CN205115390U - Insoluble matter enrichment device - Google Patents
Insoluble matter enrichment device Download PDFInfo
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- CN205115390U CN205115390U CN201520860884.8U CN201520860884U CN205115390U CN 205115390 U CN205115390 U CN 205115390U CN 201520860884 U CN201520860884 U CN 201520860884U CN 205115390 U CN205115390 U CN 205115390U
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Abstract
The utility model provides an insoluble matter enrichment device, the device is including the retort, the retort including be used for to the retort advances ejection of compact pipeline that the feed pipeline of solvent raw materials, the 1st material that is used for discharging flow and the pipeline that is used for receiving the extract, condensers, the condenser is including being used for the 1st material with coming from the retort to flow the feeding extremely the ejection of compact pipeline that the feed pipeline of condenser, the 2nd material that is used for discharging flow, the extraction box, the extraction box including be used for to the extraction box advance the raw materials oil the pipeline, be used for to the come in pipeline of the pipeline that autocondensation ware the 2nd material flows and the extract that is used for discharging of extraction box. Device easy operation, the solvent high -usage can satisfy multiple demand by one set of device.
Description
Technical field
The utility model relates to distillation and abstraction technique field, is specifically related to a kind of enrichment or solid-liquid (liquid liquid) extractive distillation device of insolubles.
Background technology
Often containing relatively large bituminous matter, toluene insolubles and quinoline insolubles and pressed powder etc. in heavy oil product, especially coal tar wet goods oil product.The existence of these insolubless or impurity, affects the processing characteristics of oil product significantly.In industrial production, before Raw material processing, often need first to filter out these insolubless, or enrichment, concentrated and analysis are carried out to these insolubless, determine that its structure forms, take corresponding means to eliminate.
Existing enrichment or analysis bituminous matter, the technology of toluene insolubles, quinoline insolubles, often adopt centrifugal separation or suction method, these two kinds of methods are subject to the restriction of instrument, processing sample amount is less, uses a large amount of poisonous and harmful solvent toluene, quinoline etc., and need multi-step to operate in operating process, enrichment time is long, and solvent utilization ratio is low.
Utility model content
For the deficiencies in the prior art, the utility model provides a kind of insolubles enriching apparatus, described device can be applicable to heavy oil product bituminous matter, toluene insolubles, quinoline insolubles enrichment, analyze in, simple to operate, solvent utilization ratio is high, set of device can meet multiple demand, also can be applicable in various extractive distillation, and can semi continuous operation be realized.Insolubles enriching apparatus described in the utility model, structure is simple, and easy to use, can significantly improve the utilising efficiency of solvent, processing sample amount enlarges markedly.
The utility model provides a kind of insolubles enriching apparatus, and described device comprises:
Matrass, it is for the treatment of solvent, obtains the 1st stream of gas phase after process, and described matrass comprises feeding line for entering from solvent materials to described matrass, for discharging the discharging pipeline of the 1st stream and the pipeline for receiving extraction liquid;
Condenser, it obtains the 2nd stream of liquid phase for the treatment of the 1st stream from matrass after process, described condenser comprises for the 1st stream from matrass being fed to the feeding line of described condenser, being used for discharging the discharging pipeline of the 2nd stream;
Extraction box, it is for the treatment of the 2nd stream and the raw material oil product that carry out condenser, and described extraction box comprises pipeline for entering from raw material oil product to described extraction box, for the pipeline of condenser the 2nd stream and the pipeline for discharging extraction liquid of coming in described extraction box;
In insolubles enriching apparatus described in the utility model, described extraction box comprises two casings, and one is reaction box, and another is safety box, is separated between reaction box and safety box by membrane filter.The described pipeline entering raw material oil product to described extraction box is connected with reaction box, and the pipeline for condenser the 2nd stream of coming in described extraction box is connected with reaction box, is connected with safety box for the pipeline of discharging extraction liquid.
In insolubles enriching apparatus described in the utility model, in the reaction box of described extraction box, agitator is set.
In insolubles enriching apparatus described in the utility model, in the reaction box of described extraction box, well heater is set.
In insolubles enriching apparatus described in the utility model, described condenser top is provided with blow-down pipe, and described blow-down pipe is provided with stopping valve.
In insolubles enriching apparatus described in the utility model, described condenser is connected with vacuum pump.
In insolubles enriching apparatus described in the utility model, described device also comprises solvent recuperation bottle, and described solvent recuperation bottle comprises the pipeline for condenser recovered solvent being fed to described solvent recuperation bottle.
Device described in the utility model is in the enrichment, analysis of heavy oil product bituminous matter, toluene insolubles, quinoline insolubles, and simple to operate, solvent utilization ratio is high, set of device can meet multiple demand.Also can be applicable in various extractive distillation, and can semi continuous operation be realized.This insolubles enriching apparatus, is furnished with solvent feed pump, stock oil fresh feed pump and discharging pump, can more novel solvent at any time, carries out semi continuous operation, improves the treatment capacity needing rich material significantly.
Accompanying drawing explanation
Fig. 1 is insolubles enriching apparatus structural representation described in the utility model.
Embodiment
Below in conjunction with accompanying drawing, embodiment of the present utility model is described in detail, but the utility model can limit according to claim and cover multitude of different ways to be implemented.
