CN205313647U - Chloridizing distillation device for extracting germanium from germanium concentrate - Google Patents
Chloridizing distillation device for extracting germanium from germanium concentrate Download PDFInfo
- Publication number
- CN205313647U CN205313647U CN201620014875.1U CN201620014875U CN205313647U CN 205313647 U CN205313647 U CN 205313647U CN 201620014875 U CN201620014875 U CN 201620014875U CN 205313647 U CN205313647 U CN 205313647U
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- CN
- China
- Prior art keywords
- germanium
- reation kettle
- reactor
- jacket
- presss
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model provides a chloridizing distillation device for extracting germanium from germanium concentrate, including feed inlet, discharge gate, evacuation pipe, reation kettle, outer jacket, the interior cover that presss from both sides, its characterized in that: reation kettle is hollow cylindrical, reation kettle top left side is provided with the feed inlet, reation kettle top right side is provided with the discharge gate, reation kettle top central point puts the vertical driving motor of being provided with, the driving motor bottom is provided with the pivot, the pivot bottom is provided with the paddle, reation kettle bottom central point puts and is provided with the evacuation pipe, the reation kettle outside is provided with outer jacket, outer jacket inside is provided with a plurality of division boards, the outer jacket outside is provided with the shell, in being provided with, reation kettle inside presss from both sides the cover, interior clamp is sheathe in and is provided with a plurality of division boards, division board bottom central point puts and is provided with rotatable flabellum, the interior cover internal surface that presss from both sides is provided with scale graphite coating, this equipment reasonable in design standard, high durability and convenient use, has well temperature control effect through the two -layer composite design who presss from both sides the cover, can be effectual with the inside temperature control of reation kettle on germanium tetrachloride's volatilization temperature, has well adaptability.
Description
Technical field
This utility model relates to the device extracting germanium in a kind of germanium metallurgical technology, espespecially a kind of chlorinated distillation device extracting germanium from germanium concentrate.
Background technology
Germanium is the base stock of high pure semiconductor, the common method extracting germanium from germanium concentrate is to adopt chlorinated distillation method, in germanium concentrate, specifically add hydrochloric acid distill, germanium volatilizees with the form of the germanium tetrachloride of gaseous state and separates with other magazines, thus reaching to extract the purpose of germanium, owing to the volatilization temperature of germanium tetrachloride is at 84 DEG C, too high or too low for temperature all can causing in a large amount of magazine entrance volatilization gas causes impurity content too high, simultaneously because hydrochloric acid and germanium tetrachloride have strong corrosivity, reactor is required higher.
Summary of the invention
A kind of chlorinated distillation device extracting germanium from germanium concentrate is provided for the problems referred to above this utility model, this equipment specification reasonable in design, easy to use, by the composite design of two-layer chuck, there is temperature control effect well, can effectively by reactor internal temperature control on the volatilization temperature of germanium tetrachloride, there is being well adapted to property.
For solving the problems referred to above, this utility model provides a kind of chlorinated distillation device extracting germanium from germanium concentrate, including charging aperture, discharging opening, evacuated tube, reactor, external jacket, internal jacket, it is characterized in that: reactor is the cylinder of hollow, reactor top left side is provided with charging aperture, reactor top right side is provided with discharging opening, reactor top center is vertically arranged with drive motor, rotating shaft it is provided with bottom drive motor, rotating shaft bottom is provided with blade, reactor bottom centre position is provided with evacuated tube, external jacket it is provided with outside reactor, external jacket is internally provided with some demarcation strips, shell it is provided with outside external jacket, reactor is internally provided with internal jacket, internal jacket is provided with some division boards, division board bottom centre position is provided with rotating flabellum, internal jacket inner surface is provided with crystalline flake graphite coating.
As further improvement of the utility model, described demarcation strip is provided with heater strip.
As further improvement of the utility model, described outer surface of outer cover is provided with epoxy coating.
Operation principle:
This utility model is designed by the Rational structure of two-layer, there is heat insulating effect well, stablizing of internal temperature can be effectively kept by the design of internal jacket, in internal jacket, it is provided with some division boards and flabellum simultaneously, disturbance can be effectively formed, enhancing hot water contacts with reactor, form stable thermal source, by the design of external jacket, there is temperature control function well simultaneously, and on demarcation strip, be provided with heater strip can effectively external jacket effectively be heated, have and be well adapted to effect, outer surface of outer cover is provided with epoxy coating has anticorrosion well simultaneously, anti-weather performance, increase the utilization rate of reactor, the design of crystalline flake graphite coating simultaneously, there is heat conduction well and anticorrosion ability.
This utility model compared with prior art has the advantages that
1, this utility model is designed by the Rational structure of two-layer, there is heat insulating effect well, stablizing of internal temperature can be effectively kept by the design of internal jacket, in internal jacket, it is provided with some division boards and flabellum simultaneously, disturbance can be effectively formed, enhancing hot water contacts with reactor, form stable thermal source, by the design of external jacket, there is temperature control function well simultaneously, and on demarcation strip, be provided with heater strip can effectively external jacket effectively be heated, have and be well adapted to effect;
2, outer surface of outer cover being provided with epoxy coating simultaneously have anticorrosion well, anti-weather performance, increase the utilization rate of reactor, the design of crystalline flake graphite coating, has heat conduction well and anticorrosion ability simultaneously.
Accompanying drawing explanation
Fig. 1 is a kind of chlorinated distillation apparatus structure schematic diagram extracting germanium from germanium concentrate;
1-charging aperture in figure; 2-internal jacket; 3-division board; 4-rotating shaft; 5-flabellum; 6-crystalline flake graphite coating; 7-blade; 8-epoxy coating; 9-shell; 10-external jacket; 11-demarcation strip; 12-heater strip; 13-discharging opening; 14-reactor; 15-drive motor; 16-evacuated tube.
