CN204911505U - Secondary divides material type reactor - Google Patents
Secondary divides material type reactor Download PDFInfo
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- CN204911505U CN204911505U CN201520676749.8U CN201520676749U CN204911505U CN 204911505 U CN204911505 U CN 204911505U CN 201520676749 U CN201520676749 U CN 201520676749U CN 204911505 U CN204911505 U CN 204911505U
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- kettle
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- type reactor
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Abstract
The utility model discloses a secondary divides material type reactor, including the cauldron body, the internal (mixing) shaft that is equipped with of cauldron, being provided with a top in the nearly charge door department in the internal upper end of jar and having the open -ended and get rid of the feed cylinder, the opening that gets rid of the feed cylinder is corresponding with the charge door, gets rid of a plurality of round holes that are equipped with evenly distributed on the lateral wall of feed cylinder, get rid of the center fixed connection (mixing) shaft of feed cylinder bottom, the cauldron body comprises endotheca and outer wall, is located to be provided with insulation material between endotheca and the outer wall of cauldron body lower extreme, is located the coil pipe that is provided with the screw thread distribution between endotheca and the outer wall of insulation material top, be provided with control panel, thermoscope and liquid level ware on the external lateral wall of cauldron, physically install the discharger in the bottom at the cauldron, the utility model discloses broken handle is carried out to the material that condenses to the operation that can distribute when the material gets into cauldron body bottom of discharger that work set up in reation kettle bottom, improves the spray deposition uniformity of material.
Description
Technical field
The utility model relates to field of fine chemical, is specially a kind of secondary sub-material type reactor.
Background technology
The production of bromide fire retardant and the use history of existing more than 30 year, the bromide fire retardant produced at present about has kind more than 70.Because the agent of bromine fire-retardant is flame retardant area traditional category, significantly and historical background and performance and price advantage, domestic and international scientific research personnel is still full of enthusiasm to the new product development of bromide fire retardant in status.
The heat resistance of three (tribromophenoxy) triazine, light resistance and not easily leaching, do not move, use can be reclaimed on the features such as material property impact is little and fire-retardant plastics thereof, this is the feature not available for numerous bromide fire retardant.The mechanism of action that it also utilizes bromine-nitrogen different simultaneously, complements each other, reaches the result of Synergistic.Three (tribromophenoxy) triazine, with its excellent performance and characteristic, at home and abroad fire retardant market all has broad prospects.
Since coming out from three (tribromophenoxy) triazine, although people update its synthesis technique, but still there is following problem in existing synthesis technique: adopt strong alkaline substance as KOH NaOH etc. be raw material, not only can corrode production equipment, and the side reaction of tribromphenol self etherificate can be caused; Carry out having in water reaction system, cause the hydrolysis of a part of Cyanuric Chloride, there is the bottleneck of conversion ratio and product purity.
In the production process of three (tribromophenoxy) triazine auxiliary material in early stage, the hybrid reaction of some material will complete within the extremely short time, this just requires the material that mixed once is less, or use high-power reactor to mix rapidly, even if also have mixing to be difficult to uniform phenomenon like this, affect product quality and production effect, functional reliability is low, the inefficiency of reactor, and raw material constantly tires out in reinforced process, easily form deposition dirt at inner wall of kettle and stir uneven situation, affecting operating efficiency and the reaction process of reactor; Existing reactor bottom discharge just exports simply by dehvery pump, and often in the condensation of autoclave body bottom material, the time one is difficult to cleaning in bottom for a long time, causes very large problem to post-processed.
Utility model content
The purpose of this utility model is to provide a kind of secondary sub-material type reactor, to solve the problem proposed in above-mentioned background technology.
For achieving the above object, the utility model provides following technical scheme:
A kind of secondary sub-material type reactor, comprises kettle, is provided with shaft in kettle; What in tank body, nearly charge door place, upper end was provided with that a top has an opening gets rid of barrel, and the opening getting rid of barrel is corresponding with charge door, and the sidewall getting rid of barrel is provided with equally distributed some circular holes; The center of getting rid of bottom barrel is fixedly connected with shaft, and shaft upper end is extended kettle outside and is connected with the stirring motor being arranged on kettle outside; Described kettle is made up of inner sleeve and outer wall, between the inner sleeve and outer wall of kettle lower end, be provided with insulation material, the inner sleeve above insulation material and be provided with between outer wall screw thread distribution coil pipe; Kettle lateral wall is provided with control panel, temperature measurer and liquid level meter; In kettle bottom, discharger is installed; Described discharger is arranged on autoclave body bottom and is connected with kettle bottom, comprise housing, be provided with dividing plate at the bosom of described housing, enclosure interior is separated into the first cavity and the second cavity by described dividing plate, the upper port of described first cavity is uncovered, and its inwall is provided with multiple points of pieces of cloth; Described second cavity is truncated cone-shaped, and inwall is provided with horizontally disposed distribution bar; Port is formed in the lower end of described housing, described port is provided with movable rotation-shaft, described movable rotation-shaft is socketed on the outer wall of discharging opening, electronic sealing up a door is provided with in described port, described dividing plate is provided with multiple distributing slot, in the middle part of dividing plate, between the port of adjacent distributions groove, be provided with conical distribution body.
