CN204911512U - Preparation granule footpath reation kettle for anatase type nanometer titanium dioxide - Google Patents
Preparation granule footpath reation kettle for anatase type nanometer titanium dioxide Download PDFInfo
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- CN204911512U CN204911512U CN201520708498.7U CN201520708498U CN204911512U CN 204911512 U CN204911512 U CN 204911512U CN 201520708498 U CN201520708498 U CN 201520708498U CN 204911512 U CN204911512 U CN 204911512U
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- shaft
- signal transmission
- transmission port
- tank body
- titanium dioxide
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Abstract
(B, ) the utility model belongs to a chemical reaction device field especially relates to a preparation granule footpath reation kettle for anatase type nanometer titanium dioxide, including the cauldron jar body (b) (b) 1 (b) (b), agitator motor (b) (b) 2 (b) (b), (mixing) shaft (b) (b) 3 (b) (b), stirring rake (b) (b) 4 (b) (b) and temperature control components, agitator motor (b) (b) 2 (b) (b) fixes at the cauldron jar body (b) (b) 1 (b) (b) top, agitator motor's (b) (b) 2 (b) (b) output shaft meets with the upper end of (mixing) shaft (b) (b) 3 (b) (b) is fixed, the lower tip of (mixing) shaft (b) (b) 3 (b) (b) meets with stirring rake (b) (b) 4 (b) (b) is fixed, temperature sensor (b) (b) 5 (b) (b) and heater (b) (b) 6 (b) (b) are arranged in the cauldron jar body (b) (b) 1 (b) (b), temp. Control module (b) (b) 7 (b) (b) arranges the cauldron jar body (b) (b) 1 (b) (b) top in, the signal transmission port of temperature sensor (b) (b) 5 (b) (b) and heater (b) (b) 6 (b) (b) meets temp. Control module (b) (b) 7 (b) (b's) signal transmission port respectively. The utility model discloses simple structure, stir efficient, effectively controlled reaction temperature and time. (B, )
Description
Technical field
The utility model belongs to chemical reaction equipment field, particularly relates to one and prepares small particle diameter anatase-type nanometer titanium dioxide reactor.
Background technology
Reactor is combined reaction container, according to reaction condition to reactor structure function and the design configuring annex.Reactor can be widely used in oil, chemical industry, rubber, agricultural chemicals, dyestuff, medicine, food, be used for the pressure vessel of the technical process such as sulfuration, nitrated, hydrogenation, hydrocarbonylation, polymerization, condensation, such as reactor, reaction pot, decomposition pot, polymeric kettle etc.; Material generally has carbon manganese steel, stainless steel, zirconium, Ni-based (Kazakhstan, Monel, inconel) alloy and other composite.Existing reactor is due to the defect in structural design, and it is low that ubiquity stirring efficiency, and reaction temperature and time lack the problems such as effectively control.In view of this, existing reactor is difficult to the requirement being suitable for small particle diameter anatase-type nanometer titanium dioxide preparation technology.
Utility model content
The utility model is intended to overcome the deficiencies in the prior art part and provides a kind of structure simple, and stirring efficiency is high, effectively can control the preparation small particle diameter anatase-type nanometer titanium dioxide reactor of reaction temperature and time.
For solving the problems of the technologies described above, the utility model realizes like this.
Preparation small particle diameter anatase-type nanometer titanium dioxide reactor, it comprises still tank body, stirring motor, shaft, paddle and temperature control assembly; Described stirring motor is fixed on still tank body top; The output shaft of described stirring motor and the upper end of shaft are fixedly connected; Bottom and the paddle of described shaft are fixedly connected; Seal member is provided with in the junction of described shaft and still tank body; Described temperature control assembly comprises temperature sensor, heater and temperature control module; Described temperature sensor and heater are placed in still tank body; Described temperature control module is placed in still tank body top; The signal transmission port of described temperature sensor and heater connects the signal transmission port of temperature control module respectively.
As a kind of preferred version, shaft central region described in the utility model is provided with the first auxiliary agitation blade; The second auxiliary agitation blade is provided with between described first auxiliary agitation blade and paddle.
Further, temperature control module described in the utility model comprises power circuit, cpu control circuit, display circuit, control output circuit and timing circuit; The signal transmission port of described cpu control circuit connects display circuit respectively and controls the signal transmission port of output circuit; The signal transmission port of described timing circuit connects the signal transmission port controlling output circuit.
Further, the utility model can be provided with overcoat at the inwall of described still tank body.
The utility model makes the overall stirring efficiency of reactor be improved by the Combination Design of stirring vane and paddle, in addition, the utility model effectively can control reaction temperature and the reaction time of small particle diameter anatase-type nanometer titanium dioxide preparation technology by the design of temperature control assembly.
Accompanying drawing explanation
Below in conjunction with the drawings and specific embodiments, the utility model is described in further detail.Protection domain of the present utility model is not only confined to the statement of following content.
Fig. 1 is overall structure schematic diagram of the present utility model.
Fig. 2 is the utility model temprature control unit schematic block circuit diagram.
In figure: 1, still tank body; 2, stirring motor; 3, shaft; 4, paddle; 5, temperature sensor; 6, heater; 7, temperature control module; 8, the first auxiliary agitation blade; 9, the second auxiliary agitation blade; 10, overcoat.
