actuating device in the chemical crystallization still of discharging.
Fig. 3 is for ease of observing and the structural representation of upper stirring rod and lower stirring rod in the chemical crystallization still of discharging.
Fig. 4 is for ease of observing and the structural representation of drawing mechanism in the chemical crystallization still of discharging.
In figure: 1-the first motor, 2-actuating device, 3-crystallization kettle ectosome, 4-interlayer cavity, body in 5-crystallization kettle, 6-scrapes wall blade, the upper stirring rod of 7-, 8-observation window, stirring rod under 9-, 10-discharging opening, 11-support, 12-drawing mechanism, 13-water inlet pipe, 14-water pump, 15-connecting tube, 16-cooling water tank, 17-return pipe, 18-rotating rod, 19-charging aperture, 20-charging mask, 21-display screen, 22-the first gear, 23-the second gear, 24-display screen fixture, 25-thermocouple, 26-screen plate, 27-comb teeth, 28-comb teeth fixes axle, 29-the second motor, 30-drawing mechanism baffle plate.
Detailed description of the invention
Below in conjunction with detailed description of the invention, the technical scheme of this patent is described in more detail.
Referring to Fig. 1-4, a kind of being easy to observes the chemical crystallization still with discharging, including body 5, agitating device and drawing mechanism 12 in crystallization kettle ectosome 3, crystallization kettle；It is provided with interlayer cavity 4 between body 5 in described crystallization kettle ectosome 3 and crystallization kettle；In crystallization kettle, body 5 top is provided with charging aperture 19；Described charging aperture 19 stretches out crystallization kettle ectosome 3 five centimeters；Charging aperture 19 is furnished with charging mask 20；Described charging mask 20 makes body 5 in crystallization kettle be hedged off from the outer world in crystallization process；Described interlayer cavity 4 top is connected to return pipe 17, and bottom is connected to water inlet pipe 13；Described return pipe 17 is connected with cooling water tank 16；Described water inlet pipe 13 is connected with water pump 14；Described water pump 14 is connected with cooling water tank 16 by connecting tube 15；When cooling down, by water pump 14, the cold water in cooling water tank 16 is pumped in interlayer cavity 4, it is back in cooling water tank 16 by the return pipe 17 of interlayer cavity 4 top setting after cold water absorption heat to carry out hot water cooling, so circulate, it is simple in crystallization kettle, the material in body 5 carries out sufficient crystallising；In crystallization kettle, body 5 is internally provided with agitating device；Described agitating device includes rotating rod 18, scrapes wall blade 6, upper stirring rod 7 and lower stirring rod 9；It is provided with in the middle part of described rotating rod 18 and scrapes wall blade 6；Described wall blade 6 of scraping is under the material scraper that will be attached in crystallization kettle on body 5, it is simple to discharging；Described upper stirring rod 7 is arranged to I-shaped；Described lower stirring rod 9 is arranged to U-shaped；Upper stirring rod 7 and lower stirring rod 9 are used for increasing stirring area, are material sufficient crystallisings；Rotating rod 18, upper stirring rod 7 and lower stirring rod 9 are provided with thermocouple 25；Described thermocouple 25 is connected with display screen 21 by the internal wire arranged of rotating rod 18；Rotating rod 18 inner hollow, top is fixing with the second gear 23 to be connected；Described second gear 23 is arranged in actuating device 2；Described actuating device 2 is additionally provided with the first gear 22；Described first gear 22 is fixedly connected in the rotating shaft of the first motor 1；Described first motor 1 is arranged on the upper surface of actuating device 2；First gear 22 and the second gear 23 engage each other, and transfer power on rotating rod 18, and rotating rod 18 drives upper stirring rod 7 and lower stirring rod 9 to be stirred；Second gear 23 is provided above display screen fixture 24；Bottom described display screen fixture 24 in movable embedding the second gear 23, top is fixing with display screen 21 to be connected；Described display screen 21, for showing the temperature that thermocouple 25 passes over, reaches in monitor in real time crystallization kettle the purpose of temperature of charge in body 5；In crystallization kettle, body 5 sidewall is provided with observation window 8；Described observation window 8 is used for observing crystallization process；Discharging opening 10 it is provided with bottom body 5 in crystallization kettle；It is connected to drawing mechanism 12 bottom described discharging opening 10；Described drawing mechanism 12 is provided with screen plate 26, comb teeth 27 and drawing mechanism baffle plate 30；The filtering holes of described screen plate 26, less than the diameter of crystal, is arranged to drawer type, it is simple to dismounting；Described comb teeth 27 is arranged on the fixing axle 28 of comb teeth；The fixing axle 28 of described comb teeth is fixing with the rotating shaft of the second motor 29 to be connected；The setting of comb teeth 27 is easy to crystal and is quickly removed, and improves work efficiency；Described drawing mechanism baffle plate 30 is for keeping the sealing of body 5 in crystallization kettle in crystallization process；It is provided with support 11 bottom crystallization kettle ectosome 3, is used for supporting whole device.
