CN205046017U - A take off ester device for isooctane production - Google Patents
A take off ester device for isooctane production Download PDFInfo
- Publication number
- CN205046017U CN205046017U CN201520692615.5U CN201520692615U CN205046017U CN 205046017 U CN205046017 U CN 205046017U CN 201520692615 U CN201520692615 U CN 201520692615U CN 205046017 U CN205046017 U CN 205046017U
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- tower
- soda
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- export
- entry linkage
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Abstract
The utility model discloses a take off ester device for isooctane production, material jar export with pickling tower entry linkage, pickling tower export with first caustic wash tower entry linkage, export of first caustic wash tower and heat exchanger entry linkage, heat exchanger export with the water wash column entry linkage, water wash column export with the centrifuge entry linkage, centrifuge export divide into two branch roads, a branch road with second caustic wash tower entry linkage, another branch road with raffinate jar entry linkage, export of second caustic wash tower and product jar entry linkage. This device is through setting up filter, pickling tower, caustic wash tower, heat exchanger, water wash column and centrifuge, and the phenomenon that the production facility is corroded has effectively been avoided to acid esters in effective desorption material when promoting final product quality, adjust temperature and liquid flow through DCS control system, control is accurate, makes to take off continuous, stable the going on of ester process.
Description
Technical field
The utility model relates to the process for refining of Chemicals, belongs to petrochemical complex fine chemistry technical field, is specifically related to a kind of de-ester apparatus produced for octane-iso.
Background technology
Along with the fast development of Fine Chemical, the especially continuous application of biochemical technology, the Reverse Micelle System that octane-iso and other organism are formed is becoming a kind of and is integrating efficient, the separation method of the novel recovery protein of highly selective.Octane-iso will be widely used in biology,drug and chemical industry industry.By the situation of the current octane-iso output of China and the market requirement, octane-iso market is totally in the state that supply falls short of demand in recent years.China's octane-iso industry cannot meet domestic market demand and demand for exports in output always.According to forecast analysis, the relation between supply and demand in following 4 years will keep the state that supply falls short of demand, therefore is badly in need of improving the octane-iso output being used for fine chemical material market.In octane-iso preparation process, esters of gallic acid by product can be generated, the existence of this type of by product affects the quality of octane-iso product on the one hand, on the other hand under the high temperature conditions, acid esters reacts further and generates acid, and corrosion production unit, reduces equipment life, add production cost virtually, therefore need to clear up it.
Utility model content
Utility model object: the utility model object is for the deficiencies in the prior art, provides a kind of efficiency high, the easy-operating de-ester apparatus produced for octane-iso.
Technical scheme: the de-ester apparatus produced for octane-iso described in the utility model, comprise strainer, pickling tower, first soda-wash tower, interchanger, water wash column, sedimentator, residual liquid tank, second soda-wash tower and products pot, material pot outlet is connected with described pickling tower entrance, described pickling tower outlet is connected with described first soda-wash tower entrance, described first soda-wash tower outlet is connected with heat exchanger entrance, described heat exchanger exit is connected with described water wash column entrance, described water wash column outlet is connected with described sedimentator entrance, described sedimentator outlet is divided into two branch roads, one branch road is connected with described second soda-wash tower entrance, another branch road is connected with described residual liquid tank entrance, described second soda-wash tower outlet is connected with products pot entrance.
Preferably, for improving manipulation accuracy, simplify the operation flow process, and described strainer, pickling tower, the first soda-wash tower, interchanger, water wash column, sedimentator are connected DCS Controlling System with the second soda-wash tower.
Preferably, be impurity in further elimination material, be provided with scalable filtering membrane bottom described sedimentator, described scalable filtering membrane edge is connected with sedimentator inwall all the time, vertically moves in sedimentator.
Preferably, for monitoring de-ester effect in real time, at the bottom of the tower top of described water wash column and tower, acidity test instrument is set.
Beneficial effect: this device, by arranging strainer, pickling tower, soda-wash tower, interchanger, water wash column and sedimentator, the acid esters in effective elimination material, effectively prevent the phenomenon that production unit is corroded while promoting end product quality; By DCS Controlling System, temperature and liquid flow rate are regulated, control accurately, to make the carrying out that de-ester process is continuous, stable.