As the utility model further technical scheme, the outer wall of described distribution bar is provided with outer raised line.
As the utility model further technical scheme, get rid of the bottom of barrel in the arc-shaped raised up.
As the utility model further technical scheme, four paddles are provided with in the lower end of described shaft, be dislocatedly distributed on shaft, two the first paddle direction being wherein positioned at top downwards and and distribute in 45 degree between shaft, be positioned at two the second paddle horizontal distribution of lower end and be 90 degree with shaft and distribute.
As the utility model further technical scheme, the first paddle described in two is provided with micropore.
As the utility model further technical scheme, kettle inside is stretched in temperature measurer one end, and the other end is connected with control panel, liquid level meter is positioned at kettle lower end, and kettle inside is goed deep in its one end, the other end is connected with control panel, and control panel is also connected with drive motors.
Compared with prior art, during utility model works, operating personnel can check the existing situation in reactor by control panel, and carry out corresponding reinforced process according to the needs of the data on control panel and actual production, time reinforced, employee only needs the key entry corresponding data at control panel, the flow controller (figure does not show) of the pipeline be connected with charging aperture just can make corresponding process, getting rid of barrel and effectively charging can be carried out refinement as the measure of first step uniform distributing and distribute equally on paddle, four paddles one group between two arranged in shaft lower end, interleaved is arranged, produce without dead angle when effectively ensure that stirring, improve mixing effect, the discharger arranged bottom reactor can carry out distribution work when material enters autoclave body bottom, break process is carried out to the material of condensation, improve the distributing homogeneity of material.
Accompanying drawing explanation
Fig. 1 is the structural representation of a kind of secondary sub-material of the utility model type reactor.
Fig. 2 is the structural representation of discharger in the utility model.
Detailed description of the invention
Be described in more detail below in conjunction with the technical scheme of detailed description of the invention to this patent.
Refer to Fig. 1 ~ 2, a kind of secondary sub-material type reactor, comprises kettle 1, is provided with shaft 3 in kettle 1; What in tank body, nearly charge door place, upper end was provided with that a top has an opening gets rid of barrel 10, the opening getting rid of barrel 10 is corresponding with charge door 7, the sidewall getting rid of barrel 10 is provided with equally distributed some circular holes 11, for preventing residual material in cylindrical shell 4, get rid of the bottom of barrel 10 in the arc-shaped raised up, so just can ensure that material all can throw away from the circular hole 11 got rid of barrel 10 sidewall; The center of getting rid of bottom barrel 10 is fixedly connected with shaft 3, shaft 3 upper end is extended kettle 1 outside and is connected with the stirring motor being arranged on kettle 1 outside, when material enter kettle 1 inner time first getting rid of in barrel 10 by High Rotation Speed, so just well can avoid the generation of material agglomeration, material is thrown out of from the circular hole 11 getting rid of barrel 10 sidewall simultaneously, be scattered in kettle 1, carry out next step and be uniformly mixed.
Described kettle 1 is made up of inner sleeve and outer wall, and all U-shaped structure in the top and bottom of kettle 1, between the inner sleeve and outer wall of kettle 1 lower end, be provided with insulation material, the inner sleeve above insulation material and be provided with the coil pipe 4 of screw thread distribution between outer wall; Kettle 1 lateral wall is provided with control panel 5, temperature measurer 6 and liquid level meter 9, it is inner that kettle 1 is stretched in temperature measurer 6 one end, the other end is connected with control panel 5, liquid level meter 9 is positioned at kettle 1 lower end, and kettle 1 inside is goed deep in its one end, the other end is connected with control panel 5, and control panel 5 is also connected with drive motors.
Four paddles are provided with in the lower end of described shaft 3, be dislocatedly distributed on shaft 3, wherein top two the first stirring arm 12 directions downwards and and distribute in 45 degree between shaft 3, be positioned at two the second paddle 13 horizontal distribution of lower end and be 90 degree with shaft 3 and distribute; And the first paddle 12 described in two is provided with micropore; Stirring arm is dislocatedly distributed and the setting of micropore, can improve the degrees of fusion of material during stirring greatly, solves the problem of mixing of materials difficulty further.
In kettle 1 bottom, discharger 2 is installed; Described discharger 2 to be arranged on bottom kettle 1 and to be connected with kettle 1 bottom, specifically comprise housing 21, dividing plate 22 is provided with at the bosom of described housing 21, enclosure interior is separated into the first cavity 23 and the second cavity 28 by described dividing plate 22, the upper port of described first cavity 23 is uncovered, and its inwall is provided with multiple points of pieces of cloth 26; Described second cavity 28 is truncated cone-shaped, and inwall is provided with horizontally disposed distribution bar 27; Port is formed in the lower end of described housing 21, described port is provided with movable rotation-shaft 211, described movable rotation-shaft 211 is socketed on the outer wall of discharging opening 210, be provided with in described port and electronicly seal up a door 29, described dividing plate 22 is provided with multiple distributing slot 25, in the middle part of dividing plate 22, between the port of adjacent distributions groove 25, be provided with conical distribution body 24.
