CN204824171U - Automatic hydrogenation purification device of nitrogen gas - Google Patents

Automatic hydrogenation purification device of nitrogen gas Download PDF

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Publication number
CN204824171U
CN204824171U CN201520368720.3U CN201520368720U CN204824171U CN 204824171 U CN204824171 U CN 204824171U CN 201520368720 U CN201520368720 U CN 201520368720U CN 204824171 U CN204824171 U CN 204824171U
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China
Prior art keywords
nitrogen
hydrogenation
nitrogen gas
automatic
pipeline
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Expired - Fee Related
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CN201520368720.3U
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Chinese (zh)
Inventor
王才华
高宗会
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Wuxi Zhongrui Air Separation Equipment Co Ltd
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Wuxi Zhongrui Air Separation Equipment Co Ltd
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Abstract

The utility model provides an automatic hydrogenation purification device of nitrogen gas, including nitrogen gas pipeline, hydrogen pipeline and deoxidation tower, the nitrogen gas pipeline includes first end and second end, the first end of nitrogen gas pipeline enters the mouth for nitrogen gas, the second end and the deoxidation tower of nitrogen gas pipeline are connected, the hydrogen pipeline includes first end and second end, the first end of hydrogen pipeline enters the mouth for hydrogen, the nitrogen gas pipeline is connected to the second end that the trachea was said, be equipped with the hydrogenation controller on the hydrogen pipeline. The utility model relates to an automatic hydrogenation purification device of nitrogen gas, the nitrogen gas purity produced of separation be more than 99.999%, has not the fluctuation of yin wendu and pressure and loses standard, good reproducibility, automatic survey control, operating pressure scope characteristics such as extend. Changed exist in the artifical manual hydrogenation when adjusting untimely, hydrogenation for a long time less, high pure nitrogen oxygen content is unstable, consume the hydrogen volume big, can not satisfy and lead to the fact the unstable shortcoming of product quality with the nitrogen requirement.

Description

A kind of Automatic-hydrogenation nitrogen purifying plant
Technical field
The utility model relates to gas purification field, particularly relates to nitrogen purification.
Background technology
Nitrogen is a kind of gas of colorless and odorless under normal condition, and usually nontoxic.78.12% (volume fraction) of nitrogen duty gas total amount, the gas density under normal conditions is 1.25g/L, and nitrogen is insoluble in water, at normal temperatures and pressures, approximately only dissolves the nitrogen of 0.02 volume in 1 volume water.Nitrogen is the gas of difficult liquefaction.
Nitrogen gathers to have in industrial production and greatly acts on, and can need nitrogen in a lot of industrial production, and therefore purification nitrogen has become the urgently problem that solves of people.
The way of existing nitrogen purification generally adopts, and liquefied air extracts nitrogen, a standard atmosphere pressure, utilize nitrogen purification nitrogen different from the liquefaction temperature of oxygen, but the nitrogen gas purity that this way is extracted is lower.
Some are also had to adopt the way of pressure swing adsorption air separation, namely be raw material with air, sorbent material is made with carbonaceous molecular sieve, utilize carbonaceous molecular sieve to the characteristic of the oxygen in air and nitrogen adsorption selection, use pressure-variable adsorption principle (pressurized adsorbent, decompression desorb also makes regenerating molecular sieve) and at normal temperature, oxygen is separated to produce nitrogen with nitrogen, the nitrogen gas purity that this method is produced is about 97% ~ 99.5%, but purity still can not reach the requirement that some special occasions use nitrogen.
Utility model content
The technical problems to be solved in the utility model overcomes existing defect, provides a kind of Automatic-hydrogenation nitrogen purifying plant, greatly improve the concentration of extracted nitrogen.
In order to solve the problems of the technologies described above, the utility model provides following technical scheme:
A kind of Automatic-hydrogenation nitrogen purifying plant, comprise nitrogen pipeline, Hydrogen Line and deoxidation tower, described nitrogen pipeline comprises first end and the second end, and the first end of described nitrogen pipeline is nitrogen inlet, and the second end of described nitrogen pipeline is connected with deoxidation tower; Described Hydrogen Line comprises first end and the second end, and the first end of described Hydrogen Line is hydrogen inlet, and the second end of described feed channel connects nitrogen pipeline; Described Hydrogen Line is provided with hydrogenation controller.
Further, described hydrogenation controller is the valve that automatically can regulate according to signal.
Further, described hydrogenation controller is intelligent hydrogenation controller.
Further, described intelligent hydrogenation controller unidirectional connection PLC, described PLC connects oxygen analyser and nitrogen gas stream gauge.
Further, the output signal of described oxygen analyser is 4-20mA.
Further, the output signal of described nitrogen gas stream gauge is 4-20mA.
A kind of Automatic-hydrogenation nitrogen purifying plant of the utility model, being separated the nitrogen gas purity produced is more than 99.999%, has not misalignment, the feature such as reproducible, automatic measurement and control, working pressure range are wide because of the fluctuation of temperature and pressure.Change also exist in hydrogenation manually adjustment not in time, hydrogenation time many time few, High Purity Nitrogen oxygen level unstable, hydrogen-consuming volume large, can not meet the shortcoming causing unstable product quality with nitrogen requirement.
Accompanying drawing explanation
Accompanying drawing is used to provide further understanding of the present utility model, and forms a part for specification sheets, is used from explanation the utility model, does not form restriction of the present utility model with embodiment one of the present utility model.In the accompanying drawings:
Fig. 1 is structural representation of the present utility model.
Embodiment
Below in conjunction with accompanying drawing, preferred embodiment of the present utility model is described, should be appreciated that preferred embodiment described herein is only for instruction and explanation of the utility model, and be not used in restriction the utility model.
As shown in Figure 1, a kind of Automatic-hydrogenation nitrogen purifying plant of the utility model, comprise nitrogen pipeline 1, Hydrogen Line 2 and deoxidation tower 3, described nitrogen pipeline 1 comprises first end and the second end, the first end of described nitrogen pipeline 1 is nitrogen inlet, and the second end of described nitrogen pipeline 1 is connected with deoxidation tower 3; Described Hydrogen Line 2 comprises first end and the second end, and the first end of described Hydrogen Line 2 is hydrogen inlet, and the second end of described feed channel 2 connects nitrogen pipeline 1; Described Hydrogen Line 2 is provided with hydrogenation controller 4; Described hydrogenation controller 4 is valve or flange; Described hydrogenation controller 4 is intelligent hydrogenation controller; Described intelligent hydrogenation controller unidirectional connection PLC5, described PLC5 connects oxygen analyser 6 and nitrogen gas stream gauge 7; The output signal of described oxygen analyser 6 is 4-20mA; The output signal of described nitrogen gas stream gauge 7 is 4-20mA.
After general nitrogen access to plant, by after pressure regulation pressure regulating valve through Flow-rate adjustment valve regulating flow, enter oxygen-removing tower, flow is taken into account oxygen analyzer and is respectively exported 4 ~ 20mA signal simultaneously, these two signal input programmable logic controllers, the program of 2H2+O2=2H2O reaction formula setting is pressed by programmable controller, export 4 ~ 20mA signal to mass flow controller, quality controller is made automatically to control to add hydrogen amount, general nitrogen and hydrogen enter oxygen-removing tower after sufficiently mixing, under catalyst action, there is 2H2+O2=2H2O reaction, and release a large amount of heat, then the micro-oxygen in nitrogen is removed.
A kind of Automatic-hydrogenation nitrogen purifying plant of the utility model, being separated the nitrogen gas purity produced is more than 99.999%, has not misalignment, the feature such as reproducible, automatic measurement and control, working pressure range are wide because of the fluctuation of temperature and pressure.Change also exist in hydrogenation manually adjustment not in time, hydrogenation time many time few, High Purity Nitrogen oxygen level unstable, hydrogen-consuming volume large, can not meet the shortcoming causing unstable product quality with nitrogen requirement.
The foregoing is only preferred embodiment of the present utility model, be not limited to the utility model, although be described in detail the utility model with reference to previous embodiment, for a person skilled in the art, it still can be modified to the technical scheme described in foregoing embodiments, or carries out equivalent replacement to wherein portion of techniques feature.All within spirit of the present utility model and principle, any amendment done, equivalent replacement, improvement etc., all should be included within protection domain of the present utility model.