Detailed description of the invention
Below in conjunction with the accompanying drawing in this utility model embodiment; technical scheme in this utility model embodiment is clearly and completely described; obviously; described embodiment is only a part of embodiment of this utility model; rather than whole embodiments, based on the embodiment in this utility model, those of ordinary skill in the art are not under making creative work premise; the every other embodiment obtained, broadly falls into this utility model protection domain.
Embodiment 1
A kind of chlorinated distillation device extracting germanium from germanium concentrate as shown in Figure 1, including charging aperture 1, discharging opening 13, evacuated tube 16, reactor 14, external jacket 10, internal jacket 2, it is characterized in that: reactor 14 is the cylinder of hollow, reactor 14 top left side is provided with charging aperture 1, reactor 14 top right side is provided with discharging opening 13, reactor 14 top center is vertically arranged with drive motor 15, rotating shaft 4 it is provided with bottom drive motor 15, rotating shaft 4 bottom is provided with blade 7, reactor 14 bottom centre position is provided with evacuated tube 16, reactor 14 is outside is provided with external jacket 10, external jacket 10 is internally provided with some demarcation strips 11, external jacket 10 is outside is provided with shell 9, reactor 14 is internally provided with internal jacket 2, internal jacket 2 is provided with some division boards 3, division board 3 bottom centre position is provided with rotating flabellum 5, internal jacket 2 inner surface is provided with crystalline flake graphite coating 6, described demarcation strip 11 is provided with heater strip 12, described shell 9 outer surface is provided with epoxy coating 8, this utility model is designed by the Rational structure of two-layer, there is heat insulating effect well, stablizing of internal temperature can be effectively kept by the design of internal jacket, in internal jacket, it is provided with some division boards and flabellum simultaneously, disturbance can be effectively formed, enhancing hot water contacts with reactor, form stable thermal source, by the design of external jacket, there is temperature control function well simultaneously, and on demarcation strip, be provided with heater strip can effectively external jacket effectively be heated, have and be well adapted to effect, outer surface of outer cover is provided with epoxy coating has anticorrosion well simultaneously, anti-weather performance, increase the utilization rate of reactor, the design of crystalline flake graphite coating simultaneously, there is heat conduction well and anticorrosion ability.
Claims (3)
1. the chlorinated distillation device extracting germanium from germanium concentrate, including charging aperture (1), discharging opening (13), evacuated tube (16), reactor (14), external jacket (10), internal jacket (2), it is characterized in that: the cylinder that reactor (14) is hollow, reactor (14) top left side is provided with charging aperture (1), reactor (14) top right side is provided with discharging opening (13), reactor (14) top center is vertically arranged with drive motor (15), drive motor (15) bottom is provided with rotating shaft (4), rotating shaft (4) bottom is provided with blade (7), reactor (14) bottom centre position is provided with evacuated tube (16), reactor (14) is outside is provided with external jacket (10), external jacket (10) is internally provided with some demarcation strips (11), external jacket (10) is outside is provided with shell (9), reactor (14) is internally provided with internal jacket (2), internal jacket (2) is provided with some division boards (3), division board (3) bottom centre position is provided with rotating flabellum (5), internal jacket (2) inner surface is provided with crystalline flake graphite coating (6).
2. a kind of chlorinated distillation device extracting germanium from germanium concentrate according to claim 1, it is characterised in that: described demarcation strip (11) is provided with heater strip (12).
3. a kind of chlorinated distillation device extracting germanium from germanium concentrate according to claim 2, it is characterised in that: described shell (9) outer surface is provided with epoxy coating (8).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620014875.1U CN205313647U (en) | 2016-01-08 | 2016-01-08 | Chloridizing distillation device for extracting germanium from germanium concentrate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620014875.1U CN205313647U (en) | 2016-01-08 | 2016-01-08 | Chloridizing distillation device for extracting germanium from germanium concentrate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205313647U true CN205313647U (en) | 2016-06-15 |
Family
ID=56201159
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620014875.1U Expired - Fee Related CN205313647U (en) | 2016-01-08 | 2016-01-08 | Chloridizing distillation device for extracting germanium from germanium concentrate |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205313647U (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109507224A (en) * | 2018-12-07 | 2019-03-22 | 谭丽娟 | A kind of building materials volatility detection method |
| CN111218559A (en) * | 2018-11-26 | 2020-06-02 | 广东先导稀材股份有限公司 | Melt evaporation device and method |
| CN115301176A (en) * | 2022-08-17 | 2022-11-08 | 临沂市海鑫化工设备有限公司 | High-speed heat exchange glass lining container with jacket provided with guide plate |
-
2016
- 2016-01-08 CN CN201620014875.1U patent/CN205313647U/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111218559A (en) * | 2018-11-26 | 2020-06-02 | 广东先导稀材股份有限公司 | Melt evaporation device and method |
| CN109507224A (en) * | 2018-12-07 | 2019-03-22 | 谭丽娟 | A kind of building materials volatility detection method |
| CN109507224B (en) * | 2018-12-07 | 2021-04-02 | 苏州市相城检测股份有限公司 | Building material volatility detection method |
| CN115301176A (en) * | 2022-08-17 | 2022-11-08 | 临沂市海鑫化工设备有限公司 | High-speed heat exchange glass lining container with jacket provided with guide plate |
| CN115301176B (en) * | 2022-08-17 | 2024-02-02 | 临沂市海鑫化工设备有限公司 | High-speed heat exchange glass lining container with guide plate on jacket |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160615 Termination date: 20210108 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |