CN205027590U - Concentrated appearance of concentrated volume of accurate control - Google Patents
Concentrated appearance of concentrated volume of accurate control Download PDFInfo
- Publication number
- CN205027590U CN205027590U CN201520705995.1U CN201520705995U CN205027590U CN 205027590 U CN205027590 U CN 205027590U CN 201520705995 U CN201520705995 U CN 201520705995U CN 205027590 U CN205027590 U CN 205027590U
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- China
- Prior art keywords
- liquid level
- sample tube
- photoelectric sensor
- terminal liquid
- concentrated
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- Expired - Fee Related
Links
- 239000007788 liquid Substances 0.000 claims abstract description 30
- NJPPVKZQTLUDBO-UHFFFAOYSA-N novaluron Chemical compound C1=C(Cl)C(OC(F)(F)C(OC(F)(F)F)F)=CC=C1NC(=O)NC(=O)C1=C(F)C=CC=C1F NJPPVKZQTLUDBO-UHFFFAOYSA-N 0.000 claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 230000002459 sustained effect Effects 0.000 claims description 3
- 238000000034 method Methods 0.000 abstract description 2
- 238000013480 data collection Methods 0.000 abstract 3
- 239000000523 sample Substances 0.000 description 32
- 239000012141 concentrate Substances 0.000 description 8
- 230000003287 optical effect Effects 0.000 description 6
- 230000005622 photoelectricity Effects 0.000 description 2
- 239000012488 sample solution Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
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- Sampling And Sample Adjustment (AREA)
Abstract
The utility model discloses a concentrated appearance of concentrated volume of accurate control, include: photoelectric sensor, data collection card and acquisition controller. The photoelectric sensor level sets up on the pedestal, the sample test tube is provided with terminal point liquid level line, photoelectric sensor's light emission mouth and terminal point liquid level line are located same height, data collection card passes through logic circuit and is connected with photoelectric sensor, acquisition controller and data collection card electric connection, acquisition controller communicates with airflow generator's operating circuit. This concentration appearance can detect concentrating sample's terminal point liquid level accurately to the automatic shutdown concentration process.
Description
Technical field
The utility model relates to experimental apparatus technical field, and particularly a kind of accurate control concentrates the concentrating instrument of volume.
Background technology
Concentrating instrument is mainly used in the concentrated of the extract sample containing organic solvent, concentrated principle is after the steam volatilized in extract sample hose rises to condenser pipe, meet condensation and form drop, discharge after the tube wall landing of condenser pipe, extract sample constantly evaporates until reach setting volume.
The pick-up unit that concentrating instrument of the prior art uses accurately can not detect the liquid level of concentrating sample, causes the target volume error of final concentrating sample larger.
Utility model content
For solving the problem, the utility model provides a kind of terminal liquid level that concentrating sample accurately can be detected, and automatically stops the accurate control of concentration process to concentrate the concentrating instrument of volume.
A kind of accurate control that the utility model provides concentrates the concentrating instrument of volume, comprising: pedestal, flow generator, jacket condensator, water bath and sample tube; Described water bath is fixed in described pedestal; Described sample tube is placed in described water bath; Described jacket condensator is fixed on the top of described sample tube; Described flow generator is fixed on the top of described jacket condensator, and described concentrating instrument comprises:
Photoelectric sensor, is horizontally set on described pedestal; Described sample tube is provided with terminal liquid level line; Light emission mouth and the described terminal liquid level line of described photoelectric sensor are positioned at sustained height;
Data collecting card, is connected with described photoelectric sensor by logical circuit;
Acquisition controller, is electrically connected with described data collecting card; Described acquisition controller is communicated with the operating circuit of described flow generator.
As preferably, described sample tube is the cylindrical tube of bottom undergauge; Described terminal liquid level line is arranged on the bottom of described sample tube.
As preferably, described concentrating instrument comprises two photoelectric sensors; Described sample tube is provided with two described terminal liquid level lines;
Light emission mouth corresponding described two terminal liquid level lines respectively of described two photoelectric sensors.
As preferably, the volume of the described sample tube that described two terminal liquid level lines are corresponding is respectively 0.5ml and 1ml.
A kind of accurate control that the utility model provides concentrates the concentrating instrument of volume by arranging photoelectric sensor, simultaneously by the light emission mouth of photoelectric sensor just to the terminal liquid level line bottom sample tube, photoelectric sensor sends optical characteristics signal to data collecting card; When in sample tube, the liquid level of sample solution is in terminal liquid level line, photoelectricity herein changes, optical characteristics signal correspondence changes, after data collecting card receives the optical characteristics signal of change, shutoff signal is sent to acquisition controller, the operating circuit of flow generator is disconnected, and then stops concentrated experiment, ensure that the final concentrated volume of sample tube is accurate to setting volume.
Accompanying drawing explanation
Fig. 1 is the configuration diagram that accurate control that the utility model embodiment provides concentrates the concentrating instrument of volume.
(parts of wherein each label representative are followed successively by: 1 flow generator, 2 jacket condensators, 3 sample tubes, 4 photoelectric sensors, 5 data collecting cards, 6 acquisition controllers)
Embodiment
In order to understand the utility model in depth, below in conjunction with drawings and the specific embodiments, the utility model is described in detail.
See accompanying drawing 1, a kind of accurate control that the embodiment of the present application provides concentrates the concentrating instrument of volume, comprising: pedestal, flow generator 1, jacket condensator 2, water bath and sample tube 3; Water bath is fixed in pedestal; Sample tube 3 is placed in water bath; Jacket condensator 2 is fixed on the top of sample tube 3; Flow generator 1 is fixed on the top of jacket condensator 2, and this concentrating instrument also comprises: photoelectric sensor 4, data collecting card 5 and acquisition controller 6.Photoelectric sensor 4 is horizontally set on pedestal; Sample tube 3 is provided with terminal liquid level line; Light emission mouth and the terminal liquid level line of photoelectric sensor 4 are positioned at sustained height; Data collecting card 5 is connected with photoelectric sensor 4 by logical circuit; Acquisition controller 6 and data collecting card 5 are electrically connected; Acquisition controller 6 is communicated with the operating circuit of flow generator 1.
