CN205055993U - Oil -water phase reation kettle - Google Patents
Oil -water phase reation kettle Download PDFInfo
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- CN205055993U CN205055993U CN201520827035.2U CN201520827035U CN205055993U CN 205055993 U CN205055993 U CN 205055993U CN 201520827035 U CN201520827035 U CN 201520827035U CN 205055993 U CN205055993 U CN 205055993U
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- material outlet
- oil phase
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Abstract
The utility model discloses an oil -water phase reation kettle, including barrel, upward elipse head, elipse head and material import down, the barrel, go up elipse head and the airtight constitution reaction kettle body of elipse head down, the material import is located the elipse head top, still include a oil -water separator, oil -water separator including install the material outlet pipe of the lower bottom of elipse head, and setting that the material outlet pipe is linked together is at the light looks drain tube of material outlet pipe side, connect at the sight glass of material outlet pipe lower extreme, install the heavy phase drain tube at the sight glass lower extreme through the outlet valve, heavy phase drain tube and sight glass between install first valve, light looks drain tube on be close to the one end of material outlet pipe is provided with the second valve. The utility model discloses the material that replaces traditional reation kettle with double -phase separator exports, directly can carry out the double -phase separation of water oil after the reaction, has shortened production cycle, the cost of using manpower sparingly.
Description
Technical field
The utility model belongs to organic phosphine production equipment field, is specifically related to a kind of water-oil phase reactor.
Background technology
At present, reactor is mainly used in the research of the type of production users such as oil, chemical industry, rubber, agricultural chemicals, dyestuff, medicine, food and various scientific experiment project, has been used for the container of the technical process such as hydrolysis, neutralization, crystallization, distillation, evaporation, storage, hydrogenation, hydrocarbonylation, polymerization, condensation, heating mixture, isothermal reaction.
The proportion of diisooctyl phosphinic acid is 0.92, water insoluble.In the preparation technology of diisooctyl phosphinic acid, diisooctyl phosphine and hydrogen peroxide reaction, generate the diisooctyl phosphinic acid aqueous solution, also needs to import in profit phase-splitter again and carry out the separation of water oil, extend the production cycle like this, add labor cost.
Utility model content
Technical problem to be solved in the utility model is to provide a kind of water-oil phase reactor, after the completion of reaction, directly carries out water-oil separating, improves efficiency.
A kind of water-oil phase reactor of the present utility model, comprise cylindrical shell, upper ellipse head, lower ellipse head and material inlet, described cylindrical shell, upper ellipse head and lower ellipse head airtight anabolic reaction still kettle, material inlet is positioned at ellipse head top, also comprises an oily-water seperating equipment; The material outlet pipe that described oily-water seperating equipment comprises the bottom being arranged on lower ellipse head, the light phase discharge piping being arranged on material outlet pipe side be connected with described material outlet pipe, be connected to the visor of material outlet pipe lower end by outlet valve, be arranged on the heavy phase discharge piping of visor lower end, between described heavy phase discharge piping and visor, the first valve is installed; One end near described material outlet pipe on described light phase discharge piping is provided with the second valve.
Further, the vortex original paper that is positioned at reactor inner bottom is also comprised.
Further, described vortex original paper is fixed on the fixed support that is positioned at below vortex original paper, and described fixed support is welded on reactor.
Further, described material inlet extends in the kettle of reactor, in J type, and the inwall of the bottom orientating reaction still of material inlet.
Further, the bottom of described material inlet towards reactor inwall on be provided with impingement baffle.
Further, the upper ellipse head of described reactor is also provided with drain and nitrogen interface outward.
Further, the two ends up and down of described cylindrical shell outer peripheral face are respectively arranged with interface of the level gauge and lower interface of the level gauge.
Further, described upper interface of the level gauge and lower interface of the level gauge all adopt gusset to fix.
Beneficial effect:
(1) the utility model two-phase laminated flow device replaces the material outlet of traditional reactor, directly can carry out the separation of water oil two-phase after the completion of reaction, shorten the production cycle, save human cost.
(2) in the bottom of reactor, vortex original paper is installed, opens vortex original paper after the reaction, make the oil phase in reactor and aqueous phase be that vortex shape stirs, such two be on good terms after better separate, reduce the two-phase mixtures layer of two phase-contact surfaces, improve product quality, improve productive rate.
(3) material mouth of the present utility model is designed to J type, and when can effectively avoid reinforced, material be directly large batch of falls in reactor; An impingement baffle is set on reactor inwall simultaneously, also reduces the uneven distribution of fluid and the erosion to reactor inwall.
Accompanying drawing explanation
Fig. 1 is the structural representation of the utility model reactor;
Wherein 1-cylindrical shell, the upper ellipse head of 2-, ellipse head under 3-, 4-material inlet, 5-material outlet pipe, 6-visor, the light phase discharge piping of 7-, 8-heavy phase discharge piping, 9-outlet valve, 10-first valve, 11-second valve, 12-vortex original paper, 13-fixed support, 14-nitrogen interface, 15-drain, the upper interface of the level gauge of 16-, interface of the level gauge under 17-, 18-gusset, 19-impingement baffle.
Detailed description of the invention
Embodiment of the present utility model is further illustrated below in conjunction with accompanying drawing.