Accompanying drawing explanation
Fig. 1 is the utility model device schema;
Wherein 1. strainers, 2. pickling tower, 3. the first soda-wash tower, 4. interchanger, 5. water wash column, 6. sedimentator, 7. residual liquid tank, 8. the second soda-wash tower, 9. products pot, 10 acidity test instrument.
Embodiment
Below by accompanying drawing, technical solutions of the utility model are described in detail, but protection domain of the present utility model is not limited to described embodiment.
Embodiment 1: a kind of de-ester apparatus produced for octane-iso, comprise strainer 1, pickling tower 2, first soda-wash tower 3, interchanger 4, water wash column 5, sedimentator 6, residual liquid tank 7, second soda-wash tower 8 and products pot 9, material pot outlet is connected with described pickling tower 2 entrance through filter 1, described pickling tower 2 outlet is connected with described first soda-wash tower 3 entrance, described first soda-wash tower 3 outlet is connected with described interchanger 4 entrance, described interchanger 4 outlet is connected with described water wash column 5 entrance, for monitoring in real time at the bottom of the tower top of water wash column 5 described in de-ester effect and tower, acidity test instrument 10 is set, described water wash column 5 outlet is connected with described sedimentator 6 entrance, described sedimentator 6 outlet is divided into two branch roads, one branch road is connected with described second soda-wash tower 8 entrance, another branch road is connected with described residual liquid tank 7 entrance, described second soda-wash tower 8 outlet is connected with described products pot 9 entrance.
In this device, for improving manipulation accuracy, simplify the operation flow process, and described strainer, pickling tower, the first soda-wash tower, interchanger, water wash column, sedimentator are connected DCS Controlling System with the second soda-wash tower.For impurity in further elimination material, be provided with scalable filtering membrane bottom described sedimentator, described scalable filtering membrane edge is connected with sedimentator inwall all the time, vertically moves in sedimentator.
As mentioned above, although represented with reference to specific preferred embodiment and described the utility model, it shall not be construed as the restriction to the utility model self.Under the spirit and scope prerequisite of the present utility model not departing from claims definition, various change can be made in the form and details to it.
Claims (3)
1. the de-ester apparatus produced for octane-iso, it is characterized in that comprising strainer, pickling tower, first soda-wash tower, interchanger, water wash column, sedimentator, residual liquid tank, second soda-wash tower and products pot, material pot outlet is connected with described pickling tower entrance, described pickling tower outlet is connected with described first soda-wash tower entrance, described first soda-wash tower outlet is connected with heat exchanger entrance, described heat exchanger exit is connected with described water wash column entrance, described water wash column outlet is connected with described sedimentator entrance, described sedimentator outlet is divided into two branch roads, one branch road is connected with described second soda-wash tower entrance, another branch road is connected with described residual liquid tank entrance, described second soda-wash tower outlet is connected with products pot entrance.
2., according to claim 1 for the de-ester apparatus that octane-iso is produced, it is characterized in that, described strainer, pickling tower, the first soda-wash tower, interchanger, water wash column, sedimentator are connected DCS Controlling System with the second soda-wash tower.
3., according to claim 1 for the de-ester apparatus that octane-iso is produced, it is characterized in that, at the bottom of the tower top of described water wash column and tower, acidity test instrument is set.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520692615.5U CN205046017U (en) | 2015-09-08 | 2015-09-08 | A take off ester device for isooctane production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520692615.5U CN205046017U (en) | 2015-09-08 | 2015-09-08 | A take off ester device for isooctane production |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205046017U true CN205046017U (en) | 2016-02-24 |
Family
ID=55339615
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520692615.5U Expired - Fee Related CN205046017U (en) | 2015-09-08 | 2015-09-08 | A take off ester device for isooctane production |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205046017U (en) |
-
2015
- 2015-09-08 CN CN201520692615.5U patent/CN205046017U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160224 Termination date: 20210908 |