Above the better embodiment of this patent is explained in detail, but this patent is not limited to above-mentioned embodiment, in the ken that one skilled in the relevant art possesses, it is also possible to make a variety of changes under the premise without departing from this patent objective.
Claims (4)
1. it is easy to observe the chemical crystallization still with discharging, including body, agitating device and drawing mechanism in crystallization kettle ectosome, crystallization kettle；It is characterized in that, in described crystallization kettle ectosome and crystallization kettle, between body, be provided with interlayer cavity；In crystallization kettle, body top is provided with charging aperture；Described interlayer cavity top is connected to return pipe, and bottom is connected to water inlet pipe；Described return pipe is connected with cooling water tank；Described water inlet pipe is connected with water pump；Described water pump is connected with cooling water tank by connecting tube；In crystallization kettle, body is internally provided with agitating device；Described agitating device includes rotating rod, scrapes wall blade, upper stirring rod and lower stirring rod；It is provided with in the middle part of described rotating rod and scrapes described in wall blade stirring rod and be arranged to I-shaped；Described lower stirring rod is arranged to U-shaped；Rotating rod, upper stirring rod and lower stirring rod are provided with thermocouple；Described thermocouple is connected with display screen by the internal wire arranged of rotating rod；Rotating rod inner hollow, top is fixing with the second gear to be connected；Described second gear is arranged in actuating device；Described actuating device is additionally provided with the first gear；Described first gear is fixedly connected in the rotating shaft of the first motor；Described first motor is arranged on the upper surface of actuating device；First gear and the second gear engage each other；Second gear is provided above display screen fixture；Body sidewall is provided with in crystallization kettle observation window；Discharging opening it is provided with bottom body in crystallization kettle；It is connected to drawing mechanism bottom described discharging opening；Described drawing mechanism is provided with screen plate, comb teeth and drawing mechanism baffle plate；The filtering holes of described screen plate is less than the diameter of crystal；Described comb teeth is arranged on the fixing axle of comb teeth；The rotating shaft of the fixing axle of described comb teeth and the second motor is fixing to be connected.
2. according to claim 1 being easy to observes the chemical crystallization still with discharging, it is characterised in that described charging aperture stretches out crystallization kettle ectosome five centimetres；Charging aperture is furnished with charging mask.
3. according to claim 1 being easy to observes the chemical crystallization still with discharging, it is characterised in that bottom described display screen fixture in movable embedding the second gear, and top is fixing with display screen to be connected.
4. according to claim 1 being easy to observes the chemical crystallization still with discharging, it is characterised in that be provided with support bottom described crystallization kettle ectosome.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620114524.8U CN205360659U (en) | 2016-02-04 | 2016-02-04 | Chemical industry crystallization kettle convenient to observe and ejection of compact |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620114524.8U CN205360659U (en) | 2016-02-04 | 2016-02-04 | Chemical industry crystallization kettle convenient to observe and ejection of compact |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205360659U true CN205360659U (en) | 2016-07-06 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620114524.8U Expired - Fee Related CN205360659U (en) | 2016-02-04 | 2016-02-04 | Chemical industry crystallization kettle convenient to observe and ejection of compact |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205360659U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110870984A (en) * | 2018-09-04 | 2020-03-10 | 山西卓联锐科科技有限公司 | Continuous crystallizer and continuous crystallization process thereof |
-
2016
- 2016-02-04 CN CN201620114524.8U patent/CN205360659U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110870984A (en) * | 2018-09-04 | 2020-03-10 | 山西卓联锐科科技有限公司 | Continuous crystallizer and continuous crystallization process thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20170621 Address after: 416300 stone street Guzhang County Hunan Province ancient town Patentee after: Hunan Hanrui new Mstar Technology Ltd Address before: 226300 Jiangsu city of Nantong province Tongzhou District Xing Dong Zhen Sun Li Qiao Cun Dong Yi Group Patentee before: NANTONG HANRUI INDUSTRIAL CO., LTD. |
|
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160706 Termination date: 20170204 |