Claims (6)

1. an Automatic-hydrogenation nitrogen purifying plant, comprise nitrogen pipeline, Hydrogen Line and deoxidation tower, it is characterized in that: described nitrogen pipeline comprises first end and the second end, the first end of described nitrogen pipeline is nitrogen inlet, and the second end of described nitrogen pipeline is connected with deoxidation tower; Described Hydrogen Line comprises first end and the second end, and the first end of described Hydrogen Line is hydrogen inlet, and the second end of described feed channel connects nitrogen pipeline; Described Hydrogen Line is provided with hydrogenation controller.
2. a kind of Automatic-hydrogenation nitrogen purifying plant according to claim 1, is characterized in that: described hydrogenation controller is the valve that automatically can regulate according to signal.
3. a kind of Automatic-hydrogenation nitrogen purifying plant according to claim 1, is characterized in that: described hydrogenation controller is intelligent hydrogenation controller.
4. a kind of Automatic-hydrogenation nitrogen purifying plant according to claim 3, is characterized in that: described intelligent hydrogenation controller unidirectional connection PLC, and described PLC connects oxygen analyser and nitrogen gas stream gauge.
5. a kind of Automatic-hydrogenation nitrogen purifying plant according to claim 4, is characterized in that: the output signal of described oxygen analyser is 4-20mA.
6. a kind of Automatic-hydrogenation nitrogen purifying plant according to claim 4, is characterized in that: the output signal of described nitrogen gas stream gauge is 4-20mA.
CN201520368720.3U 2015-05-29 2015-05-29 Automatic hydrogenation purification device of nitrogen gas Expired - Fee Related CN204824171U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201520368720.3U CN204824171U (en) 2015-05-29 2015-05-29 Automatic hydrogenation purification device of nitrogen gas

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201520368720.3U CN204824171U (en) 2015-05-29 2015-05-29 Automatic hydrogenation purification device of nitrogen gas

Publications (1)

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CN204824171U true CN204824171U (en) 2015-12-02

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111847399A (en) * 2020-08-27 2020-10-30 杭州普昌科技有限公司 Efficient nitrogen purification device and purification process
CN115215304A (en) * 2021-04-16 2022-10-21 无锡市中瑞空分设备有限公司 Modular nitrogen making machine

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111847399A (en) * 2020-08-27 2020-10-30 杭州普昌科技有限公司 Efficient nitrogen purification device and purification process
CN111847399B (en) * 2020-08-27 2021-08-31 杭州普昌科技有限公司 Efficient nitrogen purification device and purification process
CN115215304A (en) * 2021-04-16 2022-10-21 无锡市中瑞空分设备有限公司 Modular nitrogen making machine
CN115215304B (en) * 2021-04-16 2023-09-19 无锡市中瑞空分设备有限公司 Modularized nitrogen making machine

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20151202

Termination date: 20160529

CF01 Termination of patent right due to non-payment of annual fee