Embodiment 1
As shown in Figure 1, a kind of water-oil phase reactor of the present utility model, comprise cylindrical shell 1, upper ellipse head 2, lower ellipse head 3 and material inlet 4, described cylindrical shell 1, upper ellipse head 2 and lower ellipse head 3 airtight anabolic reaction still kettle, material inlet 4 is positioned at ellipse head 3 top; Also comprise an oily-water seperating equipment, the material outlet pipe 5 that described oily-water seperating equipment comprises the bottom being arranged on lower ellipse head 3, the light phase discharge piping 7 being arranged on material outlet pipe 5 side be connected with described material outlet pipe 5, be connected to the visor 6 of material outlet pipe 5 lower end by outlet valve 9, be arranged on the heavy phase discharge piping 8 of visor 6 lower end, the first valve 10 is installed between described heavy phase discharge piping 8 and visor 6; One end near described material outlet pipe 5 on described light phase discharge piping 7 is provided with the second valve 11.
Also comprise the vortex original paper 12 that is positioned at reactor inner bottom, vortex original paper 12 is fixed on the fixed support 13 that is positioned at below vortex original paper 12, and described fixed support 13 is welded on reactor.
Material inlet 4 extends in the kettle of reactor, and in J type, the inwall of the bottom orientating reaction still of material inlet, this place's inwall is provided with impingement baffle 19.
Upper ellipse head 2 is outer is also provided with drain 15 and nitrogen interface 14.
The two ends up and down of cylindrical shell 1 outer peripheral face are respectively arranged with interface of the level gauge 16 and lower interface of the level gauge 17, all adopt muscle 18 to fix.
After reaction terminates, open vortex original paper, close after 20-30 minute, static 1-2 hour, opens outlet valve and the first valve, and heavy phase is flowed in visor by material outlet pipe, flows out finally by heavy phase discharge piping; When observing two phase-contact surfaces by visor, closing the first valve, obtaining the heavy phase after being separated.Then open the second valve will gently to release mutually from light phase discharge piping, or continue unlatching first valve, after observing the discharge totally of two-phase mixtures layer by visor, then close the first valve, open the second valve and will gently release mutually from from light phase discharge piping.
Wherein 1-cylindrical shell, the upper ellipse head of 2-, ellipse head under 3-, 4-material inlet, 5-material goes out pipe, 6-visor, the light phase discharge piping of 7-, 8-heavy phase discharge piping, 9-outlet valve, 10-first valve, 11-second valve, 12-vortex original paper, 13-fixed support, 14-nitrogen interface, 15-drain, the upper interface of the level gauge of 16-, interface of the level gauge under 17-, 18-gusset, 19-impingement baffle.
Be described in detail specific embodiment of the utility model above, but it is just as example, the utility model is not restricted to above description specific embodiment.To those skilled in the art, any equivalent modifications that the utility model is carried out and substituting also all among category of the present utility model.Therefore, not departing from the equalization conversion and amendment done under spirit and scope of the present utility model, be all encompassed within the scope of the utility model.
Claims (8)
1. a water-oil phase reactor, comprise cylindrical shell, upper ellipse head, lower ellipse head and material inlet, described cylindrical shell, upper ellipse head and lower ellipse head airtight anabolic reaction still kettle, material inlet is positioned at ellipse head top, it is characterized in that, also comprise an oily-water seperating equipment; The material outlet pipe that described oily-water seperating equipment comprises the bottom being arranged on lower ellipse head, the light phase discharge piping being arranged on material outlet pipe side be connected with described material outlet pipe, be connected to the visor of material outlet pipe lower end by outlet valve, be arranged on the heavy phase discharge piping of visor lower end, between described heavy phase discharge piping and visor, the first valve is installed; One end near described material outlet pipe on described light phase discharge piping is provided with the second valve.
2. water-oil phase reactor according to claim 1, is characterized in that, also comprises the vortex original paper that is positioned at reactor inner bottom.
3. water-oil phase reactor according to claim 2, is characterized in that, described vortex original paper is fixed on the fixed support that is positioned at below vortex original paper, and described fixed support is welded on reactor.
4. water-oil phase reactor according to claim 1, is characterized in that, described material inlet extends in the kettle of reactor, in J type, and the inwall of the bottom orientating reaction still of material inlet.
5. water-oil phase reactor according to claim 4, is characterized in that, the bottom of described material inlet towards reactor inwall on be provided with impingement baffle.
6. water-oil phase reactor according to claim 1, is characterized in that, the upper ellipse head of described reactor is also provided with drain and nitrogen interface outward.
7. water-oil phase reactor according to claim 1, is characterized in that, the two ends up and down of described cylindrical shell outer peripheral face are respectively arranged with interface of the level gauge and lower interface of the level gauge.
8. water-oil phase reactor according to claim 7, is characterized in that, described upper interface of the level gauge and lower interface of the level gauge all adopt gusset to fix.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520827035.2U CN205055993U (en) | 2015-10-23 | 2015-10-23 | Oil -water phase reation kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520827035.2U CN205055993U (en) | 2015-10-23 | 2015-10-23 | Oil -water phase reation kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205055993U true CN205055993U (en) | 2016-03-02 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201520827035.2U Active CN205055993U (en) | 2015-10-23 | 2015-10-23 | Oil -water phase reation kettle |
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| CN (1) | CN205055993U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107638860A (en) * | 2017-11-10 | 2018-01-30 | 大丰鑫源达化工有限公司 | High specific gravity accessory substance separator |
-
2015
- 2015-10-23 CN CN201520827035.2U patent/CN205055993U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107638860A (en) * | 2017-11-10 | 2018-01-30 | 大丰鑫源达化工有限公司 | High specific gravity accessory substance separator |
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