CN204911727U - Device combination of high solid content graphite alkene thick liquids of reply high viscosity dispersion - Google Patents

Device combination of high solid content graphite alkene thick liquids of reply high viscosity dispersion Download PDF

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Publication number
CN204911727U
CN204911727U CN201520623513.8U CN201520623513U CN204911727U CN 204911727 U CN204911727 U CN 204911727U CN 201520623513 U CN201520623513 U CN 201520623513U CN 204911727 U CN204911727 U CN 204911727U
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China
Prior art keywords
dispersion
high viscosity
solid content
ball mill
pipeline
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Expired - Fee Related
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CN201520623513.8U
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Chinese (zh)
Inventor
顾灵锋
沈宇栋
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Wuxi Dongheng New Energy Technology Co Ltd
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Wuxi Dongheng New Energy Technology Co Ltd
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Priority to CN201520623513.8U priority Critical patent/CN204911727U/en
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Expired - Fee Related legal-status Critical Current
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Abstract

The utility model provides a device combination of high solid content graphite alkene thick liquids of reply high viscosity dispersion, including ball mill, first transfer cauldron, sand mill and second transfer cauldron, the discharge gate of ball mill is through first pipe connection the feed inlet of first transfer cauldron, the discharge gate of first transfer cauldron passes through the second pipe connection the feed inlet of sand mill, the discharge gate of sand mill pass through the third pipeline with the feed inlet of second transfer cauldron is connected, the discharge gate of second transfer cauldron passes through the fourth pipe connection the feed inlet of ball mill. Device combination of high solid content graphite alkene thick liquids of reply high viscosity dispersion, equipment is succinct, easy operation is safe high -efficient.

