CN205182734U - High -efficient reation kettle with refrigerating plant - Google Patents
High -efficient reation kettle with refrigerating plant Download PDFInfo
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- CN205182734U CN205182734U CN201520900265.7U CN201520900265U CN205182734U CN 205182734 U CN205182734 U CN 205182734U CN 201520900265 U CN201520900265 U CN 201520900265U CN 205182734 U CN205182734 U CN 205182734U
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- reation kettle
- valve
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- holding vessel
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Abstract
The utility model discloses a high -efficient reation kettle with refrigerating plant, including the reation kettle main part, the reation kettle main part outside is equipped with the hollow chamber of U type, and the hollow intracavity portion of U type is equipped with circulating cooling water system, and the hollow chamber of U type left side top is connected with the inlet tube, and the hollow chamber bottom of U type is connected with the outlet pipe, and reation kettle main part left side is equipped with the refrigerator, and the refrigerator passes through pipeline and the hollow chamber of U type intercommunication, and the inside center department of reation kettle main part is vertical to be equipped with the stirring pivot, the utility model discloses high -efficient reation kettle with refrigerating plant, can effectively cool down to reation kettle, the small household multiple -effect heat pump system saves resources, and the using efficiency of the equipment is improved, through vacuum suction with the material of reation kettle bottom take out in the holding vessel again the pressure release return arrange reation kettle in, it is abundant to make the material mix, dissolve thoroughly, take a sample from top to bottom and guarantee the homogeneity, save the increase power supply, the operation is thus simple, spiral shell area blade and stirring vane set up further stirring effect and the efficiency of having improved, make and react more thoroughly, improves the quality of products.
Description
Technical field
The utility model relates to a kind of reactor, specifically a kind of highly effective reaction still with refrigerating plant.
Background technology
Reactor is used to the container carrying out chemical reaction, and in order to adapt to the different requirements of various working condition, the kind of reactor is also more various, is widely used and biology, chemical industry, materialogy and semiconductor field.Existing reactor is combined reaction container, according to reaction condition to reactor structure function and the design configuring annex.From charging one react a discharging and all can complete pre-set reactions steps with higher automaticity, its structure is generally made up of kettle, transmission device, agitating device, heater, cooling device, sealing device.Existing reactor need adapt to different reaction environments, if produce a large amount of heats in course of reaction, in order to keep keeping certain temperature in cavity, that just needs to lower the temperature to kettle, the reactor of existing use, stir at the bottom of anchor and still and have certain distance, during solid-liquid mix and blend, fraction solids material causes precipitating with drain hole re-entrant portion bottom reactor because being difficult to dissolve and stir dead angle, cause the parameter index of material inconsistent up and down, affect the performance of product, there is stirring not exclusively in the reactor generally used in producing at present in addition, material reaction is problem not thoroughly.
Utility model content
The purpose of this utility model is to provide a kind of highly effective reaction still with refrigerating plant, to solve the problem proposed in above-mentioned background technology.
For achieving the above object, the utility model provides following technical scheme:
A kind of highly effective reaction still with refrigerating plant, comprise reactor main body, U-shaped hollow cavity is provided with outside described reactor main body, U-shaped hollow cavity inside is provided with circulating water cooling system, on the left of U-shaped hollow cavity, top is connected with water inlet pipe, U-shaped hollow cavity bottom is connected with outlet pipe, refrigeration machine is provided with on the left of reactor main body, refrigeration machine is communicated with U-shaped hollow cavity by pipeline, described reactor body interior center is vertically provided with stirring shaft, stirring shaft outer wall is horizontally installed with back shaft up and down, the two ends of back shaft are solid at the spiral flex point place of ribbon blade in the same plane respectively, two are provided with about ribbon blade, and it is symmetrical, spiral surrounding is arranged on stirring shaft, stirring shaft lower horizontal is connected with stirring vane, stirring shaft top to be stretched out outside reactor main body and is connected with electric rotating machine, described reactor bottom part body offers discharge nozzle, reactor bottom part body is provided with circulation discharge nozzle at discharge nozzle right-hand member, the circulating line that circulation discharge nozzle is arranged with reactor main body right vertical is connected, circulating line top is by the recycle feed pipe of holding vessel coupled reaction still body top, holding vessel comprises vacuum valve, exhaust-valve, returning charge valve, sample valve, outlet valve and vavuum pump, vacuum valve and exhaust-valve are positioned at the top of holding vessel, sample valve and outlet valve are positioned at the bottom of holding vessel, vacuum valve connects vavuum pump, returning charge valve is connected to the top of circulating line, outlet valve connects the loop head of holding vessel.
As further program of the utility model: the axis direction of the blade face orientating reaction still main body of described ribbon blade, and the hand of spiral of two ribbon blades is contrary.
As the utility model further scheme: described discharge nozzle is provided with outlet valve.
