CN204911013U - Device of superfine molecular sieve of continuous separation in follow thick liquid - Google Patents

Device of superfine molecular sieve of continuous separation in follow thick liquid Download PDF

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Publication number
CN204911013U
CN204911013U CN201520701812.9U CN201520701812U CN204911013U CN 204911013 U CN204911013 U CN 204911013U CN 201520701812 U CN201520701812 U CN 201520701812U CN 204911013 U CN204911013 U CN 204911013U
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China
Prior art keywords
pipeline
subsider
tank reactor
ball valve
molecular sieves
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CN201520701812.9U
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Chinese (zh)
Inventor
王向宇
常中华
温贻强
刘猛
黄晓艳
叶晓雪
高鑫
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Zhengzhou University
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Zhengzhou University
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Abstract

The utility model relates to a superfine molecular sieve recovery unit, especially a device of superfine molecular sieve of continuous separation in follow thick liquid. The device include raw materials storage tank, tank reactor, subsider and from dynamic formula centrifugal filter, first ball valve is installed through first pipeline and first tubing pump entry intercommunication to raw materials storage tank bottom discharge mouth on the first pipeline, first tubing pump export intercommunication tank reactor middle part pan feeding mouth, the tank reactor bottom discharge mouth passes through second pipeline and second tubing pump entry intercommunication, installs the second ball valve on the second pipeline, second tubing pump export intercommunication subsider lower part pan feeding mouth, subsider bottom discharge mouth passes through the third pipeline and feeds through from dynamic formula centrifugal filter pan feeding mouth, is provided with the third ball valve on the third pipeline. The utility model discloses simple structure, convenient to use, the molecular sieve rate of recovery is high, energy -conservation, the waste liquid discharges fewly.

Description

A kind of device being continuously separated superfine molecular sieves from slurries
Technical field
The utility model relates to a kind of superfine molecular sieves retracting device, especially a kind of device being continuously separated superfine molecular sieves from slurries.
Background technology
In general, industrial sieve particle diameter is less, utilize production equipment separation and recovery molecular sieve from molecular sieve pulp more difficult, and existing be continuously separated from molecular sieve pulp ultra-fine titanium silicon, pure silicon, Si-Al molecular sieve there is bulky complex in device, energy consumption is high, yield is low, cannot realize the shortcomings such as continued operation, repeatability and poor stability, the production scale of serious restriction superfine molecular sieves and application in the industry thereof.
Utility model content
Technical problem to be solved in the utility model is to provide a kind of device being continuously separated superfine molecular sieves from slurries, and described device can realize continued operation, can obtain again the higher molecular sieve rate of recovery.
In order to solve the problems of the technologies described above, the technical solution of the utility model is achieved in that
From slurries, be continuously separated a device for superfine molecular sieves, described device comprises feed sump, tank reactor, subsider and self-action filter centrifugal; Feed sump bottom discharge mouth is communicated with the first tubing pump entrance by the first pipeline, the first pipeline is provided with the first ball valve, feeding mouth in the middle part of the first tubing pump outlet tank reactor; Tank reactor bottom discharge mouth is communicated with second pipe pump intake by second pipe, second pipe is provided with the second ball valve, and second pipe pump discharge is communicated with subsider bottom feeding mouth; Subsider bottom discharge mouth is communicated with self-action filter centrifugal feeding mouth by the 3rd pipeline, the 3rd pipeline is provided with the 3rd ball valve.
Further, described feed sump is provided with emptying device, the gas produced in feed sump is arranged outward through emptying device;
Further, described tank reactor is provided with 3 charging apertures, adds settling aids by charging aperture in tank reactor;
Further, described subsider is provided with overfall, the supernatant liquor in subsider flows out through overfall;
Further, described feed sump is provided with feed arrangement, deposits for material liquid is delivered to feed sump;
Further, be provided with the first inner coil pipe and agitating device in described feed sump, material liquid is stirred in feed sump, and cools with the first inner coil pipe, and the material liquid uniform decrease in temperature in feed sump, has gas to produce;
Further, be provided with the second inner coil pipe and propeller agitator in described tank reactor, material liquid mixes with settling aids, stirs under the propeller agitator effect in tank reactor, mixed liquor generation sedimentation reaction, and the second inner coil pipe continues to cool to mixed liquor;
Further, establish separating, washing device in described self-action filter centrifugal, the sedimentation enrichment slurries flowed out by subsider, after the separation of self-action filter centrifugal, washing, obtain highly purified molecular sieve filter cake.
The utility model beneficial effect compared to existing technology:
The utility model structure is simple, and easy to use, the molecular sieve rate of recovery is high, energy-conservation, and discharging of waste liquid is few.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
In figure: 1-feed sump; 2-first ball valve; 3-first tubing pump; 4-tank reactor; 5-second ball valve; 6-second pipe pump; 7-subsider; 8-the 3rd ball valve; 9-self-action filter centrifugal; 10-emptying device; 11-charging aperture; 12-overfall.
Detailed description of the invention
Below in conjunction with accompanying drawing, the utility model is described in further detail.
As shown in Figure 1, a kind of device being continuously separated superfine molecular sieves from slurries, described device comprises feed sump 1, tank reactor 4, subsider 7 and self-action filter centrifugal 9;
On the basis of technique scheme, further provide following more detailed and concrete technical scheme, described feed sump 1 bottom discharge mouth is communicated with the first tubing pump 3 entrance by the first pipeline, first pipeline is provided with feeding mouth in the middle part of the first ball valve 2, first tubing pump 3 outlet tank reactor 4; Feed sump 1 is provided with emptying device 10, the gas produced in feed sump 1 is through the outer row of emptying device 10; Feed sump 1 being provided with feed arrangement, depositing for material liquid being delivered to feed sump 1; Be provided with the first inner coil pipe and agitating device in feed sump 1, material liquid is stirred in feed sump 1, and cools with the first inner coil pipe, and the material liquid uniform decrease in temperature in feed sump 1, has gas to produce;
Tank reactor 4 bottom discharge mouth is communicated with second pipe pump intake by second pipe, second pipe is provided with the second ball valve 5, second pipe pump 6 outlet subsider 7 bottom feeding mouth; Tank reactor 4 is provided with 3 charging apertures 11, adds settling aids by charging aperture 11 in tank reactor 4; The second inner coil pipe and propeller agitator is provided with in tank reactor 4, material liquid mixes with settling aids, stir under propeller agitator effect in tank reactor 4, mixed liquor generation sedimentation reaction, and also the second inner coil pipe continues to cool to mixed liquor;
Subsider 7 bottom discharge mouth is communicated with self-action filter centrifugal 9 feeding mouth by the 3rd pipeline, the 3rd pipeline is provided with the 3rd ball valve 8; Subsider 7 is provided with overfall 12, the supernatant liquor in subsider 7 flows out through overfall 12; After establishing separating, washing device in self-action filter centrifugal 9, the sedimentation enrichment slurries flowed out by subsider 7 are separated through self-action filter centrifugal 9, washing, obtain highly purified molecular sieve filter cake.
The workflow of the utility model device:
Material liquid is stirred in feed sump 1, and lower the temperature with the first inner coil pipe, gas is produced in feed sump 1, gas emits through emptying device 10, slurries from feed sump 1 through with the first ball valve 2, first tubing pump 3 is to the middle part charging of tank reactor 4, add settling aids through charging aperture 11 to mix with slurries, stirring with propeller agitator in tank reactor 4 makes it that sedimentation reaction occur, and lower the temperature further with the second inner coil pipe in tank reactor 4, through the second ball valve 5 second pipe pump 6, slurries are transported to subsider 7 bottom by tank reactor 4 again, the clear liquid on subsider 7 top flows out through overfall 12, sedimentation enrichment slurries bottom subsider 7 send into self-action filter centrifugal 9 through the 3rd ball valve 8, be separated through self-action filter centrifugal 9, highly purified molecular sieve filter cake is obtained after washing.
In sum, these are only preferred embodiment of the present utility model, be not intended to limit protection domain of the present utility model.All within spirit of the present utility model and principle, any amendment done, equivalent replacement, improvement etc., all should be included within protection domain of the present utility model.