The outer wall of described distribution bar 27 is provided with outer raised line, and such vibrational power flow is the efficiency in order to increase distribution dispersion, considerably increases the smoothness of discharging.
During use, operating personnel can check the existing situation in reactor by control panel, and carry out corresponding reinforced process according to the needs of the data on control panel and actual production, time reinforced, employee only needs the key entry corresponding data at control panel, the flow controller (figure does not show) of the pipeline be connected with charging aperture just can make corresponding process, and control drive motors rotation, drive stirring arm rotates, getting rid of barrel and effectively charging can be carried out refinement as the measure of first step uniform distributing and distribute equally on paddle, four paddles one group between two arranged in shaft lower end, interleaved is arranged, produce without dead angle when effectively ensure that stirring, improve mixing effect.
Above the better embodiment of this patent is explained in detail, but this patent is not limited to above-mentioned embodiment, in the ken that one skilled in the relevant art possesses, various change can also be made under the prerequisite not departing from this patent aim.
Claims (6)
1. a secondary sub-material type reactor, is characterized in that, comprise kettle, be provided with shaft in kettle; What in tank body, nearly charge door place, upper end was provided with that a top has an opening gets rid of barrel, and the opening getting rid of barrel is corresponding with charge door, and the sidewall getting rid of barrel is provided with equally distributed some circular holes; The center of getting rid of bottom barrel is fixedly connected with shaft, and shaft upper end is extended kettle outside and is connected with the stirring motor being arranged on kettle outside; Described kettle is made up of inner sleeve and outer wall, between the inner sleeve and outer wall of kettle lower end, be provided with insulation material, the inner sleeve above insulation material and be provided with between outer wall screw thread distribution coil pipe; Kettle lateral wall is provided with control panel, temperature measurer and liquid level meter; In kettle bottom, discharger is installed; Described discharger is arranged on autoclave body bottom and is connected with kettle bottom, comprise housing, be provided with dividing plate at the bosom of described housing, enclosure interior is separated into the first cavity and the second cavity by described dividing plate, the upper port of described first cavity is uncovered, and its inwall is provided with multiple points of pieces of cloth; Described second cavity is truncated cone-shaped, and inwall is provided with horizontally disposed distribution bar; Port is formed in the lower end of described housing, described port is provided with movable rotation-shaft, described movable rotation-shaft is socketed on the outer wall of discharging opening, electronic sealing up a door is provided with in described port, described dividing plate is provided with multiple distributing slot, in the middle part of dividing plate, between the port of adjacent distributions groove, be provided with conical distribution body.
2. a kind of secondary sub-material type reactor according to claim 1, it is characterized in that, the outer wall of described distribution bar is provided with outer raised line.
3. a kind of secondary sub-material type reactor according to claim 1, is characterized in that, get rid of the bottom of barrel in the arc-shaped raised up.
4. a kind of secondary sub-material type reactor according to claim 1, it is characterized in that, the lower end of described shaft is provided with four paddles, be dislocatedly distributed on shaft, two the first paddle direction being wherein positioned at top downwards and and distribute in 45 degree between shaft, be positioned at two the second paddle horizontal distribution of lower end and be 90 degree with shaft and distribute.
5. a kind of secondary sub-material type reactor according to claim 4, is characterized in that, the first paddle described in two is provided with micropore.
6. a kind of secondary sub-material type reactor according to claim 1, it is characterized in that, kettle inside is stretched in temperature measurer one end, the other end is connected with control panel, liquid level meter is positioned at kettle lower end, and kettle inside is goed deep in its one end, the other end is connected with control panel, and control panel is also connected with drive motors.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520676749.8U CN204911505U (en) | 2015-09-04 | 2015-09-04 | Secondary divides material type reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520676749.8U CN204911505U (en) | 2015-09-04 | 2015-09-04 | Secondary divides material type reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204911505U true CN204911505U (en) | 2015-12-30 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520676749.8U Expired - Fee Related CN204911505U (en) | 2015-09-04 | 2015-09-04 | Secondary divides material type reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204911505U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110756096A (en) * | 2019-11-28 | 2020-02-07 | 耒阳市旗心电子科技有限公司 | Material dispersion equipment is used in electronic product production |
| CN113304827A (en) * | 2021-05-31 | 2021-08-27 | 江西大自然制药有限公司 | Novel traditional chinese medicine is smashed device |
-
2015
- 2015-09-04 CN CN201520676749.8U patent/CN204911505U/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110756096A (en) * | 2019-11-28 | 2020-02-07 | 耒阳市旗心电子科技有限公司 | Material dispersion equipment is used in electronic product production |
| CN113304827A (en) * | 2021-05-31 | 2021-08-27 | 江西大自然制药有限公司 | Novel traditional chinese medicine is smashed device |
| CN113304827B (en) * | 2021-05-31 | 2022-09-30 | 江西大自然制药有限公司 | Novel traditional chinese medicine is smashed device |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20151230 Termination date: 20190904 |
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| CF01 | Termination of patent right due to non-payment of annual fee |