Description

A kind of equipment combination tackling the dispersion of high viscosity high solids content Graphene slurry
Technical field
The utility model belongs to Graphene production field, is specifically related to a kind of equipment combination tackling the dispersion of high viscosity high solids content Graphene slurry.
Background technology
When the equipment of existing reply high viscosity high solids content Graphene slurry dispersion is combined in and prepares Graphene slurry, graphene powder is dropped in solvent, because graphene powder specific area is large, absorbency is strong, Graphene slurry is made substantially not possess mobility, conventional stirring and high speed shear mode are difficult to be mixed, and cause slurry solid content not possess uniformity.In order to ensure that Graphene slurry is uniformly dispersed, generally can only reduce slurry solid content and ensureing its mobility, considerably increase solvent cost and the energy consumption for drying of user like this.And the dispersion efficiency of conventional high speed shear mode is low, dispersion effect is bad.Have following shortcoming: 1. pickling graphene oxide 1. height is larger than table graphene powder dispersion difficulty, convention stir, high speed shear mode cannot drop into after in solvent at graphene powder effectively disperses mixing, and slurry is uneven.2. solid content cannot be done height by high ratio table Graphene slurry.3. Graphene slurry dispersion efficiency is low.
Utility model content
The technical problems to be solved in the utility model is to provide a kind of equipment combination tackling the dispersion of high viscosity high solids content Graphene slurry, overcomes above-mentioned defect, workout cost is high, slurry is uneven, solid content is low, the problem that dispersion efficiency is high.
For solving the problems of the technologies described above, the utility model provides a kind of equipment combination tackling the dispersion of high viscosity high solids content Graphene slurry, comprise ball mill, first transfer still, sand mill and the second transfer still, the discharging opening of described ball mill connects the charging aperture of described first transfer still by the first pipeline, the discharging opening of described first transfer still connects the charging aperture of described sand mill by second pipe, the discharging opening of described sand mill is connected with the charging aperture of described second transfer still by the 3rd pipeline, the discharging opening of described second transfer still connects the charging aperture of described ball mill by the 4th pipeline.
As a kind of a kind of preferred version of tackling the equipment combination of high viscosity high solids content Graphene slurry dispersion described in the utility model, described ball mill is provided with dog-house.
As a kind of a kind of preferred version of tackling the equipment combination of high viscosity high solids content Graphene slurry dispersion described in the utility model, in described first pipeline, second pipe and the 4th pipeline, be equipped with membrane pump.
Compared with prior art, a kind of equipment combination tackling the dispersion of high viscosity high solids content Graphene slurry that the utility model proposes, this method adopts ball milling method to carry out pre-dispersed, can be even by graphene powder and solvent, dispersant, slurry is made to disperse completely by the mode of sand milling again, the slurry solid content obtained and viscosity are consistent, and efficiency is very high, more can prepare the higher Graphene slurry products of solid content by the mode of batch charging.Concrete advantage is as follows: 1, by the mode of ball milling, and after can effectively being dropped into by graphene powder in solvent, high viscosity mixture carries out dispersion and mixes, and can tentatively disperse; 2, graphene powder is due to its high-specific area nano material behavior, and its apparent volume is often greater than required cooperation solvent volume, can be improved the solid content of Graphene slurry by the mode of batch charging; 3, the dispersing mode more general high speed shear mode that combines of ball milling and sand milling is more efficient, energy consumption is lower.
Accompanying drawing explanation
In order to be illustrated more clearly in the technical scheme of the utility model embodiment, below the accompanying drawing used required in describing embodiment is briefly described, apparently, accompanying drawing in the following describes is only embodiments more of the present utility model, for those of ordinary skill in the art, under the prerequisite not paying creative work, other accompanying drawing can also be obtained according to these accompanying drawings.Wherein,
Fig. 1 is a kind of structural representation of tackling the equipment combination of high viscosity high solids content Graphene slurry dispersion of the present utility model.
Wherein: 1 for ball mill, 2 be the first transfer still, 3 for sand mill, 4 be that the second transfer still, 5 is for membrane pump.
Detailed description of the invention
A kind of equipment combination tackling the dispersion of high viscosity high solids content Graphene slurry described in the utility model, it comprises: ball mill 1, first transfer still 2, sand mill 3 and the second transfer still 4.
For enabling above-mentioned purpose of the present utility model, feature and advantage become apparent more, are described in further detail the utility model below in conjunction with detailed description of the invention.
First, alleged herein " embodiment " or " embodiment " refers to special characteristic, structure or the characteristic that can be contained at least one implementation of the utility model.Different local in this manual " in one embodiment " occurred not all refers to same embodiment, neither be independent or optionally mutually exclusive with other embodiments embodiment.
Secondly; the utility model utilizes structural representation etc. to be described in detail; when describing the utility model embodiment in detail; for ease of explanation; represent that the schematic diagram of the equipment combination structure of reply high viscosity high solids content Graphene slurry dispersion can be disobeyed general ratio and be made partial enlargement; and described schematic diagram is example, it should not limit the scope of the utility model protection at this.In addition, the three dimensions of length, width and the degree of depth should be comprised in actual fabrication.
Embodiment one
Refer to Fig. 1, Fig. 1 is a kind of structural representation of tackling the equipment combination of high viscosity high solids content Graphene slurry dispersion of the present utility model.As shown in Figure 1, the equipment combination of reply high viscosity high solids content Graphene slurry dispersion, comprises ball mill 1, first transfer still 2, sand mill 3 and the second transfer still 4.
The discharging opening of described ball mill 1 connects the charging aperture of described first transfer still 2 by the first pipeline (not shown), the discharging opening of described first transfer still 2 connects the charging aperture of described sand mill 3 by second pipe (not shown), the discharging opening of described sand mill 3 is connected with the charging aperture of described second transfer still 4 by the 3rd pipeline (not shown), and the discharging opening of described second transfer still 4 connects the charging aperture of described ball mill 1 by the 4th pipeline (not shown).
Conveniently feed intake, described ball mill 1 is provided with dog-house (not shown).
Membrane pump 5 is equipped with in described first pipeline, second pipe and the 4th pipeline.
The use procedure of above-mentioned process units is as follows:
1: common production: ball mill 1 top is provided with dog-house, first drops into solvent and dispersant by dog-house, first ball milling dispersion dispersion liquid, then drop into graphene powder by dog-house, ball milling disperses a period of time, is mixed by mixture; By membrane pump 5 on ball mill 1, material is evacuated in the first transfer still 2, by membrane pump 5 on sand mill 3 material in first transfer still 2 is evacuated in sand mill 3 and carries out sand milling, material after slurry sand milling is beaten in the second transfer still 4, period controls sand mill 3 rotating speed and material flow (pump speed) controls jitter time, is equipped with membrane pump 5 is packed by material after having disperseed by the second transfer still 3.
2: high solids content Graphene slurry disperses: adopt graphene powder fed batch mode, first drop into certain proportion graphene powder, equipment operation mode is by above-mentioned common production, be equipped with membrane pump 5 by the second transfer still 4 and material is squeezed into ball mill 1, again add certain graphene powder to disperse by the above-mentioned common mode of production, being so circulated to point sheds needs solid content ratio Graphene slurry.
What the those of ordinary skill in affiliated field should be understood that is, one of feature of the present utility model or object are: the equipment combination of reply high viscosity high solids content Graphene slurry dispersion described in the utility model, by the mode of ball milling, after can effectively being dropped into by graphene powder in solvent, high viscosity mixture carries out dispersion and mixes, and can tentatively disperse.Its concrete advantage is:
1: graphene powder is due to its high-specific area nano material behavior, and its apparent volume is often greater than required cooperation solvent volume, can be improved the solid content of Graphene slurry by the mode of batch charging.
2: the dispersing mode more general high speed shear mode that ball milling and sand milling combine is more efficient, energy consumption is lower.
It should be noted that, above embodiment is only in order to illustrate the technical solution of the utility model and unrestricted, although be described in detail the utility model with reference to preferred embodiment, those of ordinary skill in the art is to be understood that, can modify to the technical solution of the utility model or equivalent replacement, and not departing from the spirit and scope of technical solutions of the utility model, it all should be encompassed in the middle of right of the present utility model.