Compared with prior art, the beneficial effects of the utility model are: jointly cooled to reactor by the circulating water cooling system of U-shaped hollow cavity inside and refrigeration machine, good cooling results, cooldown rate are high, adding of refrigeration plant effectively saves the energy, add the scope of application of equipment, improve the service efficiency of equipment; The material of reactor body interior forms Matter Transfer near ribbon blade, fully can flow under the effect of ribbon blade, make to stir completely, shaft bottom is connected with stirring vane and further improves mixing effect and efficiency, inner material is fully mixed, makes reaction more abundant; By pull of vacuum, still prodelta clay material is extracted in holding vessel, returns after pressure release and be discharged in reactor, make mixing of materials abundant, dissolve thoroughly, sampling ensures uniformity up and down, saves increase power source, achieves energy saving, in operation set, simple and convenient, improve the operating efficiency of reactor.The utility model is with the highly effective reaction still of refrigerating plant, effective temperature-reducing can be carried out to reactor, economize on resources, improve equipment use efficiency, material bottom reactor to be extracted in holding vessel pressure release again by pull of vacuum to return and be discharged in reactor, make mixing of materials abundant, dissolve thoroughly, sampling ensures uniformity up and down, save increase power source, simple to operate, the setting of ribbon blade and stirring vane further increases mixing effect and efficiency in addition, make reaction more thorough, improve the quality of product.
Accompanying drawing explanation
Fig. 1 is the structural representation of the highly effective reaction still with refrigerating plant.
Fig. 2 is the structural representation of holding vessel in the highly effective reaction still with refrigerating plant.
Detailed description of the invention
Below in conjunction with the accompanying drawing in the utility model embodiment, be clearly and completely described the technical scheme in the utility model embodiment, obviously, described embodiment is only the utility model part embodiment, instead of whole embodiments.Based on the embodiment in the utility model, those of ordinary skill in the art are not making the every other embodiment obtained under creative work prerequisite, all belong to the scope of the utility model protection.
Refer to Fig. 1-2, in the utility model embodiment, a kind of highly effective reaction still with refrigerating plant, comprise reactor main body 1, U-shaped hollow cavity 2 is provided with outside described reactor main body, U-shaped hollow cavity 2 inside is provided with circulating water cooling system, on the left of U-shaped hollow cavity 2, top is connected with water inlet pipe 3, U-shaped hollow cavity 2 bottom is connected with outlet pipe 4, refrigeration machine 5 is provided with on the left of reactor main body 1, refrigeration machine 5 is communicated with U-shaped hollow cavity 2 by pipeline, jointly reactor is cooled by the circulating water cooling system of U-shaped hollow cavity 2 inside and refrigeration machine 5, good cooling results, cooldown rate is high, adding of refrigeration plant effectively saves the energy, add the scope of application of equipment, improve the service efficiency of equipment, described reactor main body 1 inside center place is vertically provided with stirring shaft 6, stirring shaft 6 outer wall is horizontally installed with back shaft 7 up and down, the two ends of back shaft 7 are solid at the spiral flex point place of ribbon blade 8 in the same plane respectively, ribbon blade about 8 is provided with two, and it is symmetrical, spiral surrounding is arranged on stirring shaft 6, the axis direction of the blade face orientating reaction still main body 1 of described ribbon blade 8, and the hand of spiral of two ribbon blades 8 is contrary, stirring shaft 6 lower horizontal is connected with stirring vane 9, stirring shaft 6 top to be stretched out outside reactor main body 1 and is connected with electric rotating machine 10, the material of reactor main body 1 inside forms Matter Transfer near ribbon blade 8, fully can flow under the effect of ribbon blade 8, make to stir completely, shaft 6 bottom is connected with stirring vane 9 and further improves mixing effect and efficiency, inner material is fully mixed, make reaction more abundant, discharge nozzle 11 is offered bottom described reactor main body 1, described discharge nozzle 11 is provided with outlet valve, circulation discharge nozzle 12 is provided with at discharge nozzle 11 right-hand member bottom reactor main body 1, the circulating line 13 that circulation discharge nozzle 12 is arranged with reactor main body 1 right vertical is connected, circulating line 13 top is by the recycle feed pipe 15 at holding vessel 14 coupled reaction still main body 1 top, holding vessel 14 comprises vacuum valve 141, exhaust-valve 142, returning charge valve 143, sample valve 144, outlet valve 145 and vavuum pump 146, vacuum valve 141 and exhaust-valve 142 are positioned at the top of holding vessel 14, sample valve 144 and outlet valve 145 are positioned at the bottom of holding vessel 14, vacuum valve 141 connects vavuum pump 146, returning charge valve 143 is connected to the top of circulating line 13, outlet valve 145 connects the loop head of holding vessel 14, by pull of vacuum, still prodelta clay material is extracted in holding vessel, return after pressure release and be discharged in reactor, make mixing of materials abundant, dissolve thoroughly, sampling ensures uniformity up and down, save increase power source, achieve energy saving, in operation set, simple and convenient, improve the operating efficiency of reactor, the utility model is with the highly effective reaction still of refrigerating plant, effective temperature-reducing can be carried out to reactor, economize on resources, improve equipment use efficiency, material bottom reactor to be extracted in holding vessel pressure release again by pull of vacuum to return and be discharged in reactor, make mixing of materials abundant, dissolve thoroughly, sampling ensures uniformity up and down, save increase power source, simple to operate, the setting of ribbon blade and stirring vane further increases mixing effect and efficiency in addition, make reaction more thorough, improve the quality of product.