Claims (8)

1. from slurries, be continuously separated a device for superfine molecular sieves, it is characterized in that: described device comprises feed sump (1), tank reactor (4), subsider (7) and self-action filter centrifugal (9); Feed sump (1) bottom discharge mouth is communicated with the first tubing pump (3) entrance by the first pipeline, the first pipeline is provided with the first ball valve (2), the first tubing pump (3) outlet tank reactor (4) middle part feeding mouth; Tank reactor (4) bottom discharge mouth is communicated with second pipe pump (6) entrance by second pipe, second pipe is provided with the second ball valve (5), second pipe pump (6) outlet subsider (7) bottom feeding mouth; Subsider (7) bottom discharge mouth is communicated with self-action filter centrifugal (9) feeding mouth by the 3rd pipeline, the 3rd pipeline is provided with the 3rd ball valve (8).
2. a kind of device being continuously separated superfine molecular sieves from slurries according to claim 1, is characterized in that: described feed sump (1) is provided with emptying device (10).
3. a kind of device being continuously separated superfine molecular sieves from slurries according to claim 1, is characterized in that: described tank reactor (4) is provided with 3 charging apertures (11).
4. a kind of device being continuously separated superfine molecular sieves from slurries according to claim 1, is characterized in that: described subsider (7) is provided with overfall (12).
5. a kind of device being continuously separated superfine molecular sieves from slurries according to claim 1, is characterized in that: described feed sump (1) is provided with feed arrangement.
6. a kind of device being continuously separated superfine molecular sieves from slurries according to claim 1, is characterized in that: be provided with the first inner coil pipe and agitating device in described feed sump (1).
7. a kind of device being continuously separated superfine molecular sieves from slurries according to claim 1, is characterized in that: be provided with the second inner coil pipe and propeller agitator in described tank reactor (4).
8. a kind of device being continuously separated superfine molecular sieves from slurries according to claim 1, is characterized in that: establish separating, washing device in described self-action filter centrifugal (9).
CN201520701812.9U 2015-09-11 2015-09-11 Device of superfine molecular sieve of continuous separation in follow thick liquid Active CN204911013U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201520701812.9U CN204911013U (en) 2015-09-11 2015-09-11 Device of superfine molecular sieve of continuous separation in follow thick liquid

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201520701812.9U CN204911013U (en) 2015-09-11 2015-09-11 Device of superfine molecular sieve of continuous separation in follow thick liquid

Publications (1)

Publication Number Publication Date
CN204911013U true CN204911013U (en) 2015-12-30

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Country Status (1)

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CN (1) CN204911013U (en)

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