Claims (3)

1. tackle the equipment combination of high viscosity high solids content Graphene slurry dispersion for one kind, it is characterized in that: comprise ball mill, the first transfer still, sand mill and the second transfer still,
The discharging opening of described ball mill connects the charging aperture of described first transfer still by the first pipeline, the discharging opening of described first transfer still connects the charging aperture of described sand mill by second pipe, the discharging opening of described sand mill is connected with the charging aperture of described second transfer still by the 3rd pipeline, and the discharging opening of described second transfer still connects the charging aperture of described ball mill by the 4th pipeline.
2. the equipment combination of reply high viscosity high solids content Graphene slurry as claimed in claim 1 dispersion, is characterized in that: described ball mill is provided with dog-house.
3. the equipment combination of reply high viscosity high solids content Graphene slurry as claimed in claim 1 dispersion, is characterized in that: be equipped with membrane pump in described first pipeline, second pipe and the 4th pipeline.
CN201520623513.8U 2015-08-18 2015-08-18 Device combination of high solid content graphite alkene thick liquids of reply high viscosity dispersion Expired - Fee Related CN204911727U (en)

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Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106179688A (en) * 2016-08-31 2016-12-07 无锡东恒新能源科技有限公司 A kind of slurry production line with real-time traffic control function
CN106179072A (en) * 2016-08-31 2016-12-07 无锡东恒新能源科技有限公司 A kind of high solids content slurry disperse system
CN106179073A (en) * 2016-08-31 2016-12-07 无锡东恒新能源科技有限公司 A kind of slurry disperse system
CN106179094A (en) * 2016-08-31 2016-12-07 无锡东恒新能源科技有限公司 The dispersed system of a kind of slurry automatization
CN106179074A (en) * 2016-08-31 2016-12-07 无锡东恒新能源科技有限公司 A kind of slurry integration disperse system
CN106179057A (en) * 2016-08-31 2016-12-07 无锡东恒新能源科技有限公司 A kind of high viscosity carbon nano tube paste stirred tank
CN106237910A (en) * 2016-08-31 2016-12-21 无锡东恒新能源科技有限公司 A kind of slurry Powerful dispersing device
CN106237907A (en) * 2016-08-31 2016-12-21 无锡东恒新能源科技有限公司 A kind of hot type high viscosity carbon nano tube paste premix stirring device
CN106379892A (en) * 2016-08-31 2017-02-08 无锡东恒新能源科技有限公司 Slurry production line system
CN106390816A (en) * 2016-08-31 2017-02-15 无锡东恒新能源科技有限公司 Pre-mixing device-based high-viscosity carbon nanotube slurry preparation system
CN113145283A (en) * 2021-02-23 2021-07-23 邯郸钢铁集团有限责任公司 Laboratory equipment and method for preparing graphene by using tar residues

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106179688A (en) * 2016-08-31 2016-12-07 无锡东恒新能源科技有限公司 A kind of slurry production line with real-time traffic control function
CN106179072A (en) * 2016-08-31 2016-12-07 无锡东恒新能源科技有限公司 A kind of high solids content slurry disperse system
CN106179073A (en) * 2016-08-31 2016-12-07 无锡东恒新能源科技有限公司 A kind of slurry disperse system
CN106179094A (en) * 2016-08-31 2016-12-07 无锡东恒新能源科技有限公司 The dispersed system of a kind of slurry automatization
CN106179074A (en) * 2016-08-31 2016-12-07 无锡东恒新能源科技有限公司 A kind of slurry integration disperse system
CN106179057A (en) * 2016-08-31 2016-12-07 无锡东恒新能源科技有限公司 A kind of high viscosity carbon nano tube paste stirred tank
CN106237910A (en) * 2016-08-31 2016-12-21 无锡东恒新能源科技有限公司 A kind of slurry Powerful dispersing device
CN106237907A (en) * 2016-08-31 2016-12-21 无锡东恒新能源科技有限公司 A kind of hot type high viscosity carbon nano tube paste premix stirring device
CN106379892A (en) * 2016-08-31 2017-02-08 无锡东恒新能源科技有限公司 Slurry production line system
CN106390816A (en) * 2016-08-31 2017-02-15 无锡东恒新能源科技有限公司 Pre-mixing device-based high-viscosity carbon nanotube slurry preparation system
CN113145283A (en) * 2021-02-23 2021-07-23 邯郸钢铁集团有限责任公司 Laboratory equipment and method for preparing graphene by using tar residues

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20151230

Termination date: 20180818

CF01 Termination of patent right due to non-payment of annual fee