Operation principle of the present utility model is: jointly cooled to reactor by the circulating water cooling system of U-shaped hollow cavity 2 inside and refrigeration machine 5, good cooling results, cooldown rate are high, adding of refrigeration plant effectively saves the energy, add the scope of application of equipment, improve the service efficiency of equipment; The material of reactor main body 1 inside forms Matter Transfer near ribbon blade 8, fully can flow under the effect of ribbon blade 8, make to stir completely, shaft 6 bottom is connected with stirring vane 9 and further improves mixing effect and efficiency, inner material is fully mixed, makes reaction more abundant; By pull of vacuum, still prodelta clay material is extracted in holding vessel, returns after pressure release and be discharged in reactor, make mixing of materials abundant, dissolve thoroughly, sampling ensures uniformity up and down, saves increase power source, achieves energy saving, in operation set, simple and convenient, improve the operating efficiency of reactor.
To those skilled in the art, obvious the utility model is not limited to the details of above-mentioned one exemplary embodiment, and when not deviating from spirit of the present utility model or essential characteristic, can realize the utility model in other specific forms.Therefore, no matter from which point, all should embodiment be regarded as exemplary, and be nonrestrictive, scope of the present utility model is limited by claims instead of above-mentioned explanation, and all changes be therefore intended in the implication of the equivalency by dropping on claim and scope are included in the utility model.Any Reference numeral in claim should be considered as the claim involved by limiting.
In addition, be to be understood that, although this description is described according to embodiment, but not each embodiment only comprises an independently technical scheme, this narrating mode of description is only for clarity sake, those skilled in the art should by description integrally, and the technical scheme in each embodiment also through appropriately combined, can form other embodiments that it will be appreciated by those skilled in the art that.
Claims (3)
1. the highly effective reaction still with refrigerating plant, comprise reactor main body, it is characterized in that, U-shaped hollow cavity is provided with outside described reactor main body, U-shaped hollow cavity inside is provided with circulating water cooling system, on the left of U-shaped hollow cavity, top is connected with water inlet pipe, U-shaped hollow cavity bottom is connected with outlet pipe, refrigeration machine is provided with on the left of reactor main body, refrigeration machine is communicated with U-shaped hollow cavity by pipeline, described reactor body interior center is vertically provided with stirring shaft, stirring shaft outer wall is horizontally installed with back shaft up and down, the two ends of back shaft are solid at the spiral flex point place of ribbon blade in the same plane respectively, two are provided with about ribbon blade, and it is symmetrical, spiral surrounding is arranged on stirring shaft, stirring shaft lower horizontal is connected with stirring vane, stirring shaft top to be stretched out outside reactor main body and is connected with electric rotating machine, described reactor bottom part body offers discharge nozzle, reactor bottom part body is provided with circulation discharge nozzle at discharge nozzle right-hand member, the circulating line that circulation discharge nozzle is arranged with reactor main body right vertical is connected, circulating line top is by the recycle feed pipe of holding vessel coupled reaction still body top, holding vessel comprises vacuum valve, exhaust-valve, returning charge valve, sample valve, outlet valve and vavuum pump, vacuum valve and exhaust-valve are positioned at the top of holding vessel, sample valve and outlet valve are positioned at the bottom of holding vessel, vacuum valve connects vavuum pump, returning charge valve is connected to the top of circulating line, outlet valve connects the loop head of holding vessel.
2. the highly effective reaction still with refrigerating plant according to claim 1, is characterized in that, the axis direction of the blade face orientating reaction still main body of described ribbon blade, and the hand of spiral of two ribbon blades is contrary.
3. the highly effective reaction still with refrigerating plant according to claim 1, it is characterized in that, described discharge nozzle is provided with outlet valve.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520900265.7U CN205182734U (en) | 2015-11-12 | 2015-11-12 | High -efficient reation kettle with refrigerating plant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520900265.7U CN205182734U (en) | 2015-11-12 | 2015-11-12 | High -efficient reation kettle with refrigerating plant |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205182734U true CN205182734U (en) | 2016-04-27 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520900265.7U Expired - Fee Related CN205182734U (en) | 2015-11-12 | 2015-11-12 | High -efficient reation kettle with refrigerating plant |
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| CN (1) | CN205182734U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114210292A (en) * | 2021-12-08 | 2022-03-22 | 浙江胡涂硅有限公司 | Preparation method and equipment of electronic-grade hexamethyldisilazane |
-
2015
- 2015-11-12 CN CN201520900265.7U patent/CN205182734U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114210292A (en) * | 2021-12-08 | 2022-03-22 | 浙江胡涂硅有限公司 | Preparation method and equipment of electronic-grade hexamethyldisilazane |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160427 Termination date: 20171112 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |