CN204873852U - Equipment of high -efficient production chlorination graphite alkene - Google Patents
Equipment of high -efficient production chlorination graphite alkene Download PDFInfo
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- CN204873852U CN204873852U CN201520613757.8U CN201520613757U CN204873852U CN 204873852 U CN204873852 U CN 204873852U CN 201520613757 U CN201520613757 U CN 201520613757U CN 204873852 U CN204873852 U CN 204873852U
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Abstract
The utility model provides an equipment of high -efficient production chlorination graphite alkene, retrieve jar, nitrogen gas storage tank, waste gas recovery treater including raw materials storage tank, pyroreaction jar, product aftertreatment jar, chlorine storage tank, chlorine, link to each other through the pipeline between each part, raw materials storage tank outer joint vacuum pump, it opens one to be equipped with the unloading between raw materials storage tank and the pyroreaction jar, be equipped with chlorine flow control controller between pyroreaction jar and the chlorine storage tank, and be equipped with chlorine recovery valve between the chlorine recovery jar, be equipped with unloading switch no. 2 between pyroreaction jar and the product aftertreatment jar, be equipped with nitrogen gas flow control controller between product aftertreatment jar and the nitrogen gas storage tank, and be equipped with the tail gas treatment valve between the waste gas recovery treater, raw materials storage tank and product aftertreatment jar all have the installation stirring rake, and pyroreaction jar side is equipped with agitating unit. This equipment has in succession the advantage that uninterruptedly prepared the product in a large number, and pollution -free, low in production cost, and equipment is simple.
Description
Technical field
The utility model relates to Graphene production unit technical field, is specifically related to a kind of High-efficient Production chlorination Graphene equipment.
Background technology
Graphene be a kind of by monolayer carbon atom with sp
2the hexangle type lattice two dimensional crystal of hybridized orbital composition, there is very high specific surface area, the character that the mechanical property of good conduction, thermal conductivity and excellence etc. are unique, makes it be with a wide range of applications in electrode materials, high strength composite, transistor, sensor.Graphene is the semi-metal semiconductor material of class zero band gap, by carrying out element doping to it thus the energy band structure of change material, optical property and electrical properties, become a kind of brand-new composite nano material, this nano material has played great effect at numerous areas such as opto-electronic device, novel material and new forms of energy.
Chlorination Graphene is a kind of novel nano material, is a kind of important derivatives of Graphene.At present, the research of chlorination Graphene is relatively less, mainly all rests on laboratory stage, and the subject matter that its production unit exists is high to the requirement of equipment, and complicated operation, preparation efficiency is low, is difficult to the needs meeting scale operation.China Patent No. CN103111312A discloses " a kind of chlorine doped graphene and preparation method thereof and application ", the magnesium rod activation methyl chloride of this invention burning, generate dichlorocarbene, these dichlorocarbenes again self-assembly generate chlorine doped graphene, obtained chlorine doped graphene catalytic activity is good, can be used as cathode catalysis material to apply in oxygen reduction electrode, but the method needs to carry out separating for several times, precipitation, washing to product, it is periodical operation, and aftertreatment comparatively bothers, be not suitable for scale operation.
To sum up, how to provide a kind of production process simple, the equipment of with low cost and high quality chlorination Graphene large-scale production, has become one of this area important topic needing solution badly.
Summary of the invention
Technical problem to be solved in the utility model is the equipment proposing a kind of High-efficient Production chlorination Graphene; there is the advantage that can prepare in a large number uninterruptedly; and it is pollution-free; production cost is low; equipment is simple; easily be automated and suitability for industrialized production, and the problem of high quality chlorination Graphene large-scale production can be solved.
To achieve these goals, solution of the present utility model is:
An equipment for High-efficient Production chlorination Graphene, comprises raw material storage tank, pyroreaction tank, product aftertreatment tank, chlorine storage tank, chlorine withdrawing can, nitrogen storage tank, waste gas recovery treater, is connected between each several part by pipeline; Raw material storage tank connects vacuum pump outward; Be provided with blanking between raw material storage tank and pyroreaction tank and open one; Be provided with chlorine flowrate adjustment control between pyroreaction tank and chlorine storage tank, and be provided with chlorine between chlorine withdrawing can and reclaim valve; Blanking switch two is provided with between pyroreaction tank and product aftertreatment tank; Be provided with nitrogen flow adjustment control between product aftertreatment tank and nitrogen storage tank, and be provided with vent gas treatment valve between waste gas recovery treater; Raw material storage tank and product aftertreatment tank all have installation stirring rake, and pyroreaction tank side is provided with whipping appts.
Described pyroreaction tank top is provided with opening for feed and air outlet, and both sides are provided with heating cooling jacket, and bottom is provided with feed opening and inlet mouth, and left side is provided with whipping appts, and whipping appts comprises agitator motor, rotating shaft, dispersion leaf, dispersed with stirring dish.