The utility model provides a kind of insolubles enriching apparatus, and described device comprises:
Matrass 1, it is for the treatment of solvent, obtains the 1st stream of gas phase after process, and described matrass 1 comprises feeding line 6 for entering from solvent materials to described matrass, for discharging the discharging pipeline 7 of the 1st stream and the pipeline 8 for receiving extraction liquid;
Condenser 2, it is for the treatment of the 1st stream from matrass, the 2nd stream of liquid phase is obtained after process, described condenser 2 comprises for the 1st stream from matrass being fed to the feeding line 7 of described condenser, being used for discharging the discharging pipeline 9 of the 2nd stream, the discharging pipeline 9 of described discharge the 2nd stream is provided with stopping valve, described condenser top is provided with blow-down pipe 10, and described blow-down pipe 10 is provided with stopping valve 11, and described condenser is connected with vacuum pump 12;
Extraction box 3, described extraction box comprises two casings, one is reaction box 4, another is safety box 5, separated by membrane filter 15 between reaction box 4 and safety box 5, agitator and well heater are set in described reaction box, it is for the treatment of the 2nd stream and the raw material oil product that carry out condenser, described extraction box 3 comprises the pipeline 13 for entering raw material oil product to described extraction box 3, for the pipeline 9 of condenser the 2nd stream and the pipeline 8 for discharging extraction liquid of coming in described extraction box 3, the pipeline 13 wherein entering raw material oil product to described extraction box is connected with reaction box 4, pipeline 9 for condenser the 2nd stream of coming in described extraction box is connected with reaction box 4, pipeline 8 for discharging extraction liquid is connected with safety box 5.
The novel described device of this use in use, first the blow-off valve on condenser top is opened, easy volatile solvent is avoided to heat the danger such as the blast caused, then in matrass 1, solvent is added by feeding line 6, matrass is heated, the 1st stream solvent vapour produced enters condenser 2 by discharging pipeline 7, in condenser 2, condensing reflux becomes the 2nd stream and enters reaction box 4 by pipeline 9, under heating and stirring condition, in reaction box, extractive reaction is there is with the oil product being entered reaction box by pipeline 13, the extraction liquid obtained after reaction enters safety box 5 by membrane filter, enter in matrass 1 further by pipeline 8, solvent carries out double evaporation-cooling in matrass, continuous extraction, improve the utilization ratio of solvent.By continuous print extracting operation, in reaction box, be enriched insolubles, being enriched in matrass can extracted component.At the end of extraction, close the stopping valve 18 on pipeline 9, open the stopping valve 19 on pipeline 19, heating further can be carried out concentrated to mixed solution in matrass, solvent in further recovery extraction liquid, recovered solvent enters solvent recuperation bottle 17 through pipeline 16, further increases the utilization ratio of solvent.
For high boiling solvent, as quinoline etc., when device is brought into use, first close the emptying on condenser top, 11, open the vacuum pump 12 that branch road is connected, operate under the reduced pressure atmosphere of setting, heat matrass, subsequent operations above-mentioned steps is the same.
Claims (9)
1. an insolubles enriching apparatus, described device comprises:
Matrass, it is for the treatment of solvent, obtains the 1st stream of gas phase after process, and described matrass comprises feeding line for entering from solvent materials to described matrass, for discharging the discharging pipeline of the 1st stream and the pipeline for receiving extraction liquid;
Condenser, it obtains the 2nd stream of liquid phase for the treatment of the 1st stream from matrass after process, described condenser comprises for the 1st stream from matrass being fed to the feeding line of described condenser, being used for discharging the discharging pipeline of the 2nd stream;
Extraction box, it is for the treatment of the 2nd stream and the raw material oil product that carry out condenser, and described extraction box comprises pipeline for entering from raw material oil product to described extraction box, for the pipeline of condenser the 2nd stream and the pipeline for discharging extraction liquid of coming in described extraction box.
2. according to device according to claim 1, it is characterized in that: described extraction box comprises two casings, one is reaction box, and another is safety box, is separated between reaction box and safety box by membrane filter.
3. according to device according to claim 2, it is characterized in that: the described pipeline for entering raw material oil product to described extraction box is connected with reaction box, pipeline for condenser the 2nd stream of coming in described extraction box is connected with reaction box, is connected with safety box for the pipeline of discharging extraction liquid.
4. according to device according to claim 2, it is characterized in that: in the reaction box of described extraction box, agitator is set.
5. according to device according to claim 2, it is characterized in that: in the reaction box of described extraction box, well heater is set.
6. according to device according to claim 1, it is characterized in that: described condenser top is provided with blow-down pipe, and described blow-down pipe is provided with stopping valve.
7. according to device according to claim 1, it is characterized in that: described condenser is connected with vacuum pump.
8. according to device according to claim 1, it is characterized in that: describedly on the pipeline of condenser the 2nd stream of coming in described extraction box, be provided with stopping valve.
9. according to device according to claim 1, it is characterized in that: described device also comprises solvent recuperation bottle, described solvent recuperation bottle comprises the pipeline for condenser recovered solvent being fed to described solvent recuperation bottle.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520860884.8U CN205115390U (en) | 2015-11-02 | 2015-11-02 | Insoluble matter enrichment device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520860884.8U CN205115390U (en) | 2015-11-02 | 2015-11-02 | Insoluble matter enrichment device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205115390U true CN205115390U (en) | 2016-03-30 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520860884.8U Active CN205115390U (en) | 2015-11-02 | 2015-11-02 | Insoluble matter enrichment device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205115390U (en) |
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2015
- 2015-11-02 CN CN201520860884.8U patent/CN205115390U/en active Active
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| GR01 | Patent grant |