Detailed description of the invention
As shown in the figure, preparation small particle diameter anatase-type nanometer titanium dioxide reactor, comprises still tank body 1, stirring motor 2, shaft 3, paddle 4 and temperature control assembly; Described stirring motor 2 is fixed on still tank body 1 top; The output shaft of described stirring motor 2 and the upper end of shaft 3 are fixedly connected; Bottom and the paddle 4 of described shaft 3 are fixedly connected; Seal member 11 is provided with the junction of still tank body 1 at described shaft 3; Described temperature control assembly comprises temperature sensor 5, heater 6 and temperature control module 7; Described temperature sensor 5 and heater 6 are placed in still tank body 1; Described temperature control module 7 is placed in still tank body 1 top; The signal transmission port of described temperature sensor 5 and heater 6 connects the signal transmission port of temperature control module 7 respectively.
For strengthening mixing effect, shaft 3 central region described in the utility model is provided with the first auxiliary agitation blade 8; The second auxiliary agitation blade 9 is provided with between described first auxiliary agitation blade 8 and paddle 4.
Temperature control module 7 described in the utility model comprises power circuit, cpu control circuit, display circuit, control output circuit and timing circuit; The signal transmission port of described cpu control circuit connects display circuit respectively and controls the signal transmission port of output circuit; The signal transmission port of described timing circuit connects the signal transmission port controlling output circuit.The utility model is provided with overcoat 10 at the inwall of described still tank body 1.
The utility model temperature sensor input signal enters the cpu control circuit in temperature control module.Data after process are input to display circuit and control output circuit and carry out showing and exports control power circuit for cpu control circuit and provide power supply by cpu control circuit; Timing circuit provides time data for controlling output circuit.The temperature signal in still tank body is gathered by temperature sensor.Temperature signal converts the signal of telecommunication to, is input in cpu control circuit and carries out data processing, and shows the temperature in current still tank body by display circuit.Power circuit provides power supply for whole temperature control system.Reaction time in timing circuit real-time judge still tank body, when system arrive set by time time, system stop heating.When system does not reach the reaction time of setting, system will continue the reaction temperature judging setting.
The utility model, when concrete operations, adopts ethanol as the solvent of butyl titanate or titanium tetrachloride, adds aliphatic acid and distilled water, be uniformly mixed, be transferred in the utility model reactor, heating.
The foregoing is only preferred embodiment of the present utility model, be not limited to the utility model, for a person skilled in the art, the utility model can have various modifications and variations.All within spirit of the present utility model and principle, any amendment done, equivalent replacement, improvement etc., all should be included within protection domain of the present utility model.
Claims (4)
1. prepare small particle diameter anatase-type nanometer titanium dioxide reactor, it is characterized in that, comprise still tank body (1), stirring motor (2), shaft (3), paddle (4) and temperature control assembly; Described stirring motor (2) is fixed on still tank body (1) top; The output shaft of described stirring motor (2) and the upper end of shaft (3) are fixedly connected; Bottom and the paddle (4) of described shaft (3) are fixedly connected; Seal member (11) is provided with at described shaft (3) and the junction of still tank body (1); Described temperature control assembly comprises temperature sensor (5), heater (6) and temperature control module (7); Described temperature sensor (5) and heater (6) are placed in still tank body (1); Described temperature control module (7) is placed in still tank body (1) top; The signal transmission port of described temperature sensor (5) and heater (6) connects the signal transmission port of temperature control module (7) respectively.
2. preparation small particle diameter anatase-type nanometer titanium dioxide reactor according to claim 1, is characterized in that: described shaft (3) central region is provided with the first auxiliary agitation blade (8); The second auxiliary agitation blade (9) is provided with between described first auxiliary agitation blade (8) and paddle (4).
3. preparation small particle diameter anatase-type nanometer titanium dioxide reactor according to claim 2, is characterized in that: described temperature control module (7) comprises power circuit, cpu control circuit, display circuit, control output circuit and timing circuit; The signal transmission port of described cpu control circuit connects display circuit respectively and controls the signal transmission port of output circuit; The signal transmission port of described timing circuit connects the signal transmission port controlling output circuit.
4. preparation small particle diameter anatase-type nanometer titanium dioxide reactor according to claim 3, is characterized in that: be provided with overcoat (10) at the inwall of described still tank body (1).
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201520708498.7U CN204911512U (en) | 2015-09-15 | 2015-09-15 | Preparation granule footpath reation kettle for anatase type nanometer titanium dioxide |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN201520708498.7U CN204911512U (en) | 2015-09-15 | 2015-09-15 | Preparation granule footpath reation kettle for anatase type nanometer titanium dioxide |
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CN204911512U true CN204911512U (en) | 2015-12-30 |
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CN201520708498.7U Expired - Fee Related CN204911512U (en) | 2015-09-15 | 2015-09-15 | Preparation granule footpath reation kettle for anatase type nanometer titanium dioxide |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107824142A (en) * | 2017-11-21 | 2018-03-23 | 佛山汇众森泰科技有限公司 | A kind of environment protecting and power-saving refining equipment |
-
2015
- 2015-09-15 CN CN201520708498.7U patent/CN204911512U/en not_active Expired - Fee Related
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107824142A (en) * | 2017-11-21 | 2018-03-23 | 佛山汇众森泰科技有限公司 | A kind of environment protecting and power-saving refining equipment |
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Legal Events
Date | Code | Title | Description |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20151230 Termination date: 20160915 |
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CF01 | Termination of patent right due to non-payment of annual fee |