Feature of the present utility model and beneficial effect:
(1) raw material storage tank can provide the reaction mass after vacuum-drying at any time easily, realizes the continuity of chlorination Graphene production process;
(2) setting of high-temperature reactor side agitator improves the contact efficiency of graphene powder and chlorine, is conducive to the degree of depth chlorination realizing Graphene, improves product quality;
(3) be provided with chlorine withdrawing can and waste gas recovery treater, improve the utilization ratio of chlorine on the one hand, on the other hand aftertreatment is carried out to tail gas, without producing environmental pollution;
(4) production unit structure is simple, and operation steps is few, and production efficiency is high, easily is automated and suitability for industrialized production, is of great practical significance.
Accompanying drawing explanation
Fig. 1 is the structural representation of a kind of High-efficient Production chlorination Graphene described in the utility model;
Fig. 2 is the front view of pyroreaction tank described in the utility model;
Description of reference numerals: 1 is raw material storage tank, 2 is blanking switch one, 3 is pyroreaction tank, 3-1 is opening for feed, 3-2 is air outlet, 3-3 is heating cooling jacket, 3-4 is agitator motor, 3-5 is dispersion leaf, 3-6 is dispersed with stirring dish, 3-7 is inlet mouth, 3-8 is feed opening, 4 is blanking switch two, 5 is product aftertreatment tank, 6 is vacuum pump, 7 is chlorine storage tank, 8 is chlorine flowrate adjustment control, 9 is chlorine recovery valve, 10 is chlorine withdrawing can, 11 is nitrogen storage tank, 12 is nitrogen flow adjustment control, 13 is vent gas treatment valve, 14 is waste gas recovery treater.
Embodiment
In order to better understand the utility model, illustrate content of the present utility model further below in conjunction with embodiment, but the utility model content is not only confined to following specific embodiment.
As Fig. 1,2 known, a kind of equipment of High-efficient Production chlorination Graphene, comprise raw material storage tank 1, pyroreaction tank 3, product aftertreatment tank 5, chlorine storage tank 7, chlorine withdrawing can 10, nitrogen storage tank 11, waste gas recovery treater 14, be connected by pipeline between each several part; Raw material storage tank connects vacuum pump 6 outward; Be provided with blanking between raw material storage tank and pyroreaction tank and open 1; Be provided with chlorine flowrate adjustment control 8 between pyroreaction tank and chlorine storage tank, and be provided with chlorine between chlorine withdrawing can and reclaim valve 9; Blanking switch 24 is provided with between pyroreaction tank and product aftertreatment tank; Be provided with nitrogen flow adjustment control 12 between product aftertreatment tank and nitrogen storage tank, and be provided with vent gas treatment valve 13 between waste gas recovery treater; Raw material storage tank and product aftertreatment tank all have installation stirring rake, and pyroreaction tank side is provided with whipping appts.
Described pyroreaction tank top is provided with opening for feed 3-1 and air outlet 3-2, both sides are provided with heating cooling jacket 3-3, bottom is provided with inlet mouth 3-7 and feed opening 3-8, and left side is provided with whipping appts, and whipping appts comprises agitator motor 3-4, rotating shaft, dispersion leaf 3-5, dispersed with stirring dish 3-6.
The above, be only the utility model preferred embodiment, therefore once can not limit the scope that the utility model implements, the equivalence namely done according to the utility model claim and description change with modify, all should still belong in scope that the utility model patent contains.
Claims (2)
1. the equipment of a High-efficient Production chlorination Graphene, it is characterized in that: this equipment comprises raw material storage tank, pyroreaction tank, product aftertreatment tank, chlorine storage tank, chlorine withdrawing can, nitrogen storage tank, waste gas recovery treater, be connected by pipeline between each several part; Raw material storage tank connects vacuum pump outward; Be provided with blanking between raw material storage tank and pyroreaction tank and open one; Be provided with chlorine flowrate adjustment control between pyroreaction tank and chlorine storage tank, and be provided with chlorine between chlorine withdrawing can and reclaim valve; Blanking switch two is provided with between pyroreaction tank and product aftertreatment tank; Be provided with nitrogen flow adjustment control between product aftertreatment tank and nitrogen storage tank, and be provided with vent gas treatment valve between waste gas recovery treater; Raw material storage tank and product aftertreatment tank all have installation stirring rake, and pyroreaction tank side is provided with whipping appts.
2. the equipment of High-efficient Production chlorination Graphene according to claim 1, it is characterized in that pyroreaction tank top is provided with opening for feed and air outlet, both sides are provided with heating cooling jacket, bottom is provided with feed opening and inlet mouth, left side is provided with whipping appts, and whipping appts comprises agitator motor, rotating shaft, dispersion leaf, dispersed with stirring dish.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520613757.8U CN204873852U (en) | 2015-08-14 | 2015-08-14 | Equipment of high -efficient production chlorination graphite alkene |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520613757.8U CN204873852U (en) | 2015-08-14 | 2015-08-14 | Equipment of high -efficient production chlorination graphite alkene |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204873852U true CN204873852U (en) | 2015-12-16 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520613757.8U Active CN204873852U (en) | 2015-08-14 | 2015-08-14 | Equipment of high -efficient production chlorination graphite alkene |
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| Country | Link |
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| CN (1) | CN204873852U (en) |
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2015
- 2015-08-14 CN CN201520613757.8U patent/CN204873852U/en active Active
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