Further, sample tube 3 is the cylindrical tube of bottom undergauge, and namely sample tube 3 is made up of large diameter pipe and narrow tube, and narrow tube is equivalent to collector tube, and after having concentrated, concentrating sample is collected in collector tube; Terminal liquid level line is arranged on the bottom of sample tube 3, and namely terminal liquid level line is arranged on collector tube.
Further, concentrating instrument comprises two photoelectric sensors 4; Sample tube 3 is provided with two terminal liquid level lines; Light emission mouth corresponding two terminal liquid level lines respectively of two color sensors 4.As a kind of preferred embodiment, the volume of the sample tube 3 that two terminal liquid level lines are corresponding is respectively 0.5ml and 1ml.Like this, according to different experiments needs, different sample can be concentrated to different volumes respectively.
A kind of accurate control that the utility model provides concentrates the concentrating instrument of volume by arranging photoelectric sensor 4, simultaneously by the light emission mouth of photoelectric sensor 4 just to the terminal liquid level line bottom sample tube 3, photoelectric sensor 4 sends optical characteristics signal to data collecting card 5; When in sample tube 3, the liquid level of sample solution is in terminal liquid level line, photoelectricity herein changes, optical characteristics signal correspondence changes, after data collecting card 5 receives the optical characteristics signal of change, shutoff signal is sent to acquisition controller 6, the operating circuit of flow generator 1 is disconnected, and then stops concentrated experiment, ensure that the final concentrated volume of sample tube 3 is accurate to setting volume.
Above-described embodiment; the purpose of this utility model, technical scheme and beneficial effect are further described; be understood that; the foregoing is only embodiment of the present utility model; be not limited to the utility model; all within spirit of the present utility model and principle, any amendment made, equivalent replacement, improvement etc., all should be included within protection domain of the present utility model.
Claims (4)
1. accurately control a concentrating instrument for concentrated volume, comprising: pedestal, flow generator, jacket condensator, water bath and sample tube; Described water bath is fixed in described pedestal; Described sample tube is placed in described water bath; Described jacket condensator is fixed on the top of described sample tube; Described flow generator is fixed on the top of described jacket condensator, it is characterized in that, described concentrating instrument comprises:
Photoelectric sensor, is horizontally set on described pedestal; Described sample tube is provided with terminal liquid level line; Light emission mouth and the described terminal liquid level line of described photoelectric sensor are positioned at sustained height;
Data collecting card, is connected with described photoelectric sensor by logical circuit;
Acquisition controller, is electrically connected with described data collecting card; Described acquisition controller is communicated with the operating circuit of described flow generator.
2. concentrating instrument as claimed in claim 1, is characterized in that,
Described sample tube is the cylindrical tube of bottom undergauge; Described terminal liquid level line is arranged on the bottom of described sample tube.
3. concentrating instrument as claimed in claim 1, is characterized in that,
Described concentrating instrument comprises two photoelectric sensors; Described sample tube is provided with two described terminal liquid level lines;
Light emission mouth corresponding described two terminal liquid level lines respectively of described two photoelectric sensors.
4. concentrating instrument as claimed in claim 3, is characterized in that,
The volume of the described sample tube that described two terminal liquid level lines are corresponding is respectively 0.5ml and 1ml.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201520705995.1U CN205027590U (en) | 2015-09-14 | 2015-09-14 | Concentrated appearance of concentrated volume of accurate control |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN201520705995.1U CN205027590U (en) | 2015-09-14 | 2015-09-14 | Concentrated appearance of concentrated volume of accurate control |
Publications (1)
Publication Number | Publication Date |
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CN205027590U true CN205027590U (en) | 2016-02-10 |
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Family Applications (1)
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CN201520705995.1U Expired - Fee Related CN205027590U (en) | 2015-09-14 | 2015-09-14 | Concentrated appearance of concentrated volume of accurate control |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109269872A (en) * | 2018-10-24 | 2019-01-25 | 南宁市第二人民医院 | Plasma lipid sample automatic concentration instrument |
CN111803978A (en) * | 2020-09-01 | 2020-10-23 | 赛默飞世尔(上海)仪器有限公司 | Solvent evaporation device and solvent evaporation system |
CN112666127A (en) * | 2020-12-29 | 2021-04-16 | 湖南金泰环保科技有限公司 | Method for rapidly judging sample concentration end point and parallel concentrator |
-
2015
- 2015-09-14 CN CN201520705995.1U patent/CN205027590U/en not_active Expired - Fee Related
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109269872A (en) * | 2018-10-24 | 2019-01-25 | 南宁市第二人民医院 | Plasma lipid sample automatic concentration instrument |
CN111803978A (en) * | 2020-09-01 | 2020-10-23 | 赛默飞世尔(上海)仪器有限公司 | Solvent evaporation device and solvent evaporation system |
CN112666127A (en) * | 2020-12-29 | 2021-04-16 | 湖南金泰环保科技有限公司 | Method for rapidly judging sample concentration end point and parallel concentrator |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CB03 | Change of inventor or designer information |
Inventor after: Li Fei Inventor after: Wang Jun Inventor after: Dai Shanwei Inventor after: Zhu Jingjing Inventor before: Chu Tao Inventor before: Wang Jun Inventor before: Dai Shanwei Inventor before: Zhu Jingjing |
|
CB03 | Change of inventor or designer information | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160210 |